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50results about How to "No evaporation" patented technology

Selective-oxidized chitosan and heterogeneous preparation method thereof

InactiveCN107474161AHigh oxidation selectivityMild reaction conditionsSolubilityReaction rate
The invention discloses a selective-oxidized chitosan and a heterogeneous preparation method thereof. The method is characterized in that according to preparation of the oxidized chitosan, macromolecular chitosan is dissolved in an ionic liquid, the chitosan is precipitated from the ionic liquid by adding absolute ethyl alcohol, and porous chitosan is obtained after the ionic liquid in a precipitation is fully replaced through absolute ethyl alcohol dipping and ultrasonic oscillation; the porous chitosan is moistened and expanded in the ionic liquid to form a semisolid gel with certain viscosity, and then partial or all hydroxyls at C6 position in pyranose rings of the chitosan are selectively oxidized into carboxyls in an ionic liquid medium to obtain the selective-oxidized chitosan with adoption of a concentrated nitric acid-concentrated phosphoric acid-sodium nitrite system. According to the method, operation is simple and convenient, the oxidation reaction rate is high, the oxidation degree of the chitosan is easily controlled, oxidation products are easy to separate, the yield of the products is high, the prepared carboxyl chitosan has good antibacterial activity and water solubility, and the ionic liquid can be recycled for cyclic utilization, which is environmentally friendly.
Owner:TAIHE KERUNGE GARMENT CO LTD

Technology for producing boracic acid and monohydrate magnesium sulfate by employing ascharite ore sulfuric acid process

The invention relates to a technique for preparing boracic acid and magnesium sulfate monohydrate by utilizing ascharite sulfuric acid process. The method drives mother liquid and washing water to be heated to have acidolysis with ascharite powder and sulfuric acid when returned to an acidolysis tank; acid decomposing liquid is pumped into a magnesium extracting machine after filtering while hot; temperature in the magnesium extracting machine is raised and crystal magnesium sulfate monohydrate is separated out at a constant temperature while the boracic acid stays in liquid phase and magnesium sulfate monohydrate products are obtained after filtering and drying while hot. Filtrate is pumped into a boracic acid crystallizer and cooled to crystallize according to a well-known way and boracic acid products are obtained after centrifugal separation, washing with added water and drying. The mother liquid and washing water of the boracic acid return to acidolysis process for reusing. The invention solves the problem that a large discharge amount of mother liquid of the boracic acid is changed to be completely recycled. About a ton of magnesium sulfate monohydrate and 200 kilograms of boracic acid can be recycled from the mother liquid in production of each ton of boracic acid. The invention saves resources, reduces environmental pollution and promotes economic benefit of enterprises, thus being characterized by little investment, low energy consumption, low cost and high benefit.
Owner:李皛

Method for quantitatively measuring baicalein and wogonin in scutellaria baicalensis simultaneously

InactiveCN102128889AThe method of proof is simpleQuick proof methodComponent separationPlant ingredientsPhosphoric acidLength wave
The invention discloses a self enzymolysis approach method of baicalein and wogonin in scutellaria baicalensis. The measurement method disclosed by the invention comprises the following steps of: carrying out enzymolysis on saponin compounds, such as baicalin, wogonoside, and the like in an aqueous solution by utilizing enzyme contained in scutellaria baicalensis at a proper temperature; after finishing enzymolysis, adding acid methanol; maintaining the stability of the baicalein when killing scutellaria baicalensis enzyme; fully dissolving emzymatically-decomposed baicalein; and filtering and adding filtered liquid as a sample solution. The baicalein and wogonin in the scutellaria baicalensis are simultaneously measured by an HPLC (High Performance Liquid Chromatography) by using a methanol-0.1 percent phosphoric acid solution with the volume ratio of (51-54):(49-46) as a mobile phase and 275nm as a detecting wavelength. The method has the advantages of simplicity, convenience, high speed, complete enzymolysis of components to be detected, and favorable wave crest separation. The self enzymolysis approach method of baicalein and wogonin in scutellaria baicalensis is reported for the first time and provides real basic content data for the full extraction and separation of the components. A content practical measured value of the baicalein is larger than a theoretical value calculated by molecular weights of baicalin and baicalein.
Owner:北京赛尔泰和生物医药科技有限公司

HPLC (High Performance Liquid Chromatography) quantitative method for cephaeline hydrochloride and ipecine hydrochloride in ipecacuanha medicinal material and preparation of ipecacuanha medicinal material

