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48results about How to "The principle is scientific and reasonable" patented technology

Graphene-magnesium seawater battery device

ActiveCN106898764ALong-term stable independent power supplyEasy to useCell electrodesImmersion cellsEngineeringOxygen
The invention belongs to the technical field of seawater battery equipment, and in particular relates to a graphene-magnesium seawater battery device. The graphene-magnesium seawater battery device consist of 1 to n groups of graphene-magnesium seawater battery units; the main body structure of each graphene-magnesium seawater battery unit comprises a shell, an upper part water-permeable hole, a bottom water-permeable hole, a convex cone, a magnesium alloy anode polar plate, a negative pole binding post, a graphene composite cathode polar plate, a positive pole binding post, an ion conducting plate grid, an inner seal cover, a binding post through hole, an outer seal cover, a lead hole, a voltage-resistant area, a negative pole output lead and a positive pole output lead; based on the technical principle of a fuel battery, the anode material adopts high-potential and inert AZ31 magnesium alloy, the cathode adopts a graphene composite material with high electrical conductivity and prominent catalytic reduction efficiency on seawater dissolved oxygen, and a seawater solution with dissolved oxygen more than or equal to 5 ppm and sodium chloride more than or equal to 3.5 percent serves as electrolyte; the graphene-magnesium seawater battery device is simple in structure, scientific and reasonable in principle, high in operability, low in cost, friendly in using environment, safe, environmentally friendly, high in popularization value, and easy to popularize and use.
Owner:QINGDAO HUAGAO GRAPHENE CORP LTD

Gas cutting early stage monitoring method

InactiveCN105298472ATroubleshooting Annular Fluid Pressure IssuesReduce manufacturing costSurveyConstructionsWell loggingEngineering
The invention belongs to the technical field of monitoring methods, and relates to a gas cutting early stage monitoring method. The method is implemented through a gas cutting early stage monitoring device. A lower pressure meter and an upper pressure meter are installed on an underground drill rod according to a set interval, the annulus fluid pressure at the positions where the lower pressure meter and the upper pressure meter are located is measured and the annulus fluid density is further calculated. The installation distance between the lower pressure meter and the upper pressure meter can be adjusted, and the problem that the annulus fluid pressure between two close distance points cannot be measured due to the low underground fluid density is solved. The method does not depend on well logging during drilling equipment, production cost is lowered, applicability is improved, underground gas cutting is monitored through a conventional MWD or EMWD or ATWD in the oil and natural gas drilling process, and the purposes of early discovery, timely coping, avoiding of property and personnel losses are achieved. The technological process is simple, the principle is scientific and reasonable, operation is convenient, practicability is good, the using environment is friendly, universality is high, and the method is safe, reliable and easy to apply and popularize.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Green tide information extraction method

The invention belongs to the technical field of remote sensing image processing, and relates to a green tide information extraction method. The method comprises: obtaining a sea area satellite remote sensing image with a conventional method, screening images of green tide regions, and performing preprocessing operations of geometric correction and image mosaicking; calculating and determining a green tide range by adopting a normalized difference vegetation index; cutting a region of interest in any shape to generate an irregular image file containing the green tide regions; extracting green tide information by adopting a split Bregman fast projection algorithm of a variational level set two-phase image segmentation based Chen-Wees model; and finally, quantitatively calculating the green tide regions by adopting a quantitative formula. The image segmentation based variational model accurately extracts and quantifies the green tide information on the satellite remote sensing image, so that a conventional manual threshold method can be completely replaced and operational application can be realized; and method is scientific and reasonable in principle, low in human factor quantity, high in calculation speed, accurate and stable in result, high in operability, friendly in application environment, high in practicality and easy to popularize.
Owner:国家海洋局北海预报中心

Manufacturing method for hybrid heterojunction solar cell

The invention belongs to the technical field of solar cell manufacturing, and relates to a manufacturing method for a hybrid heterojunction solar cell. The manufacturing method comprises the five steps of manufacturing a conductive glass substrate, manufacturing an ordered TiO2 nanorod array film layer, manufacturing an Sb2S3 nano film layer, manufacturing a P3HT nano film layer and manufacturing an Ag film electrode. The ordered TiO2 nanorod array film layer is manufactured by adopting a one-step low-temperature hydrothermal method, the Sb2S3 nano film layer is formed by depositing Sb2S3 on the surface of the ordered TiO2 nanorod array film layer by adopting a chemical liquid phase deposition method, the P3HT nano film layer is formed by depositing P3HT on the surface of the Sb2S3 nano film layer by adopting a spin-coating method, and an Ag electrode is plated on the surface of the P3HT nano film layer by adopting a thermal evaporation method or a magnetron sputtering method at last, thereby manufacturing the TiO2/Sb2S3/P3HT hybrid heterojunction solar cell. The manufacturing method has the advantages of simple and controllable process, scientific and reasonable principle, low energy consumption and production cost, high operability, energy conservation, environment protection and friendly operating environment, can be recycled and reused, and is suitable for large-scale production, popularization and use.
Owner:QINGDAO UNIV

