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35results about How to "Low total acid" patented technology

Preparation method of hydrotreating catalyst

The invention discloses a preparation method of a hydrotreating catalyst. The method consists of: first pulping aluminum hydroxide or alumina into a slurry, adding concentrated phosphoric acid to react so as to obtain a sol; then taking the sol as a binder, kneading the sol with large hole alumina and small hole alumina, and conducting shaping, drying and roasting to obtain an alumina carrier; and then steeping the alumina carrier with an active metal component steeping solution, and carrying out drying and roasting so as to obtain the hydrotreating catalyst. In the invention, phosphorus is introduced into the alumina carrier in the form of a binder, and can play a structural assistant role to improve the active metal dispersity on the alumina carrier. The weak acid amount of the carrier is increased, the amount of strong-medium acid is decreased, and the total acid amount is reduced. Particularly, the corrosive effect of the phosphorus-containing binder on an alumina carrier frame is greatly mitigated, the pore structure and mechanical strength of the alumina carrier and the catalyst can be significantly improved, meanwhile, consumption of the phosphorus-containing sol binder is low, and the preparation process is environment-friendly and pollution-free.
Owner:CHINA PETROLEUM & CHEM CORP +1

Mechanical production method of Fangxian rice wine

InactiveCN107794180AGrowth inhibitionGuaranteed High Sugar FlavorAlcoholic beverage preparationYeastVinasse
The invention discloses a mechanical production method of Fangxian rice wine. The method includes (1), steaming sticky rice after soaking, cooling the sticky rice through spreading, adding Chinese yeast and water, performing squeezing after nest saccharification and fermentation to obtain first wind liquid and first vinasse, and adding water into the first vinasse to continue fermentation; (2), steaming the sticky rice after soaking, cooling the sticky rice through water pouring, adding the Chinese yeast for saccharification, adding the first wine liquid for fermentation, performing squeezingto obtain second wine liquid and second vinasse, and adding the second vinasse into vinasse fermentation liquid in the step (1) to continue fermentation; (3), steaming the sticky rice after soaking, cooling the sticky rice through water pouring, adding the Chinese yeast for saccharification, and adding the second wine liquid for fermentation; (4), after fermentation, performing squeezing to obtainthird wine liquid and third vinasse, performing clarification and sterilization on the third wine liquid to obtain finished sweet Fangxian rice wine, adding the third vinasse into the vinasse fermentation liquid in the step (2) to continue fermentation, and performing squeezing, clarification and sterilization after fermentation to obtain the finished semi-dry Fangxian rice wine. By the mechanical production method, the problems of ropiness of fermented mash and acid vinosity of conventional Fangxian rice wine are solved.
Owner:HUBEI UNIV OF TECH +1

Phosphorus-containing and supported-metal-containing MFI molecular sieve and preparation method thereof

The invention discloses a phosphorus-containing and supported-metal-containing MFI molecular sieve and a preparation method thereof, wherein the n(SiO2) / n(Al2O3) of the molecular sieve is greater than100, the phosphorus content of the molecular sieve is 0.1-5 wt%, the supported metal content of the molecular sieve is 0.1-5 wt%, the Al distribution parameter D (Al) of the molecular sieve is more than or equal to 0.6 and is less than or equal to 0.85, the volume of the mesopores of the molecular sieve accounts for 40-80% of the total pore volume, the volume of the mesopores with the pore size of 2-20 nm accounts for more than 90% of the total mesopore volume, the amount of the strong acid of the molecular sieve accounts for 60-80% of the total acid amount, and a ratio of the acid B to the acid L is 15-80. According to the present invention, with the catalyst or the auxiliary agent prepared by using the phosphorus-containing and supported-metal-containing MFI structure molecular sieve asthe active component, the yield of gasoline in the catalytic cracking reaction of petroleum hydrocarbons can be maintained while the octane number of gasoline can be effectively increased, or the octane value of gasoline can be maintained while the yield of gasoline is improved.
Owner:CHINA PETROLEUM & CHEM CORP +1

Traditional Chinese drug component composition for treating stomach ulcer and duodenal ulcer, and preparation thereof