The invention relates to a HPLC (High Performance Liquid Chromatography) quantitative method for cephaeline hydrochloride and ipecine hydrochloride in an ipecacuanha medicinal material and a preparation of ipecacuanha medicinal material. The method is characterized by comprising the following steps: firstly, performing common isocratic elution according to PHLC method, and taking acetonitrile-carbinol-0.1% of phosphoric acid at a volume ratio of (8-9.5):(3-5):(86-88) as a flowing phase, wherein a detecting wavelength is 205nm; and simultaneously measuring the contents of the cephaeline hydrochloride and ipecine hydrochloride in the ipecacuanha medicinal material and a fluid extract, extract and tincture thereof so as to end the history of the measurement of total alkaloids of the ipecacuanha alkaloids in an acid base titration form according to the standard in multiple countries: after performing column chromatography separation for 4 times, respectively measuring the cephaeline hydrochloride and ipecine hydrochloride through delta A at 283nm and 350nm by adopting differential spectrophotometry. According to the method, only acidic aqueous carbinol or aqueous carbinol is used; after fine powder of the medicinal material is ultrasonically extracted or each preparation is diluted, a certain amount of subsequent filtrate is absorbed; and an alumina column is used for removing impurities so as to measure. The method is quick, convenient, accurate and capable of reappearing.
Owner:JING JING PHARMA

Electric heating plate with unbalanced fins shaped like Chinese character 'feng' and heating and humidification device

ActiveCN103791621AAvoid threadingOvercome or even eliminate thermal resistanceAir heatersHeating element materialsChinese charactersEvaporation
The invention provides an electric heating plate with unbalanced fins shaped like a Chinese character 'feng'. The electric heating plate with the unbalanced fins shaped like the Chinese character 'feng' comprises a substrate, wherein S-shaped electric heating tubes are cast in the substrate, air heating fins and evaporation fins are cast on the two sides of the substrate respectively, a separating plate is arranged at the front end of the substrate in an extension mode, and is used for isolation between a main ventilation area and a water mist evaporation area, evaporation baffles are arranged on the left side and the right side of the evaporation fins respectively, and the evaporation fins are thin and high. The invention further provides a heating and humidification device. The heating and humidification device comprises a heat-insulating shell, wherein an air suction inlet and an exhaust outlet are formed in the two ends of the heat-insulating shell respectively, and centrifugal fans, nozzles, the electric heating plate with the unbalanced fins shaped like the Chinese character 'feng' and a gas-and-steam mixing area are arranged in sequence from the air suction inlet. According to the electric heating plate with the unbalanced fins shaped like the Chinese character 'feng' and the heating and humidification device, the mode that operation of heating drying and operation of water supply vaporization humidification are independently carried out or are carried out in parallel is achieved, and the effects that the main ventilation area is free of water scale and the water mist evaporation area is descaled in a thermal shock mode are ensured.
Owner:浙江鼎美智装股份有限公司

Low-temperature liquid filling method and system for detecting evaporation rate of low-temperature heat insulation gas bottle

The invention discloses a low-temperature liquid filling method and system for detecting the evaporation rate of a low-temperature heat insulation gas bottle. The method comprises the following stepsthat the low-temperature heat insulation gas bottle is preheated, an emptying valve and a bypass valve are opened, the bypass valve communicates with a low-temperature storage tank, a main valve is closed, the bypass valve conducts second-time pre-cooling on the low-temperature heat insulation gas bottle with the first preset filling mass rate, large-flow filling of the low-temperature heat insulation gas bottle is conducted, the aperture of an electric valve is increased, the main valve is opened, the bypass valve is closed, the low-temperature heat insulation gas bottle is filled with liquidfrom the low-temperature storage tank with the second preset filling mass rate through the main valve via a rotational flow generator, and the process is stopped when the liquid mass in the low-temperature heat insulation gas bottle reaches the 75% filling rate; and the aperture of the electric valve is reduced, the low-temperature heat insulation gas bottle is filled with the liquid from the low-temperature storage tank with the third preset filling mass rate through the main valve via the rotational flow generator, the main valve is closed after filling is conducted to the rated filling rate, standing is conducted for the preset time till the inner liquid surface stops rotating, and filling is finished.
Owner:XI AN JIAOTONG UNIV +1

