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44results about How to "Spinnable" patented technology

Preparation method of spinnable polycarbosilane precursor material

The invention discloses a preparation method of a spinnable polycarbosilane precursor material. The preparation method includes the steps: placing polydimethyl silane into a pyrolysis kettle, openinga vacuum valve of the pyrolysis kettle, turning on a vacuum pump, closing the vacuum valve of the pyrolysis kettle when the pyrolysis kettle is vacuumized to be -0.08 to -0.09Mpa, opening a nitrogen valve of the pyrolysis kettle, leading in nitrogen, enabling the internal pressure of the pyrolysis kettle to be 0.04Mpa and maintaining the pressure for 20-24 hours; vacuumizing the pyrolysis kettle to be lower than -0.09Mpa, turning on a stirring device and a heating device of the pyrolysis kettle, heating the inside of the pyrolysis kettle to reach the temperature of 200 DEG C, keeping the temperature for 1-3 hours, continuously stirring the polydimethyl silane in the pyrolysis kettle at high temperature and low pressure to remove residual solvents of the polydimethyl silane, increasing thetemperature for pyrolysis, transferring the polydimethyl silane to a synthesis kettle and performing synthesis at the high temperature and high pressure to obtain polycarbosilane. A molecular chain inthe prepared polycarbosilane is good in linearity, branches on the molecular chain are fewer and less crossed, the polycarbosilane is moderate in viscosity and good in spinnability, the molecular weight of the prepared polycarbosilane is moderately 800-1300, and the polycarbosilane is the most spinnable.
Owner:福建立亚化学有限公司

Semi-dull high-strength low-elongation viscose fiber as well as preparation method and application thereof

The invention provides a semi-dull high-strength low-elongation viscose fiber as well as a preparation method and application thereof. The viscose fiber is obtained by sequentially performing soaking, grinding, squeezing crushing, kneading, directional polymerization reduction, yellowing, dissolving, filtering, defoaming, curing, spinning drawing and after-treatment on a pulp raw material, and has an index system that the dry fracture strength is more than or equal to 3.20cN / dtex, the wet fracture strength is more than or equal to 1.70cN / dtex, the strength needed for generating 5% of the elongation in a wet state is more than or equal to 0.6cN / dtex, the dry elongation at break is 13.0-16%, and the wet elongation at break is 16.0-21.0%. The semi-dull high-strength viscose fiber provided by the invention is prepared by virtue of technical innovation, and is a novel fiber variety which has an index system different from that of ordinary viscose fibers and Modal fibers, and a product of the fiber shows high and strong fiber characteristics and also shows skin affinity stronger than that of cotton fibers, so that the semi-dull high-strength low-elongation viscose fiber can effectively replace the existing differentiation viscose fiber, the development and the industrial upgrading of downstream novel textiles can be promoted while the processability of the downstream process of the viscose fiber is improved, and the semi-dull high-strength low-elongation viscose fiber can be well applied to the field of producing underclothes and high-grade woven fabrics.
Owner:YIBIN GRACE GROUP CO LTD +2

Heat-proof PPS (polyphenylene sulfide) filament adopting copper-loaded bergmeal as filling material and preparation and application of heat-proof PPS filament

The invention relates to a heat-proof PPS (polyphenylene sulfide) filament adopting copper-loaded bergmeal as a filling material and the preparation and the application of the heat-proof PPS filament. In the heat-proof PPS filament, the mass content of the copper-loaded bergmeal composite filling material is 5 to 30 percent. A preparation method of the heat-proof PPS filament comprises the following steps: (1) mixing bergmeal with deionized water to preparing a turbid liquid, adding reductant, copper ion contained lyotrope and copper protecting agent, performing reaction, and then performing ball-milling to obtain the micro-nano powdered copper-loaded bergmeal filling material; (2) premixing the micro-nano powdered copper-loaded bergmeal filling material with PPS chips through kneading to obtain premix, then extruding out the premix, and finally palletizing to obtain heat-proof PPS master batches; and (3) drying and crystallizing the heat-proof PPS master batches, performing melt spinning for forming, cooling, applying oil, performing preliminary reeling, and then drawing for shaping to obtain the heat-proof PPS filament. The PPS filament provided by the invention has the advantages of favorable spinnability, excellent heat resistance and wide application prospect.
Owner:DONGHUA UNIV

Semi-dull low-extensibility viscose fiber as well as preparation method and application thereof