The invention discloses a traditional Chinese drug component composition for treating stomach ulcer and duodenal ulcer, wherein the composition is prepared from berberine hydrochloride, curcumin and common bletilla tuber polysaccharide according to a certain weight part ratio, and is prepared into an oral administration formation such as powder, granule, tablet, capsule, pill, oral liquid, syrup, emulsion, suspension, and the like. According to the present invention, 1) significant bactericidal killing and bacterial inhibiting effects on helicobacter pylori are provided; 2) effects of inhibition of H<+>/K<+>-ATP enzyme activity, reduction of gastric juice amount, reduction of gastric free acid, reduction of the total acid discharge, reduction of pepsin discharge, analgesic, and anti-inflammation are provided; and 3) functions of promotion of wound surface tissue cell proliferation, promotion of healing quality and speed of gastrointestinal mucous membrane tissue, and improvement of barrier function of gastrointestinal mucous membrane are provided. Animal experiment results show that the traditional Chinese drug component composition has pharmacologic actions of significant reduction of ulcer indexes of a hydrochloric acid/ethanol type animal stomach ulcer model, a cold water stress type animal stomach ulcer model, a pylorus ligation type animal stomach ulcer model, and other animal stomach ulcer models, inhibition and killing of helicobacter pylori, inhibition of gastric juice secretion, and the like, and can be used as a drug for treating stomach ulcer and duodenal ulcer.
Owner:JIANGXI UNIVERSITY OF TRADITIONAL CHINESE MEDICINE

Method for improving quality of fruit juice or fruit wine

The invention discloses a method for improving quality of fruit juice or fruit wine. The method comprises the following steps of performing bitterness removal treatment, brown stain removal treatmentand acid reduction treatment on fruit juice and fruit wine through resins so as to obtain fruit juice or fruit wine after bitterness removal, brown strain removal and acid reduction; enabling bitter substances, brown stain substances, organic acid, all or part of aroma components and fragrance precursor substances namely glucoside to be adsorbed to used resins; performing regeneration on the usedresins under mild conditions, and enabling the resins to be repeatedly used for the bitterness removal treatment, the brown stain removal treatment and the acid reduction treatment on the fruit juiceand the fruit wine; enabling regeneration fluid obtained through the regeneration process to be subjected to pH adjustment, adding an appropriate quantity of glycosidase, and performing hydrolysis for1-5h so as to obtain hydrolysis liquid containing components of aroma components and the like; enabling the hydrolysis liquid to be subjected to pH adjustment and low temperature distillation to obtain fragrance liquid; adding the fragrance liquid to the fruit juice or the fruit wine after bitterness removal, brown strain removal and acid reduction, and then mixing the fruit juice or the fruit wine to which the fragrance liquid is added, with untreated fruit juice or fruit wine so as to obtain the fruit juice or the fruit wine which is rich and full in fragrance, not bitter, free from brown stain and low in total acid content.
Owner:YANTAI UNIV

Brewing process of tea wine having functions of invigorating stomach and intestine and nourishing Yin and Yang

The invention discloses a brewing process of tea wine having functions of invigorating stomach and intestine and nourishing Yin and Yang. The brewing process comprises the following steps: (1) primaryfermentation: mixing wolfberry fruit, fructus ziziphi jujubae, okra, water and saccharomycetes, fermenting in an environment of 25 to 28 DEG C for 6 to 8 days, mixing finished product tea, water andthe saccharomycetes, and fermenting in an environment of 25 to 30 DEG C for 6 to 10 days; (2) secondary fermentation: mixing two materials obtained by fermentation in the step (1) to form a mixed material, adding the saccharomycetes, stirring uniformly, and fermenting in an environment of 22 to 30 DEG C for 15 to 30 days, wherein the ratio of the mixed material to the saccharomycetes is 100 to 1.5. The primary fermentation and the secondary fermentation are performed according to the formula of the invention, so that the total acid content and total sugar content of the brewed tea wine are lowered effectively, and the natural tea polyphenol content is greatly increased; moreover, a proper amount of wolfberry fruit, fructus ziziphi jujubae and okra are added, so that the tea wine has the effects of nourishing liver, nourishing kidney, moistening lung, tonifying middle-Jiao and Qi, nourishing the blood and tranquilizing, moderating the property of medicine, invigorating stomach and intestine and nourishing Yin and Yang, and the product has a higher nutritional value.
Owner:鹰潭正道生物科技有限公司

Method for preparing multi-stage pore Y molecular sieve through H4EDTA-NaOH co-treatment

InactiveCN110065952AIncreased mesopore specific surface areaReduce crystallinityFaujasite aluminosilicate zeoliteMolecular sievePore diameter
The invention discloses a method for preparing a multi-stage pore Y molecular sieve through H4EDTA-NaOH co-treatment, which comprises the following steps: (1) acid treatment of H4EDTA solution, namelyadding a NaY molecular sieve into H4EDTA aqueous solution to obtain an acid treatment sample; (2) NaOH solution alkali treatment: mixing the NaOH solution with the acid treatment sample in step (1) to obtain an alkali treatment sample; (3) Na2H2EDTA solution acid treatment: adding the Na2H2EDTA solution into the alkali treatment sample. The mesoporous specific surface area of the NaY molecular sieve can be increased by 200%, and the mesoporous pore volume can be increased by 849%. Meanwhile, the specific surface area of the micropores is reduced by only 36%, the volume of the micropores is reduced by only 5%, and the average pore diameter of the molecular sieve is 10.1 nm. The NaY molecular sieve has the advantages of the best pore system for the step distribution of mesopores-micropores.Meanwhile, the crystallinity of the molecular sieve modified by acid and alkali is reduced, and the total acid content is slightly reduced. Comparing the acid distribution of the molecular sieves before and after the modification, the acid content of the modified sample B is increased, and the L acid content is decreased.
Owner:GUANGDONG UNIV OF PETROCHEMICAL TECH