cigs solar cell film production line

The invention discloses a CIGS solar cell film production line. The CIGS solar cell film production line comprises a plurality of coating sub-lines. The sub-lines sequentially and independently conduct vertical coating on a film. Each sub-line at least comprises an unreeling chamber, a coating chamber and a reeling chamber in the film unfolding direction, wherein a main drive roller is arranged in the unreeling chamber and the reeling chamber, a plurality of transmission rollers are arranged in cavities of the sub-line, and a tension detection roller and a tension adjusting roller are arranged in at least one cavity of the sub-line. The tension detection rollers are adjacent to the tension adjusting rollers, the tension detection rollers are used for monitoring the tension of the film in real time, and the tension adjusting rollers adjust the rotation speed of the tension adjusting rollers according to the feedback of the tension detection rollers so as to adjust the transmission speed of the film in the cavities; and the tension adjusting rollers are non-transmission rollers, and the unfolding track that the film passes the tension detection rollers and the tension adjusting rollers is the nonlinear track. According to the provided CIGS solar cell film production line, the element diffusion path is short, intermediate products are avoided, element evaporation is avoided, the film efficiency is high, and the CIGS solar cell film production line is particularly suitable for large-area scale industrial production.
Owner:旭科新能源股份有限公司 +1

Isotope sample collection device for inhibiting evaporation and exchange of water sample

The invention belongs to the technical field of isotope collection devices, and particularly relates to an isotope sample collection device for inhibiting evaporation and exchange of a water sample. The isotope sample collection device comprises a sample storage container, a funnel and a water guide pipe, wherein the sample storage container and the funnel are hermetically connected through the water guide pipe, the top end of the water guide pipe is hermetically communicated with a water leakage port at the bottom of the funnel, and a floating ball is placed at the bottom of the funnel; the bottom end of the water guide pipe extends into the bottom end of the sample storage container, a thread is arranged on the outer surface of the bottom end of the water guide pipe, a water outlet hole is formed above the thread, the bottom end of the water guide pipe is sleeved with a closed sleeve, and a thread is arranged at the bottom end in the closed sleeve and is matched and screwed with the thread at the bottom end of the water guide pipe; the bottom end of the funnel is further communicated with a pressure relief pipe which is arranged at the bottom of the floating ball, and the other end of the pressure relief pipe is communicated with the sample storage container. A small amount of rainfall is stored in the water guide pipe for the first time to form a small liquid level, and large-area water sample evaporation is avoided; the arrangement of the pressure relief pipe enables all rainfall in the funnel to flow into the sample storage container.
Owner:INST OF HYDROGEOLOGY & ENVIRONMENTAL GEOLOGY CHINESE ACAD OF GEOLOGICAL SCI

Method for preventing tube from scaling by using tubular heat exchanger for concentration of aqueous protein solution

The invention belongs to the technical field of bioengineering. In view of a technical problem that an existing tube is easy to scale, the invention provides a method for preventing a tube from scaling by using a tubular heat exchanger for concentration of an aqueous protein solution, wherein the method comprises a step of using the tubular heat exchanger for exchanging heat with the aqueous protein solution; the method is characterized in that an independent flash evaporation region is arranged above the interior of the tubular heat exchanger; a top end of the tube extends into the flash evaporation region; a tube cavity of the tube is always filled with a liquid material during heat exchanging operation; the heated liquid material is boiled in the flash evaporation region to form a gas-liquid mixture; an evaporation tank is also provided; the gas-liquid mixture in the flash evaporation region is injected into a material storage region at the bottom of the evaporation tank; gas-liquidseparation is performed by the evaporation tank; the concentrated aqueous protein solution is settled at the bottom of the evaporation tank; and an evaporated gas is discharged from an exhaust port in the top of the evaporation tank. The method provided by the invention has a beneficial effect of preventing the tube from drywall phenomenon to avoid occurrence of scaling in the tube.
Owner:荣成鸿德海洋生物科技有限公司

