The invention belongs to the technical field of machinery equipment, and relates to a preparation device of graphene composite dispersion liquid. A main body structure of the preparation device comprises a reaction kettle, a No.1 electrohydraulic servo mechanism, a No.1 sampling valve, a No.1 sampling opening, a No.1 pressurizing cylinder, a No.2 electrohydraulic servo mechanism, a No.2 pressurizing cylinder, a No.3 electrohydraulic servo mechanism, a No.1 pressure reduction cylinder, a No.4 electrohydraulic servo mechanism, a No.2 pressure reduction cylinder, a No.5 electrohydraulic servo mechanism, a storage container, a No.1 pressure meter, a No.1 branch pipeline, a No.1 one-way jet flow valve, a No.2 pressure meter, a safety valve, a liquid inflating valve, a liquid filling opening, a No.2 branch pipeline, a two-way jet flow valve, a No.3 pressure meter, a No.2 sampling valve, a No.2 sampling opening, a No.2 one-way jet flow valve, a No.4 pressure meter, a No.3 one-way jet flow valve, a No.5 pressure meter, a No.4 one-way jet flow valve, a No.3 sampling valve, a discharging valve, a No.3 sampling opening and a valve. The preparation device has the advantages that the structure is simple; safety and environment protection are realized; the preparation device can be widely used in the fields of chemical engineering, medicine, food processing and the like; the popularization and the use are easy.