Brewing process of tea wine with various health care functions

The invention discloses a brewing process of tea wine with various health care functions. The brewing process comprises the following steps: (1) brewing wolfberry fruit, fructus ziziphi jujubae, Maca,herba dendrodii officinalis, veratryl alcohol, okra, herba cistanche, honeysuckle flower, oyster, cordyceps militaris, semen allii tuberosi, raspberry fruit, folium phyllostachys, semen plantaginis and 52-degree finished product tea wine raw stock together for 40 to 50 days; (2) filtering: precisely filtering the materials brewed in the step (1); (3) adjusting: adjusting the degree and mouthfeelof filtrate obtained in the step (2) to obtain desired tea wine; (4) assembling: bottling and packaging the desired tea wine. The total acid content and total sugar content of the tea wine made by theprocess are lowered effectively, and the natural tea polyphenol content is greatly increased; moreover, the tea wine has various health care functions of nourishing liver, nourishing kidney, tonifying middle-Jiao and Qi, nourishing the blood and tranquilizing, moderating the property of medicine, nourishing and strengthening body, promoting the secretion of saliva or body fluid, invigorating stomach, nourishing yin, clearing heat, moistening lung, nourishing kidney, improving eyesight, strengthening waist, invigorating stomach and intestine and nourishing Yin and Yang, and has a higher nutritional value.
Owner:鹰潭正道生物科技有限公司

Phosphorus and loading metal containing MFI structure molecular sieve and preparation method thereof

The invention discloses a phosphorus and loading metal containing MFI structure molecular sieve. According to the phosphorus and loading metal containing MFI structure molecular sieve, n(SiO2)/n(Al2O3) is larger than 100; with P2O5 for calculation and the dry basis weight of the molecular sieve being a reference, the phosphorus content of the molecular sieve is 0.1-5wt%; with loading metal oxides for calculation and the dry basis weight of the molecular sieve being a reference, the loading metal content of the molecular sieve is 0.5-5wt%; the Al distribution parameter D of the molecular sieve meets the equation of 0.5<=D<=0.8; the proportion of the medium pore volume to the total pore volume of the molecular sieve is 15-30vt%; the proportion of the strong acid amount to the total acid amount of the molecular sieve is 60-80%, and the ratio of the amount of acid B to the amount of acid L is 20-100. The phosphorus and loading metal containing MFI structure molecular sieve serves as an active component for preparing catalysts or auxiliaries, and in a petroleum hydrocarbon catalytic cracking reaction, the gasoline octane value can be effectively increased while the gasoline yield is kept, or the gasoline yield is increased while the gasoline octane value is kept.
Owner:CHINA PETROLEUM & CHEM CORP +1

Brewing process for tea wine with nourishing and body building functions

InactiveCN107699424AIncreased content of natural tea polyphenolsPalliative propertiesNervous disorderDigestive systemChemistryDiuresis
The invention discloses a brewing process for a tea wine with nourishing and body building functions. The brewing process comprises the following steps: (1) primary fermentation: mixing fructus lycii,red dates, maca, folium phyllostachys, water and saccharomycetes, performing fermentation for 10-18 days in the environment with the temperature of 25-30 DEG C, mixing an end product (tea), water andsaccharomycetes, and performing fermentation for 6-10 days in the environment with the temperature of 25-30 DEG C; (2) secondary fermentation: mixing two materials obtained through fermentation in the step (1) to form a mixed material, adding saccharomycetes, and performing uniform mixing and fermentation; (3) primary distillation; (4) secondary distillation; and (5) placing in a tank for aging,and at last, performing blending and filling. As primary fermentation and secondary fermentation are performed after the formula is adopted, the total content of acids and sugars in the tea wine obtained through brewing is effectively reduced; the content of natural tea polyphenol is greatly increased; and as fructus lycii, red dates, maca and folium phyllostachys are appropriately added, the teawine has the effects of nourishing the liver and the kidney, moistening the lung, tonifying middle-Jiao and Qi, nourishing blood for tranquillization, moderating the nature of drugs, nourishing for body building, clearing heat and relieving restlessness, promoting secretion of saliva or body fluid, inducing diuresis and the like.
Owner:鹰潭正道生物科技有限公司

A kind of MFI structure molecular sieve containing phosphorus and loaded metal and preparation method thereof

