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32results about How to "Preserve intrinsic properties" patented technology

Mechanical stripping method of functionalized boron nitride nanosheet

ActiveCN111717900ADiffraction peak intensity of apparent crystal planeEfficient strippingNitrogen compoundsNanotechnologyLiquid productHexagonal boron nitride
The invention relates to a mechanical stripping method of a functionalized boron nitride nanosheet. The method adopts boric acid and commercial bulk hexagonal boron nitride as raw materials, and comprises the following three steps: uniformly mixing boric acid and commercial hexagonal boron nitride in a mortar, and carrying out high-temperature pretreatment to make the commercial bulk hexagonal boron nitride eroded by dehydrated boric acid and fixed by boron oxide in order to obtain a uniformly reacted solid mixture; roughly grinding the solid mixture obtained after the reaction, putting the ground solid mixture into a ball milling tank, and carrying out mechanical ball milling treatment; and dissolving and dispersing white powder obtained after ball milling into deionized water, and carrying out repeated washing multiple times to ensure that free boric acid is completely washed away so as to obtain a functionalized boron nitride nanosheet dispersion liquid product; or drying a productobtained by centrifugal washing to obtain a functionalized boron nitride nanosheet powder product. The method is simple to operate, harsh experimental conditions are not needed, boric acid and deionized water can be recycled, and the obtained products are high in crystallinity and functionalization degree.
Owner:HEBEI UNIV OF TECH

Old style forming method of Jinshan stone with decoration effect

ActiveCN103387415ASimple and elegant decorative effectUnique and ingenious ideaEmulsionEthyl acetate
The invention relates to an old style forming method of Jinshan stone with a decoration effect, and relates to the technical field of building materials. According to the invention, a key technology of accelerating color penetration and strengthening color attachment is adopted, specifically, the method comprises the following steps of: brewing 100g of tea leaves by using 1L of boiled water, cooling to the room temperature, filtering by using gauze to obtain tea water for spare use; placing 5g of potassium permanganate in 25L of tap water, and uniformly stirring, thus obtaining a solution for accelerating color permeation for spare use; adding 250ML of poly ethyl acetate emulsion adhesive into the solution for accelerating color permeation, and uniformly stirring, thus obtaining a solution for accelerating color permeation and strengthening color attachment for spare use; adding the tea water into the solution for accelerating color permeation and strengthening color attachment, uniformly stirring, and placing for one hour, thus obtaining the old style forming liquid for spare use; painting the old style forming liquid on the surface of Jinshan stone by using a soft fur brush, cooling, and preparing an old-style Jinshan stone product. The Jinshan stone old style forming method is used for old forming decoration treatment on Jinshan stone, is simple, ingenious and practical, ensures that the product is plain and elegant, and ensures that the decoration effect is good.
Owner:GAUNGLIN SUZHOU CO LTD

Limonite purple-clay product and preparation method thereof

The invention discloses a limonite purple-clay product, which consists of the following raw materials in percentage by weight: 30 to 50 percent of limonite, and 50 to 70 percent of purple-clay mud. The preparation method comprises the following steps: grinding the limonite and the purple clay mud into powder of between 80 and 120 meshes; mixing according to a proportion, adding water and stirringto prepare unfired pottery; sealing and packaging the unfired pottery, and aging for 10 to 15 days; preparing a blank of the required product, and drying in the shade indoors for 2 to 3 days; grinding and polishing the shady dried blank to prepare a semi-finished product; and firing the prepared semi-finished product in a kiln for 15 to 20 hours at the temperature of between 1,120 and 1,180 DEG C, and cooling to prepare the required product. In the invention, the limonite resource is sufficiently utilized, and waste is turned into wealth; and the fired limonite purple-clay product has light weight, high strength and no toxicity or radiation, the original characteristic and separated trace elements of the limonite have no changes, and the advantages of good ventilation and plasticity of the purple-clay are combined. The limonite purple-clay product can be manufactured into various nice new material tea sets, mugs and other products.
Owner:北方红杉生态科技有限公司