The invention provides a semi-dull low-elongation viscose fiber as well as a preparation method and application thereof. The viscose fiber is obtained by sequentially performing soaking, grinding, squeezing crushing, kneading, directional polymerization reduction, yellowing, dissolving, filtering, defoaming, curing, spinning drawing and after-treatment on a pulp raw material, and has an index system that the dry fracture strength is more than or equal to 3.10cN/dtex, the wet fracture strength is more than or equal to 1.60cN/dtex, the strength needed for generating 5% of the elongation in a wet state is more than or equal to 0.55cN/dtex, the dry elongation at break is 12-14.5%, and the wet fracture extensibility is 16.0-21.0%. The semi-dull high-strength viscose fiber provided by the invention is prepared by virtue of technical innovation, is a novel fiber variety which has an index system different from that of ordinary viscose fibers and Modal fibers, shows high and strong fiber characteristics, and also shows skin affinity stronger than that of cotton fibers, so that the viscose fiber can effectively replace the existing differentiation viscose fiber, the development and the industrial upgrading of downstream novel textiles can be promoted while the processability of the downstream process of the viscose fiber is improved, and the semi-dull low-elongation viscose fiber can be well applied to the field of production of jean fabrics.
Owner:YIBIN GRACE GROUP CO LTD +2

Semi-dull high-intensity low-elongation viscose fiber and preparing method thereof

The invention provides semi-dull high-intensity low-elongation viscose fiber and a preparing method of the semi-dull high-intensity low-elongation viscose fiber. The viscose fiber is obtained through sequentially carrying out soaking, grinding, pressing and crushing, kneading, polymerization reduction, yellowing, dissolution, filtering, defoaming, aging, spinning traction and post treatment on pulp raw materials. The viscose fiber has the following indexes that the fiber number is 1.11 to 1.67 dtex, the dry fracture intensity is greater than or equal to 3.10cN / dtex, the wet fracture intensity is higher than or equal to 1.60cN / dtex, the intensity required for generating the 5-percent elongation rate in the wet state is higher than or equal to 0.55N / dtex, and the dry fracture elongation rate is 11.0 to 19.0 percent. The high-intensity low-elongation viscose fiber related by the invention is a novel fiber variety realized through technical innovation, an index system is different from that of ordinary viscose fiber and modal fiber; a product shows the high-intensity and low-elongation fiber features of the modal fiber, and also shows the higher skin affinity than cotton fiber; the existing differentiated viscose fiber can be effectively replaced; the downstream work procedure processing performance of the viscose fiber is improved; meanwhile, the development and the industrial updating of downstream novel textiles can also be promoted.
Owner:YIBIN GRACE GROUP CO LTD +2

Ultrafine semi-dull high-strength low-elongation viscose fiber and preparation method thereof

The invention provides an ultrafine semi-dull high-strength low-elongation viscose fiber and a preparation method thereof. The viscose fiber is obtained by sequentially performing soaking, grinding, squeezing crushing, kneading, polymerization reduction, yellowing, dissolving, filtering, defoaming, curing, spinning drawing and after-treatment on a pulp raw material, and has the following indexes that the fineness is 0.8-1.11dtex, the dry fracture strength is more than or equal to 3.10cN / dtex, the wet fracture strength is more than or equal to 1.60cN / dtex, the strength needed for generating 5% of the elongation in a wet state is more than or equal to 0.55cN / dtex, and the dry elongation at break is 11.0-19.0%. The ultrafine high-strength low-elongation viscose fiber is a novel fiber variety realized by virtue of technical innovation, and has an index system which is different from that of ordinary viscose fibers and Modal fibers, and a product of the fiber shows the fiber characteristics of high strength and low elongation of the Modal fibers and also shows skin affinity stronger than that of cotton fibers, so that the ultrafine semi-dull high-strength low-elongation viscose fiber can effectively replace the existing differentiation viscose fiber, and while the processability of the downstream process of the viscose fiber is improved, the development and the industrial upgrading of downstream novel textiles are promoted.
Owner:YIBIN GRACE GROUP CO LTD +2

A semi-dull high-strength low-elongation viscose fiber and its preparation method

The invention provides a semi-dull, high-strength, low-elongation viscose fiber and a preparation method thereof. The viscose fiber is prepared by impregnating pulp raw materials, grinding, crushing, kneading, depolymerizing, yellowing, dissolving, and filtering in sequence. , defoaming, ripening, spinning and drawing and post-treatment, the viscose fiber has the following indicators: dry breaking strength ≥ 3.10 cN / dtex, wet breaking strength ≥ 1.60 cN / dtex, 5% elongation in wet state The strength required for elongation is ≥0.55cN / dtex, and the dry elongation at break is 11.0-19.0%. The high-strength and low-elongation viscose fiber involved in the present invention is a new type of fiber achieved through technological innovation. It has an index system different from ordinary viscose fiber and modal fiber, and its products not only show the high-strength, low-elongation fiber characteristics of modal fiber , it also shows stronger skin-friendly properties than cotton fibers, which can effectively replace the existing differentiated viscose fibers. While improving the processing performance of viscose fibers in downstream processes, it can also promote the development and industrialization of downstream new textiles upgrade.
Owner:YIBIN GRACE GROUP CO LTD +2
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