The invention discloses a phosphorus-containing and supported-metal-containing MFI structure molecular sieve and a preparation method thereof, wherein the n(SiO2) / n(Al2O3) of the molecular sieve is greater than 100, the phosphorus content of the molecular sieve is 0.1-5 wt%, the supported metal content of the molecular sieve is 0.5-5 wt%, the Al distribution parameter D (Al) of the molecular sieveis more than or equal to 0.6 and is less than or equal to 0.85, the volume of the mesopores of the molecular sieve accounts for 40-80% of the total pore volume, the volume of the mesopores with the pore size of 2-20 nm accounts for more than 90% of the total mesopore volume, the amount of the strong acid of the molecular sieve accounts for 60-80% of the total acid amount, and a ratio of the acidB to the acid L is 15-80. According to the present invention, with the catalyst or the auxiliary agent prepared by using the phosphorus-containing and supported-metal-containing MFI structure molecular sieve as the active component, the yield and the octane number of gasoline can be improved in the catalytic cracking reaction of petroleum hydrocarbons while the olefin content in gasoline can be effectively reduced.
Owner:CHINA PETROLEUM & CHEM CORP +1

A kind of MFI structure molecular sieve containing phosphorus and loaded metal and preparation method thereof

The invention discloses a phosphorus-containing and supported-metal-containing MFI structure molecular sieve and a preparation method thereof, wherein the n(SiO2) / n(Al2O3) of the molecular sieve is greater than 100, the phosphorus content of the molecular sieve is 0.1-5 wt%, the supported metal content of the molecular sieve is 0.5-5 wt%, the Al distribution parameter D (Al) of the molecular sieveis more than or equal to 0.5 and is less than or equal to 0.8, the supported metal distribution parameter D (M) of the molecular sieve is more than or equal to 2 and is less than or equal to 10, thevolume of the mesopores of the molecular sieve accounts for 15-30% of the total pore volume, the amount of the strong acid of the molecular sieve accounts for 60-80% of the total acid amount, and a ratio of the acid B to the acid L is 20-100. According to the present invention, with the catalyst or the auxiliary agent prepared by using the phosphorus-containing and supported-metal-containing MFI structure molecular sieve as the active component, the yield and the octane number of gasoline can be improved in the catalytic cracking reaction of petroleum hydrocarbons while the olefin content in gasoline can be effectively reduced.
Owner:CHINA PETROLEUM & CHEM CORP +1

A kind of MFI structure molecular sieve containing phosphorus and loaded metal and preparation method thereof

The invention discloses a phosphorus-containing and supported-metal-containing MFI molecular sieve and a preparation method thereof, wherein the n(SiO2) / n(Al2O3) of the molecular sieve is greater than100, the phosphorus content of the molecular sieve is 0.1-5 wt%, the supported metal content of the molecular sieve is 0.1-5 wt%, the Al distribution parameter D (Al) of the molecular sieve is more than or equal to 0.6 and is less than or equal to 0.85, the volume of the mesopores of the molecular sieve accounts for 40-80% of the total pore volume, the volume of the mesopores with the pore size of 2-20 nm accounts for more than 90% of the total mesopore volume, the amount of the strong acid of the molecular sieve accounts for 60-80% of the total acid amount, and a ratio of the acid B to the acid L is 15-80. According to the present invention, with the catalyst or the auxiliary agent prepared by using the phosphorus-containing and supported-metal-containing MFI structure molecular sieve asthe active component, the yield of gasoline in the catalytic cracking reaction of petroleum hydrocarbons can be maintained while the octane number of gasoline can be effectively increased, or the octane value of gasoline can be maintained while the yield of gasoline is improved.
Owner:CHINA PETROLEUM & CHEM CORP +1

A kind of phosphorus-containing MFI structure molecular sieve and preparation method thereof

The present disclosure provides a phosphorus-containing MFI-structure molecular sieve and a preparation method thereof, wherein the n(SiO2) / n(Al2O3) of the molecular sieve is more than 100, the phosphorus content (calculated as P2O5) of the molecular sieve is 0.1-5 wt% by using the dry base weight of the molecular sieve as the reference, the Al distribution parameter D of the molecular sieve is more than or equal to 0.6 and is less than or equal to 0.85, the volume of the mesopores of the molecular sieve accounts for 40-80% of the total pore volume, the volume of the mesopores with the pore size of 2-20 nm accounts for more than 90% of the total mesopore volume, the amount of the strong acid of the molecular sieve accounts for 60-80% of the total acid amount, and a ratio of the acid B to the acid L is 15-80. According to the present invention, with the catalyst or the auxiliary agent prepared by using the phosphorus-containing MFI-structure molecular sieve as the active component, theyield of gasoline in the catalytic cracking reaction of petroleum hydrocarbons can be maintained while the octane number of gasoline can be effectively increased, or the octane value of gasoline can be maintained while the yield of gasoline is improved.
Owner:CHINA PETROLEUM & CHEM CORP +1
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