Preparation method of graphene/styrene-butadiene rubber composite with functional characteristic

The invention relates to a preparation method of a graphene/styrene-butadiene rubber composite with a functional characteristic and aims at compounding directionally-arranged graphene nanosheets intostyrene-butadiene rubber so as to provide excellent conductivity, wear resistance and the like. The material provided by the invention is of a double-layer structure, one layer is a functional layer mainly formed by directional arrangement of the graphene nanosheets, and the other layer is an elastic insulation layer mainly made of the styrene-butadiene rubber. The preparation method comprises thesteps: (1) carrying out ultrasonic treatment on the graphene nanosheets in a polyvinylpyrrolidone (PVP) solution to obtain a graphene dispersion solution; (2) adding the graphene dispersion solutioninto styrene-butadiene latex to carry out ultrasonic treatment or mechanical stirring; and (3) pouring the mixed solution obtained in the step (2) into a die, and carrying out solidification at a certain temperature to obtain a final composite. The composite is low in graphene nanosheet addition amount, excellent in conductivity and wear resistance in a direction parallel to the directional arrangement direction of the graphene nanosheets, good in insulation property in a direction vertical to the arrangement direction of the graphene nanosheets, soft and foldable and can be used in the fieldsuch as electrostatic protection and electromagnetic wave shielding.
Owner:SICHUAN UNIV

Coating of polysilicon reduction furnace, preparation method of coating, polysilicon reduction furnace and uses of polysilicon reduction furnace

The invention provides a coating of a polysilicon reduction furnace, a preparation method of the coating, the polysilicon reduction furnace and uses of the polysilicon reduction furnace, and relates to the field of polysilicon technical equipment in production. The preparation method of the coating of the polysilicon reduction furnace comprises the steps of spraying first particles on the surface,in contact with materials, of the polysilicon reduction furnace by virtue of first cold gas dynamic spraying to form a base layer, and spraying second particles on the surface, away from the polysilicon reduction furnace, of the base layer by virtue of second cold gas dynamic spraying to form a surface layer. The speed of the first particles of the first cold gas dynamic spraying and the speed ofthe second particles of the second cold gas dynamic spraying are both supersonic speed, and the speed of the first particles is greater than the speed of the second particles. The base layer and thesurface layer are suitable for reflecting infrared radiation. The spraying speed of the first particles forming the base layer is higher, so that the bonding strength of the base layer and the surfaceof the polysilicon reduction furnace is higher. The spraying speed of the second particles forming the surface layer is lower so as to facilitate the reduction of the spraying cost of the coating.
Owner:ASIA SILICON QINGHAI +1

Activation method of high-capacity lithium ion battery negative electrode material

The invention provides an activation method of a high-capacity lithium ion battery negative electrode material. The activation method comprises the following steps of 1) performing film formation on agraphene oxide aqueous solution in a porous template by a drop-coating method, and allowing to stand; 2) spraying the graphene oxide aqueous solution onto the dried three-dimensional graphene oxide / template attachment material, and drying for use; 3) impregnating the material in an aqueous solution dissolved with an activation agent, and allowing to stand after ultrasonic processing; and 4) placing the product in a tubular furnace for oxygen-free sintering after drying, cooling the sintered product to a room temperature, washing the product with deionized water until washing water is neutral,and drying, thereby obtaining the activated graphene / template negative electrode material. By the activation method, the inherent characteristic of a two-dimensional graphene sheet is maintained, meanwhile, graphene and the porous template are more uniformly distributed, the active sites of graphene phase-template phase-electrolyte phase catalytic reaction are remarkably improved, and the power density and the cycle rate performance are remarkably improved.
Owner:HEFEI GUOXUAN HIGH TECH POWER ENERGY CO LTD CO LTD

Reduction furnace bell jar inner wall spraying device and spraying method and reduction furnace

