3results about How to "Small crystal size" patented technology

The application discloses a high-density high-purity polycrystalline kaolinite preparation method under hot isostatic pressing conditions. –3 The steel ladle is placed in a graphite furnace cylinder body of a hot isostatic pressing high-pressure container, and a graphite sealing cover is covered on the steel ladle; argon is used as a pressure transmission medium, a multi-gradient cylinder body temperature and pressure increasing mode is adopted, the pressure in the cylinder sample bin is increased to 105.8 MPa, the temperature is increased to 800 DEG C, and the temperature and pressure are kept for 4.8 hours; a multi-gradient cylinder body temperature and pressure decreasing mode is adopted, the temperature in the cylinder sample bin is decreased to 177 DEG C, and the pressure is decreased to 71.8 MPa; finally, the pressure is released, the temperature is decreased to room temperature, and the polycrystalline kaolinite aggregate is obtained; and the technical blank of preparing a high-density polycrystalline kaolinite aggregate bulk body rich in aluminosilicate mineral experimental samples under high-temperature and high-pressure conditions is solved.

This invention discloses a method for preparing high-density, high-purity polycrystalline barite polymers under hot isostatic pressing conditions, wherein barite sample powder is compacted and sealed to a vacuum degree of 10. –3 The sample was placed in a steel cladding with dimensions of 55.89 mm outer diameter × 88.76 mm height × 3 mm wall thickness. The cladding was then placed inside the graphite furnace cylinder of a hot isostatic pressure vessel and sealed with a graphite cap. Using argon as the pressure transfer medium, a multi-gradient cylinder heating and pressurization method was employed to raise the temperature inside the sample chamber to 950 °C and the pressure to 112.5 MPa. This pressure and temperature were maintained for 6.0 hours. A multi-gradient cylinder cooling and depressurization method was then used to lower the temperature inside the sample chamber to 178 °C and the pressure to 71.1 MPa. The pressure was then released and the sample was cooled to room temperature to obtain a polycrystalline barite polymer. This method filled the technical gap in the preparation of bulk sulfate experimental samples of high-density polycrystalline barite polymers under high temperature and high pressure conditions.

The application discloses a preparation method of high-density high-densification polycrystalline trachyandesite under high-temperature high-pressure conditions. –3 The application discloses a preparation method of high-density high-densification polycrystalline trachyandesite under high-temperature high-pressure conditions, which comprises the following steps: completely sealing trachyandesite sample powder in a ladle cover with a vacuum degree of 10 –3 Pa; placing the ladle cover in a graphite furnace cylinder body of a high-pressure container of a hot isostatic pressing device, covering a graphite sealing cover; taking argon as a pressure transmission medium; adopting a multi-gradient hot isostatic pressing forming process of first increasing pressure and then increasing temperature to increase the temperature in the cylinder body sample bin to 950°C and the pressure to 91.5 MPa, and keeping constant temperature and constant pressure for 6.8 hours; adopting a multi-gradient cylinder body temperature and pressure decreasing mode to decrease the temperature in the cylinder body sample bin to 176°C and the pressure to 58.7 MPa; and finally, decreasing the pressure and temperature to room temperature to obtain a polycrystalline trachyandesite aggregate sample; and the technical blank of preparing a large bulk experimental sample of high-densification polycrystalline trachyandesite aggregate under high-temperature high-pressure conditions is solved.