Preparation device of graphene composite dispersion liquid

The invention belongs to the technical field of machinery equipment, and relates to a preparation device of graphene composite dispersion liquid. A main body structure of the preparation device comprises a reaction kettle, a No.1 electrohydraulic servo mechanism, a No.1 sampling valve, a No.1 sampling opening, a No.1 pressurizing cylinder, a No.2 electrohydraulic servo mechanism, a No.2 pressurizing cylinder, a No.3 electrohydraulic servo mechanism, a No.1 pressure reduction cylinder, a No.4 electrohydraulic servo mechanism, a No.2 pressure reduction cylinder, a No.5 electrohydraulic servo mechanism, a storage container, a No.1 pressure meter, a No.1 branch pipeline, a No.1 one-way jet flow valve, a No.2 pressure meter, a safety valve, a liquid inflating valve, a liquid filling opening, a No.2 branch pipeline, a two-way jet flow valve, a No.3 pressure meter, a No.2 sampling valve, a No.2 sampling opening, a No.2 one-way jet flow valve, a No.4 pressure meter, a No.3 one-way jet flow valve, a No.5 pressure meter, a No.4 one-way jet flow valve, a No.3 sampling valve, a discharging valve, a No.3 sampling opening and a valve. The preparation device has the advantages that the structure is simple; safety and environment protection are realized; the preparation device can be widely used in the fields of chemical engineering, medicine, food processing and the like; the popularization and the use are easy.
Owner:QINGDAO HUAGAO GRAPHENE CORP LTD

GO/NR composite preparation method and open mill for preparation thereof

The invention discloses a GO/NR composite preparation method which comprises the following steps of S100, putting silicon dioxide, deionized water and a GO aqueous solution into a stirrer for stirring, and dispersing a mixture into a GO-SiO2 mixed liquid with a high-speed shearing machine; S200, adding 100 parts of centrifugal concentrated natural latex by mass in the GO-SiO2 mixed liquid, and performing ultrasonic vibration to obtain a GO-SiO2/NRL mixed liquid; S300, pouring the GO-SiO2/NRL mixed liquid into an open mill, obtaining a rubber master batch on a roller of the open mill, and scraping and collecting the rubber master batch with a scraper on the roller after the rubber master batch is dried for later use; and S400, mixing the prepared rubber master batch, zinc oxide (ZnO), stearic acid (SAD), an accelerant DPG and an anti-aging agent 4020 to finish preparation of a GO-SiO2/NRL composite. By adopting the GO/NR composite preparation method, the phenomenon of uneven combinationof molecules in the rubber master batch caused by the accumulation of groups in the process of standing and jetting is avoided, and then liquid drops are instantaneously dehydrated and dried to obtain GO-SiO2/NRL rubber master batch; and GO/NR composite preparation method is simple and controllable in process, scientific and reasonable in principle, low in energy consumption and production cost,strong in operability, more uniform in dispersion and friendly in use environment.
Owner:QINGDAO UNIV OF SCI & TECH

Disc type aircraft

The invention belongs to the technical field of flight equipment and relates to a disc type aircraft. The aircraft can vertically take off and land. A main body structure comprises a high-pressure air chamber, a disc body, a load bearing bin, exhaust pipes, landing supports, exhaust holes, a high-pressure air flow supply device and an air valve. The high-pressure air flow supply device controls high-pressure air flow to be sprayed along the upper surface of the disc body through the exhaust holes, so the disc body generates raising force larger than the gravity of the disc type aircraft, and the disc type aircraft starts to ascend and take off; The exhaust pipes at corresponding positions are controlled to be opened and closed through the air valve so that the disc type aircraft can fly in different directions, and the disc type aircraft can move forward and backward, hover, horizontally move and steer; the aircraft can be manufactured into a remote control toy, an air photography device, a low-altitude ground reconnaissance device, an agricultural condition inspection device, a disaster scene rescue device and an offshore area detection and rescue device. The aircraft is simple in structure, scientific and reasonable in principle, safe and reliable in performance, low in manufacturing and maintenance cost, and convenient to operate and maintain, and the flight environment is friendly.
Owner:吴锜