The invention provides a reduction furnace bell jar inner wall spraying device and spraying method and a reduction furnace, and relates to the technical field of polycrystalline silicon equipment. Thespraying device comprises a bell jar, a rotating part, a sealing part, a vacuumizing part, an exhaust part and a cold gas power spraying part; and after a closed space is formed in the bell jar through a sealing part, the interior of the bell jar is in a high-temperature protective gas atmosphere through the vacuumizing part, the cold gas power spraying part and the exhaust part, then the cold gas power spraying part is adopted to spray powder to the inner wall of the bell jar to form a coating on the inner wall of the bell jar, the interior of the bell jar is in the high-temperature protective gas atmosphere before spraying, oxidation of the coating in the spraying process can be avoided, and the intrinsic performance of a coating material can be reserved to the maximum extent; and meanwhile, the inner wall of the bell jar is preheated by using high-temperature protective gas, so that the coating with high bonding strength is obtained under a relatively low spraying condition. The invention further provides the reduction furnace bell jar inner wall spraying method.
Owner:ASIA SILICON QINGHAI +1

Limonite purple-clay product and preparation method thereof

The invention discloses a limonite purple-clay product, which consists of the following raw materials in percentage by weight: 30 to 50 percent of limonite, and 50 to 70 percent of purple-clay mud. The preparation method comprises the following steps: grinding the limonite and the purple clay mud into powder of between 80 and 120 meshes; mixing according to a proportion, adding water and stirringto prepare unfired pottery; sealing and packaging the unfired pottery, and aging for 10 to 15 days; preparing a blank of the required product, and drying in the shade indoors for 2 to 3 days; grinding and polishing the shady dried blank to prepare a semi-finished product; and firing the prepared semi-finished product in a kiln for 15 to 20 hours at the temperature of between 1,120 and 1,180 DEG C, and cooling to prepare the required product. In the invention, the limonite resource is sufficiently utilized, and waste is turned into wealth; and the fired limonite purple-clay product has light weight, high strength and no toxicity or radiation, the original characteristic and separated trace elements of the limonite have no changes, and the advantages of good ventilation and plasticity of the purple-clay are combined. The limonite purple-clay product can be manufactured into various nice new material tea sets, mugs and other products.
Owner:北方红杉生态科技有限公司

A kind of activation method of high-capacity lithium-ion battery negative electrode material

The invention provides an activation method of a high-capacity lithium ion battery negative electrode material. The activation method comprises the following steps of 1) performing film formation on agraphene oxide aqueous solution in a porous template by a drop-coating method, and allowing to stand; 2) spraying the graphene oxide aqueous solution onto the dried three-dimensional graphene oxide / template attachment material, and drying for use; 3) impregnating the material in an aqueous solution dissolved with an activation agent, and allowing to stand after ultrasonic processing; and 4) placing the product in a tubular furnace for oxygen-free sintering after drying, cooling the sintered product to a room temperature, washing the product with deionized water until washing water is neutral,and drying, thereby obtaining the activated graphene / template negative electrode material. By the activation method, the inherent characteristic of a two-dimensional graphene sheet is maintained, meanwhile, graphene and the porous template are more uniformly distributed, the active sites of graphene phase-template phase-electrolyte phase catalytic reaction are remarkably improved, and the power density and the cycle rate performance are remarkably improved.
Owner:HEFEI GUOXUAN HIGH TECH POWER ENERGY CO LTD CO LTD

Old style forming method of Jinshan stone with decoration effect

The invention relates to an old style forming method of Jinshan stone with a decoration effect, and relates to the technical field of building materials. According to the invention, a key technology of accelerating color penetration and strengthening color attachment is adopted, specifically, the method comprises the following steps of: brewing 100g of tea leaves by using 1L of boiled water, cooling to the room temperature, filtering by using gauze to obtain tea water for spare use; placing 5g of potassium permanganate in 25L of tap water, and uniformly stirring, thus obtaining a solution for accelerating color permeation for spare use; adding 250ML of poly ethyl acetate emulsion adhesive into the solution for accelerating color permeation, and uniformly stirring, thus obtaining a solution for accelerating color permeation and strengthening color attachment for spare use; adding the tea water into the solution for accelerating color permeation and strengthening color attachment, uniformly stirring, and placing for one hour, thus obtaining the old style forming liquid for spare use; painting the old style forming liquid on the surface of Jinshan stone by using a soft fur brush, cooling, and preparing an old-style Jinshan stone product. The Jinshan stone old style forming method is used for old forming decoration treatment on Jinshan stone, is simple, ingenious and practical, ensures that the product is plain and elegant, and ensures that the decoration effect is good.
Owner:GAUNGLIN SUZHOU CO LTD