Large-area AZO glass coating film production line

The invention discloses a large-area AZO glass coating film production line, which comprises a coating film line and a conveying line, wherein the coating film line comprises an inlet chamber, an inlet buffer chamber, an inlet conveying chamber, a sputtering chamber, an outlet conveying chamber, an outlet buffer chamber, an outlet chamber and a quality inspection chamber, the inlet chamber, the inlet buffer chamber, the inlet conveying chamber, the sputtering chamber, the outlet conveying chamber, the outlet buffer chamber, the outlet chamber and the quality inspection chamber are sequentiallyconnected, at least a valve is arranged between the adjacent chambers, the conveying line comprises transmission rollers and a coating film quality inspection roller, the sequentially connected transmission rollers are respectively arranged in the inlet chamber, the inlet buffer chamber, the inlet conveying chamber, the sputtering chamber, the outlet conveying chamber, the outlet buffer chamber and the outlet chamber, the coating film quality inspection roller is arranged in the quality inspection chamber, the transmission roller in the outlet chamber is connected to the coating film qualityinspection roller, and the transmission rollers and the coating film quality inspection roller are used for conveying a coating film substrate. According to the present invention, with the large-areaAZO glass coating film production line, the large-batch and low-cost production of various large-area coating films can be achieved, the sputter deposition rate is high, the process has strong versatility, the diffusion path is short, no intermediate product is generated, and no element is evaporated, such that the preparation is fast, the efficiency is high, the yield rate is over 95%, and the production line is especially suitable for large-scale industrial production.
Owner:XIANGTAN HONGDA VACUUM TECH CO LTD

Multipurpose metal film layer vacuum coating production line

The invention discloses a multipurpose metal film layer vacuum coating production line. The production line comprises an inlet chamber, an inlet buffer chamber, an inlet conveying chamber, a sputtering chamber, an outlet conveying chamber, an outlet buffer chamber, an outlet chamber and a quality inspection chamber, wherein the inlet chamber, the inlet buffer chamber, the inlet conveying chamber,the sputtering chamber, the outlet conveying chamber, the outlet buffer chamber and the outlet chamber are connected in sequence; transferring rollers connected with each other are arranged in the inlet chamber, the inlet buffer chamber, the inlet conveying chamber, the sputtering chamber, the outlet conveying chamber, the outlet buffer chamber and the outlet chamber; a film coating quality inspection roller and a quality inspection system are arranged in the quality inspection chamber; the transferring roller in the outlet chamber is connected with the film coating quality inspection roller;and the transferring rollers and the film coating quality inspection roller are used for transferring a film coating substrate. According to the multipurpose metal film layer vacuum coating productionline, mass and low-cost production of various coatings are achieved with high sputtering deposition rate and strong process universality; an element diffusion path is short with no intermediate product and no element evaporation, so that the preparation speed and the efficiency are high, the yield is 95% or above, and the production line is particularly suitable for large-scale industrial production.
Owner:XIANGTAN HONGDA VACUUM TECH CO LTD

HPLC (High Performance Liquid Chromatography) quantitative method for cephaeline hydrochloride and ipecine hydrochloride in ipecacuanha medicinal material and preparation of ipecacuanha medicinal material

The invention relates to a HPLC (High Performance Liquid Chromatography) quantitative method for cephaeline hydrochloride and ipecine hydrochloride in an ipecacuanha medicinal material and a preparation of ipecacuanha medicinal material. The method is characterized by comprising the following steps: firstly, performing common isocratic elution according to PHLC method, and taking acetonitrile-carbinol-0.1% of phosphoric acid at a volume ratio of (8-9.5):(3-5):(86-88) as a flowing phase, wherein a detecting wavelength is 205nm; and simultaneously measuring the contents of the cephaeline hydrochloride and ipecine hydrochloride in the ipecacuanha medicinal material and a fluid extract, extract and tincture thereof so as to end the history of the measurement of total alkaloids of the ipecacuanha alkaloids in an acid base titration form according to the standard in multiple countries: after performing column chromatography separation for 4 times, respectively measuring the cephaeline hydrochloride and ipecine hydrochloride through delta A at 283nm and 350nm by adopting differential spectrophotometry. According to the method, only acidic aqueous carbinol or aqueous carbinol is used; after fine powder of the medicinal material is ultrasonically extracted or each preparation is diluted, a certain amount of subsequent filtrate is absorbed; and an alumina column is used for removing impurities so as to measure. The method is quick, convenient, accurate and capable of reappearing.
Owner:JING JING PHARMA

Manufacturing device for sludge solidification test samples

The invention relates to a manufacturing device for sludge solidification test samples and belongs to the technical field of environmental geotechnics.The manufacturing device for the sludge solidification test samples is composed of a storage system, a sample manufacturing system and an intelligent control rack system.A rubber bag is arranged in a piston cavity, a controllable feed port and a controllable discharge port are formed in the rubber bag, and it is guaranteed that no water evaporation or odor diffusion exists in the sample manufacturing process.By means of the mode of vacuum pumping and piston extrusion, it is guaranteed that initial raw materials are uniform and free of air, and sample manufacturing is rapid.A sample injection gun head is combined with a power compression piston controlled by a computer and a bearing table with an inductor, and it is guaranteed that a die cutting ring is tightly and fully filled with solidified sludge in the sample manufacturing process.The problems that more sample manufacturing materials are needed, consumed time is long, the samples are easily disturbed, holes are easily formed, the identity of the samples cannot be guaranteed, sample manufacturing is slow, the smell is heavy in the manufacturing process, and the reproduction of the samples is low are effectively solved through the manufacturing device.
Owner:LIAONING TECHNICAL UNIVERSITY