Visual blood collection needle

PendingCN108354618ASimple structureThe process of instruction is clear and fastDiagnostic recording/measuringSensorsBlood collectionInverted-T shape
The invention relates to a visual blood collection needle. The visual blood collection needle solves the technical problems that for visual blood collection needles in the prior art, the blood returning chambers are large, the indication process is unclear, the speed is low, the blood is wasted, and the accuracy of blood collection samples is low. The visual blood collection needle is provided with a transparent needle base and a stainless steel needle tube with needle tips at the two ends; a blood returning chamber is provided with a blood returning tube and a lower-end blood returning chamber which define an inverted T shape; the two ends of the stainless steel needle tube are in fixed and sealed connection with the two ends of the needle base respectively, and a gap is firmed between the stainless steel needle tube and the blood returning tube; a blood returning hole runs through the stainless steel needle tube in the blood returning tube and is communicated with the blood returningtube; a ventilation hole runs through the side wall of a filling chamber and is communicated with the exterior; the filling chamber is further internally provided with a filtering core and filled with the filtering core, and the filtering core is made of materials which can be ventilated when dried and sealed when expanded by liquid. The visual blood collection needle is widely applied to the field of medical instruments.
Owner:威海赛威医疗科技有限公司

A lifesaving seawater desalination device

The invention belongs to the technical field of marine life-saving equipment, and relates to a life-saving seawater desalination device. The main structure includes a top cover, a cup-shaped permeable core, a permeable shield, a suction pipe, a permeable layer, a one-way suction nozzle, a hanging rope, a rope winder, Inflatable air chamber, encapsulated lead, fresh water cavity, sea water cavity, cup body and sealing ring, using graphene as the main material for desalination to manufacture emergency seawater desalination devices in marine environment, providing drinking water for trapped persons in marine environment , to achieve zero energy consumption in the process of seawater desalination, and to provide a basis for the miniaturization of seawater desalination equipment. It has the characteristics of small size, light weight, convenient and reliable use, and is equipped with life jackets and life rafts on ships, aircraft and offshore platforms. On the equipment, it is used by ordinary people under extreme conditions, and can continuously provide drinking water for people trapped at sea; its structure is simple, the principle is scientific and reasonable, the operability is strong, the use environment is friendly, the survival probability of the trapped people is improved, and it is easy to popularize and use. .
Owner:QINGDAO HUAGAO GRAPHENE CORP LTD

Automatic detection control method for overflow leakage of liquid pipeline

The invention belongs to the technical field of fluid overflow leakage detection and relates to an automatic detection control method for overflow leakage of a liquid pipeline. The automatic detection control method comprises the steps that firstly, an automatic liquid pipeline overflow leakage detection control device is installed between a heating radiator and a heating pipeline; heater flow parameters are monitored by a flow sensor in real time and uploaded to a control chip; the control chip is used for operation and processing according to a set command; and when leakage of the heating pipeline is judged, the chip is controlled to control a valve to be closed automatically, and thus the loss of a heater user is reduced. The heater user regulates the heater supply quantity according to heating requirements, the control chip is used for monitoring the temperature, flow and pressure of heating media and parameter information of the flow speed in real time according to the flow sensor and controlling the valve to operate, and the valve can be closed in time when unusual conditions happen; a heating control center can check heating fee according to temperature data recorded and stored by the control chip, and the heating fee can be refunded for overpayment or supplementary payment is demanded for shortage; and the technological process is simple, the theory is scientific and reasonable, the performance is safe and reliable, energy is saved, environmental friendliness is achieved, and the use environment is friendly.
Owner:QINGDAO RUIXUEZHAO RADIATOR CO LTD