A method for preparing vertical arrays of carbon nanotubes covered with flexible thin layers of carbon

The invention specifically relates to a preparation method for a flexible vertically-aligned carbon nanotube array covered with thin-layer carbon, belonging to the field of preparation of flexible vertically-aligned carbon nanotube arrays. The preparation method comprises the following steps: depositing a thin layer of carbon on the surface of a substrate through plasma deposition; then growing carbon nanotubes by using a plasma-enhanced chemical vapor deposition method so as to obtain a composite structure of a vertically-aligned carbon nanotube array covered with the thin-layer carbon, wherein the thin-layer carbon located at the top allows the carbon nanotubes in the vertically-aligned array to be interconnected so as to guarantee that all the carbon nanotubes in the array participate in heat transfer; simply pressing the vertically-aligned array and peeling the vertically-aligned array from the substrate so as to obtain the self-supported flexible vertically-aligned carbon nanotubearray. The prepared self-supported flexible vertically-aligned carbon nanotube array has excellent thermal conductivity, good bendability and strong adhesion, and has good application prospects in the fields of flexible thermal interface materials and flexible energy storage materials.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Anti-corrosion flexible epoxy composite coiled material as well as preparation method and application thereof

The invention relates to an anti-corrosion flexible epoxy composite coiled material as well as a preparation method and application thereof, and the flexible epoxy composite coiled material comprises a first resin layer, a first reinforcing layer, a second resin layer, a second reinforcing layer and a third resin layer which are sequentially stacked, the first resin layer, the second resin layer and the third resin layer are respectively compounded by light-cured epoxy acrylic resin and light-cured polyurethane acrylic resin as main raw materials, and the light-cured epoxy acrylic resin is selected from aliphatic flexible long-chain modified epoxy acrylic resin; and the light-cured polyurethane acrylic resin is selected from aliphatic polyurethane acrylic resin with polyfunctionality. The three resin layers not only retain the inherent characteristics of epoxy resin, but also increase the advantages of acrylic resin and polyurethane resin, and meanwhile, the film layer is toughened from the molecular level to form a cross-linked network composite film layer structure reinforced in an elastomer; the composite resin system has weather resistance, flexibility and good mechanical strength at the same time.
Owner:JIANGSU CANLON BUILDING MATERIALS

Lithium-ion battery anode material structure, lithium-ion battery and preparation method thereof

The invention provides a lithium ion battery anode material structure, a lithium ion battery and a preparation method of the lithium ion battery anode material structure. The preparation method comprises the steps of: (1), putting a silicon nano-material, a carbon nano-material and an additive in an organic solvent to prepare dispersion liquid; (2), providing a metal catalytic substrate, and coating the dispersion liquid on the upper surface of the metal catalytic substrate; and (3), forming a graphene film on the upper surface of the structure obtained in the step (2). According to the battery anode material structure provided by the invention, the inherent characteristics of the silicon anode material and graphene are reserved; furthermore, the synergistic effect between the silicon anode material and graphene can be played; simultaneously, effective contact between a silicon nano-material / carbon nano-material composite film and a metal catalytic substrate current collector can be realized; high-efficiency lithium storage capability can be provided; furthermore, great volume change of the silicon nano-material in a charging and discharging process can be relieved; and generation of the internal stress of the anode material can be effectively inhibited and improved, so that pulverization of the anode material can be avoided.
Owner:SHANGHAI PYLON TECH CO LTD

A kind of preparation method of graphene/styrene-butadiene rubber composite material with multifunctional properties