A Feng-shaped unbalanced fin electric heating plate and a heating and humidifying device

ActiveCN103791621BAvoid threadingOvercome or even eliminate thermal resistanceAir heatersHeating element materialsChinese charactersEvaporation
The invention provides an electric heating plate with unbalanced fins shaped like a Chinese character 'feng'. The electric heating plate with the unbalanced fins shaped like the Chinese character 'feng' comprises a substrate, wherein S-shaped electric heating tubes are cast in the substrate, air heating fins and evaporation fins are cast on the two sides of the substrate respectively, a separating plate is arranged at the front end of the substrate in an extension mode, and is used for isolation between a main ventilation area and a water mist evaporation area, evaporation baffles are arranged on the left side and the right side of the evaporation fins respectively, and the evaporation fins are thin and high. The invention further provides a heating and humidification device. The heating and humidification device comprises a heat-insulating shell, wherein an air suction inlet and an exhaust outlet are formed in the two ends of the heat-insulating shell respectively, and centrifugal fans, nozzles, the electric heating plate with the unbalanced fins shaped like the Chinese character 'feng' and a gas-and-steam mixing area are arranged in sequence from the air suction inlet. According to the electric heating plate with the unbalanced fins shaped like the Chinese character 'feng' and the heating and humidification device, the mode that operation of heating drying and operation of water supply vaporization humidification are independently carried out or are carried out in parallel is achieved, and the effects that the main ventilation area is free of water scale and the water mist evaporation area is descaled in a thermal shock mode are ensured.
Owner:浙江鼎美智装股份有限公司

Flexible film vertical vacuum coating production line

The invention discloses a vertical type vacuum coating production line for flexible thin films. The production line comprises multiple coating sublines, each subline is used for independently carryingout vertical type coating of thin films, each subline at least comprises an unreeling chamber, a coating chamber and a reeling chamber along the thin film expansion direction, a main drive roller isarranged in the unreeling chamber and the reeling chamber, multiple driving rollers are arranged in each chamber of the subline, and a tension force detection roller and a tension force adjusting roller are arranged in at least one chamber of the subline; wherein the tension force detection roller and the tension force adjusting roller are adjacently arranged, the tension force detection roller isused for real time monitoring tension of the thin film, the tension force adjusting roller is used for adjusting self rotating speed according to feedback of the tension force detection roller in order to adjust transmission speed of the thin film in each chamber, the tension force adjusting roller is a non-driving roller, and the expansion track of the thin film through the tension force detection roller and the tension force adjusting roller is a non-linear track. The vertical type vacuum coating production line for flexible thin films has the advantages of short element diffusion path without intermediate products and element evaporation, and high thin film efficiency; and the production line is especially suitable for large-area and large-scale industrial production.
Owner:XIANGTAN HONGDA VACUUM TECH CO LTD

Reactor capable of controllably loading multiple catalytic materials, coating device and preparation method

The invention discloses a reactor capable of controllably loading various catalytic materials, a coating device and a preparation method. A rotor of the coating device is provided with a plurality of capillary tube positioning structures for fixing capillary tubes, and when the capillary tubes are fixed on the capillary tube positioning structures and centrifuged by a centrifugal machine, the axis of the capillary tube is in a plane perpendicular to the axis of the rotating shaft, and the axis of the capillary tube does not coincide with any diameter of the rotating shaft. A catalytic reactor is prepared by adopting the coating equipment, a reactor capable of controllably loading multiple catalytic materials is obtained, and during centrifugation, the total length of the same capillary tube is controlled to be located on the same side of the middle axial surface of a rotating shaft perpendicular to the axis of the capillary tube. According to the invention, PDMS liquid is coated on the set area of the capillary tube, so that catalytic materials can be fixed in the set area of the capillary tube, and various catalytic materials can be loaded on the same capillary tube by changing the mounting angle of the capillary tube during each centrifugal operation.
Owner:山东优检生物技术有限公司 +1
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