Light resisting type sliding window sash

The invention belongs to the technical field of construction and building material equipment, and relates to a light resisting type sliding window sash. A major structure comprises a sash, an upper window edge, a lower window edge, a left window edge, a right window edge, elastic stop pieces, a window body, a groove and a spring. The window sash of the rectangular frame-shaped structure is formed by defining the upper window edge, the lower window edge, the left window edge and the right window edge. A window body is arranged in the center of the window sash. Grooves of a rectangular inward concave type structure are formed in the left window edge and the right window edge in the perpendicular direction. The elastic stop pieces of an inverted T-shaped structure are arranged in the grooves in a clamped mode. 2-4 springs are arranged at the bottoms of the elastic stop pieces at equal intervals. The length of the elastic stop pieces is equal to the length of the grooves. The popup height of the elastic stop pieces is the perpendicular distance between the horizontal plane where the window body is located and the horizontal plane where the left window edge or the right window edge is located. The light resisting type sliding window sash is simple in structure, scientific and reasonable in principle, good in sealing performance and light resisting performance, environmentally friendly to use, easy to manufacture, low in manufacturing cost and applicable to building installation engineering such as residential buildings and office buildings.
Owner:QINGDAO HAICHENG INTPROP SERVICES CO LTD

A kind of preparation method of hybrid heterojunction solar cell

The invention belongs to the technical field of solar cell preparation, and relates to a method for preparing a hybrid heterojunction solar cell, comprising preparing a conductive glass substrate, preparing an ordered TiO2 nanorod array film layer, preparing a Sb2S3 nano film layer, and preparing a P3HT nano film layer And the five steps of preparing Ag thin film electrodes, using one-step low-temperature hydrothermal method to prepare ordered TiO2 nanorod array film layer, and then using chemical liquid deposition method to deposit Sb2S3 on the surface of ordered TiO2 nanorod array film layer to form Sb2S3 nano film layer , and then use the spin coating method to deposit P3HT on the surface of the Sb2S3 nano-film layer to form a P3HT nano-film layer, and finally use thermal evaporation or magnetron sputtering to plate Ag electrodes on the surface of the P3HT nano-film layer to prepare TiO2 / Sb2S3 / P3HT hybrid heterojunction solar cell; the process is simple and controllable, the principle is scientific and reasonable, the energy consumption and production cost are low, the operability is strong, energy saving and environmental protection, the use environment is friendly, it can be recycled and reused, and it is easy to be mass-produced and popularized. .
Owner:QINGDAO UNIV

A kind of preparation method of cnt/iir composite material and jet atomization gun for preparation thereof

ActiveCN109957184BAchieve dispersion effectAchieve microscopic dispersion effectMasterbatchAir pump
The invention discloses a method for preparing a CNT / IIR composite material, comprising the following steps: S100, obtaining a CNT / IIRL mixed liquid, and mixing and stirring it for standby; S200, spraying the CNT / IIRL mixed liquid to a high temperature through a gas-phase assisted spray atomizing gun On the roller of the open mill, when the water of the mixed solution on the roller evaporates, the masterbatch formed on the roller is scraped off and collected for later use; S300, add 111phr masterbatch, zinc oxide ZnO, hard Fatty acid SAD, sulfur, super-accelerator TMTD, DM accelerator, RD anti-aging agent, anti-aging agent 4020 for mixing, plasticizing and banburying of the masterbatch, and completing the preparation of GO / IIR composite materials, and atomization devices, including Assembling the frame, as well as the batching bottle, air pump and deflector set on the assembly frame, the inside of the assembly frame is provided with a micro-motion component, the micro-motion component is provided with an atomizing nozzle, and the deflector is connected to the assembly frame There is an air curtain groove at the center, the process is simple and controllable, and the principle is scientific and reasonable, which ensures uniform atomization and avoids secondary dripping due to the adhesion of water vapor.
Owner:QINGDAO UNIV OF SCI & TECH

A kind of preparation method of high temperature resistant ceramic track

The invention belongs to the technical field of novel material caterpillar bands and relates to a preparation method of a high-temperature-resistant ceramic caterpillar band. The process course comprises the three steps of preparing of powder, forming of a blank and microwave sintering. By taking aluminum oxide and 3Y-TZP micropowder as raw materials, the ceramic caterpillar band which is high in high-temperature strength, good in thermal shock property, wear-resistant, corrosion-resistant and good in dimensional stability is prepared by dispersing metastable tetragonal phase zirconium oxide particles into an aluminum oxide matrix by means of a dry pressing+isostatic pressing method and a microwave sintering techolgoy, wherein the microscopic structures are uniform fine grains 3Y-TZP-Al2O3. After sintering, the surface of the caterpillar band only needs to be polished, so that a grinding step after sintering is avoided. The service life is 10-20 times of that of a stainless steel caterpillar band, the manufacturing cost of the high-temperature-resistant ceramic caterpillar band is lowered, and the production links are reduced on the premise of improving the performance indexes, the product quality and the production efficiency of the ceramic material, so that the high-temperature-resistant ceramic caterpillar band is favorably promoted and used. The high-temperature-resistant ceramic caterpillar band is scientific and reasonable in principle, high in yield and environment-friendly and has a good industrial application prospect.
Owner:QINGDAO UNIV