The invention relates to a preparation method of a graphene / styrene-butadiene rubber composite with a functional characteristic and aims at compounding directionally-arranged graphene nanosheets intostyrene-butadiene rubber so as to provide excellent conductivity, wear resistance and the like. The material provided by the invention is of a double-layer structure, one layer is a functional layer mainly formed by directional arrangement of the graphene nanosheets, and the other layer is an elastic insulation layer mainly made of the styrene-butadiene rubber. The preparation method comprises thesteps: (1) carrying out ultrasonic treatment on the graphene nanosheets in a polyvinylpyrrolidone (PVP) solution to obtain a graphene dispersion solution; (2) adding the graphene dispersion solutioninto styrene-butadiene latex to carry out ultrasonic treatment or mechanical stirring; and (3) pouring the mixed solution obtained in the step (2) into a die, and carrying out solidification at a certain temperature to obtain a final composite. The composite is low in graphene nanosheet addition amount, excellent in conductivity and wear resistance in a direction parallel to the directional arrangement direction of the graphene nanosheets, good in insulation property in a direction vertical to the arrangement direction of the graphene nanosheets, soft and foldable and can be used in the fieldsuch as electrostatic protection and electromagnetic wave shielding.
Owner:SICHUAN UNIV

Method for dyeing wool quickly at low temperature

The invention relates to a method for dyeing wool quickly at low temperature. The method comprises the following steps of: preparing a levelling agent, preparing a dye solution and dyeing the wool at the low temperature, wherein 1) the levelling agent is prepared from the following raw materials in part by weight: 15 to 25 parts of sodium acetate, 25 to 35 parts of aromatic polyether sodium benzene sulfonate, 5 to 15 parts of sodium hydrogensulfite, 15 to 25 parts of n-amyl alcohol and 1,000 parts of water, and a method for preparing the levelling agent comprises the following steps of: weighing the sodium acetate in the ratio, adding the sodium acetate into the water, dissolving and stirring uniformly; and regulating the pH value to reach 4.5 by using glacial acetic acid, adding the aromatic polyether sodium benzene sulfonate, the sodium hydrogensulfite and the n-amyl alcohol, and stirring the mixture in a constant temperature oscillator uniformly for 30 minutes for later use; and 2)the dye solution is prepared from the following raw materials in part by weight: 2 to 8 parts of dye, 1 to 5 parts of levelling agent and 1,000 parts of water, and a method for preparing the dye solution comprises the following steps of: adding the dye and the levelling agent into the water in the ratio, stirring uniformly, and regulating the pH value to be between 4.5 and 5 by using glacial acetic acid for later use.
Owner:SHANDONG RUYI WOOLEN GARMENT GRP CO LTD

A mechanical exfoliation method of functionalized boron nitride nanosheets

ActiveCN111717900BDiffraction peak intensity of apparent crystal planeEfficient strippingNitrogen compoundsNanotechnologyHexagonal boron nitridePhysical chemistry
The invention is a mechanical stripping method of functionalized boron nitride nanosheets. The method adopts boric acid and commercial hexagonal boron nitride as raw materials, and synthesizes them through the following three steps: taking boric acid and commercial hexagonal boron nitride in a mortar After uniform mixing, high-temperature pretreatment is carried out, so that the commercial block hexagonal boron nitride is corroded by dehydration boric acid and fixed by boron oxygen, and a uniformly reacted solid mixture is obtained; the solid mixture obtained after the reaction is roughly ground and placed in a ball mill tank In the process, mechanical ball milling is carried out; the white powder obtained after ball milling is dissolved and dispersed in deionized water, and washed repeatedly to ensure that the free boric acid is completely washed away, and the functionalized boron nitride nanosheet dispersion product is obtained; or The product obtained by centrifugal washing is dried to obtain a functionalized boron nitride nanosheet powder product. The method is simple to operate, does not require harsh experimental conditions, boric acid and deionized water can be recycled, and the obtained product has high crystallinity and functionalization degree.
Owner:HEBEI UNIV OF TECH
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