A kind of preparation method of porous carbon material

The invention belongs to the technical field of preparation of porous materials and in particular relates to a preparation method of a porous carbon material. A technological process comprises the following six steps: preparing a carrageenan water solution, preparing a metal salt solution, preparing hydrogel, washing and freezing the hydrogel, freeze-drying the hydrogel and preparing the porous carbon material. The porous carbon material is prepared based on carrageenan and the carrageenan is heated and dissolved into secondary distilled water to form a carrageenan solution; then the carrageenan solution and the metal salt solution are mixed to be subjected to gelation reaction, so as to generate the hydrogel; then the hydrogel is washed, frozen, freeze-dried and pyrolyzed to prepare the Fe and S hybridized porous carbon material; in the preparation process, the reaction is moderate and easy to control and the yield and the purity of the product are high; a novel method is provided for synthesis of the porous carbon material and an application field of the porous carbon material is expanded; the technological process has the advantages of simplicity, scientific and reasonable principle, strong operability, environment protection and energy saving, friendly utilization environment and wide application prospect.
Owner:QINGDAO UNIV

System and method for prolonging service life of light quantum lamp

PendingCN113613357ASolve large fluctuations in current, frequent start and stop, and accelerated damage to discharge lamp equipmentThe principle is scientific and reasonableElectrical apparatusElectric lighting sourcesComputational physicsPotentiometer
The invention discloses a system for prolonging the service life of a light quantum lamp, and the system comprises a lamp current sensor module which is used for detecting the current value of the light quantum lamp; a potentiometer module used for adjusting the voltage and current of the light quantum lamp; a comparison module used for comparing one path of input voltage with one path of fixed reference voltage; a protection electrode used for maintaining the discharge electrode in the discharge tube and eliminating residual nitrogen, oxygen and water vapor; a timing module used for system timing; and a control module used for controlling the system module. The lamp current sensor module, the potentiometer module, the comparison module, the protection electrode and the timing module are electrically connected to the control module, the maximum safety rated current of the lamp current sensor module is 200-400 mA, and the voltage of the lamp current sensor module is 6-3 v. Through the implementation of the light quantum lamp, the service life of the light quantum lamp is prolonged, residual nitrogen, oxygen and water vapor can be eliminated, the principle is scientific and reasonable, the effect is high, and prominent progress is achieved.
Owner:浙江光氧环保科技有限公司

A kind of cnt-sio 2 /nbr material preparation method and atomizing spray gun

ActiveCN109985710BAchieve dispersion effectAchieve microscopic dispersion effectGrain treatmentsSlurrySilicon oxide
The invention discloses a CNT-SiO 2 / NBR material preparation method, S100, grind silica to 100-200 mesh, place deionized water in a beaker, disperse into silica water dispersion, and stir to obtain silica slurry; S200, CNT aqueous solution and di The silica slurry was stirred and mixed, and the centrifuged concentrated nitrile latex was added to CNT‑SiO 2 In the mixture, stir to complete the CNT‑SiO 2 Preparation of / NBRL mixed solution; S300, CNT-SiO 2 / NBRL mixture using gas phase assisted jet atomization gun to CNT‑SiO 2 / NBRL mixture is sprayed onto the roller of the high-temperature open mill; S400, adjust the temperature of the roller to make CNT-SiO 2 / NBRL mixed solution is atomized into droplets to obtain dry masterbatch, and the scraper on the roller scrapes off the masterbatch and collects it for later use; S500, banbury the prepared masterbatch on the open mill, and add masterbatch and zinc oxide in turn ZnO, stearic acid SAD, DPG accelerator, anti-aging agent 4020 are mixed to obtain CNT-SiO 2 / NBR composite material, the process is simple and controllable, and the principle is scientific and reasonable, which ensures uniform atomization and mixing compatibility, and avoids secondary dripping caused by water vapor adhesion.
Owner:QINGDAO UNIV OF SCI & TECH

a cnt-sio 2 /ci material preparation method and grinding device

The invention discloses a preparation method of a CNT-SiO2 / CI material. The preparation method comprises the following steps: S100, mixed liquid of silicon dioxide and deionized water is dispersed into silicon dioxide aqueous dispersion through a high-speed shearing machine, and then ground through a grinding machine; S200, obtained silicon dioxide slurry is stirred and mixed with a CNT water solution with the appropriate proportion, and a centrifuged and concentrated neoprene latex is added to be mixed and stirred; S300, CNT-SiO2 / CIL mixed liquid is sprayed onto a roller of a high-temperatureopen mill, and an adhesive layer is formed ; S400, the adhesive layer is scraped down for standby application; and S500, masterbatch is plastified and subjected to banburying on the open mill. A grinding device comprises a base and a mounting groove formed in the base; a planet wheel is arranged in the mounting groove, and a fixing support is arranged on a star wheel of the planet wheel; and thefixing support is provided with a grinding tank through a movable hinge device, a pressing rod device is mounted on the grinding tank, a shunt disc is arranged on the upper part of the grinding tank,is connected into the mounting groove, and comprises an inner wheel disc and an outer rail ring, thus grinding is sufficient, and the grinding confusion degree of the slurry is increased.
Owner:QINGDAO UNIV OF SCI & TECH

An intelligent heating valve

The invention belongs to the technical field of valves and relates to an intelligent heating valve. The intelligent heating valve comprises a valve body, a display panel, a flow sensor, a control chip, an alarm module, an operation module, a wireless transmission module, a charging module and a battery compartment, wherein the display panel and the battery compartment are fixedly arranged at the outer part of the valve body, the flow sensor is arranged between the valve body and a heating pipeline, and the control chip consisting of the alarm module, the operation module, the wireless transmission module and the charging module is arranged in the valve body; and the display panel is in electric information communication with the flow sensor and the control chip, the flow sensor is in electric information communication with the control chip, and the valve body is separately in wireless connection with a heat supply control center and a heating user. The heating user can remotely grasp heat supply information, pay heating fees and regulate heat supply quantity according to requirements, and the heat supply control center can open and close the valve and calculate, gather and return heating fees. The intelligent heating valve is simple in structure, is scientific and reasonable in principles, is safe and reliable in performance, is energy-conservative and environment-friendly, is low in maintenance cost and is friendly to use environment.
Owner:QINGDAO RUIXUEZHAO RADIATOR CO LTD

A method for early monitoring of air intrusion

InactiveCN105298472BTroubleshooting Annular Fluid Pressure IssuesReduce manufacturing costSurveyConstructionsLow densityPetroleum
The invention belongs to the technical field of monitoring methods, and relates to an early monitoring method for gas intrusion, which is implemented by using an early gas intrusion monitoring device, and a lower pressure measuring device and an upper pressure measuring device are installed on a downhole drill pipe according to a set interval to measure the positions respectively The annular fluid pressure and the annular fluid density are calculated. The installation distance between the lower pressure measuring device and the upper pressure measuring device can be adjusted, which solves the problem that the annular fluid pressure between two close points cannot be measured due to the low density of the downhole fluid. Do not rely on logging while drilling equipment, reduce production costs, increase applicability, use conventional MWD, EMWD or ATWD in the process of oil and gas drilling to monitor the occurrence of downhole gas invasion, realize early detection, timely response, and avoid property and personnel The purpose of loss; the technological process is simple, the principle is scientific and reasonable, the operation is convenient, the practicability is good, the use environment is friendly, the versatility is strong, safe and reliable, and it is easy to popularize and use.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

A kind of preparation method of ceramic wire drawing die

The invention belongs to the technical field of production of dies for novel materials and relates to a production method of a ceramic drawing die; the production method comprises the steps of preparing a suspension, forming a green body, sintering conventionally, and sintering by microwave; alumina and 3Y-TZP micropowder are subjected as materials to advanced isostatic one-step forming technique and microwave sintering technique to produce the ceramic drawing die; after sintering, polishing the surface of the ceramic drawing die is only required for use; wear-resistant crystal of the ceramic die is tightly combined in solid-phase combination manner, and the ceramic crystal has improved bonding strength and increased density; the ceramic is subjected to solid-phase sintering, integral hardness is improved, the ceramic crystal interfacial strength and toughness can resist drawing pressure stress and shearing damage, a wear mechanism of the drawing die is changed, the service life of the drawing die is 4-6 longer than that of a hard alloy die, the manufacture cost of the ceramic drawing die is lowered, and production steps are lessened at the premise of improving performance index, quality and production efficiency of ceramic material; the principle of the method is scientific and reasonable, and the yield is high.
Owner:QINGDAO UNIV
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