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100 results about "Polyamide epoxy" patented technology

Preparation method of permeation resistant addition agent with functions of reinforcing stiffness and wet-strength

The invention discloses a preparation method of a permeation resistant addition agent with functions of reinforcing stiffness and wet-strength. The preparation method comprises the following main operating steps of: (1) firstly synthesizing midbody polyamide, then carrying out epoxidation on the polyamide and chloroepoxy propane to obtain polyamide epoxy chloropropane resin; (2) firstly synthesizing seed emulsion, then synthesizing a shell, obtaining a product which is fluorine containing acrylic ester core-shell emulsion; (3) carrying out composition modification on polyamide epoxy chloropropane and the fluorine containing acrylic ester core-shell emulsion to obtain the permeation resistant addition agent with the functions of reinforcing stiffness and wet-strength. According to the preparation method, the fluorine containing acrylic ester core-shell emulsion is used for carrying out composition modification on the PAE (Polyamide Epoxy chloropropane resin) so that the periphery of the emulsion particles are adsorbed and coated by macromolecules of the PAE (Polyamide Epoxy chloropropane resin) to prepare the cationization PAE (Polyamide Epoxy chloropropane resin) modified fluorinecontaining acrylic ester core-shell emulsion; the modified PAE (Polyamide Epoxy chloropropane resin) is a stable multifunctional papermaking addition agent and has the characteristic of wet-strength sizing.
Owner:GUANGXI UNIV

Method for preparing C21dicarboxylic acid polyamide epoxy hardener from methyl eleostearate

InactiveCN101280056AReduce energy consumptionEasy to distill and purifyEpoxyPolyamide
The invention belongs to the preparation field of epoxy curing agents and discloses a method of preparing C21 dicarboxylates polyamide epoxy curing agent with methyl eleostearate as follows: the first step: 100 molar portions of methyl eleostearate, 20.6-30.9 molar portions of acrylic acid, and inhibitor accounting for 0.5% to 1.5% mass of the acrylic acid are processed with addition reaction at 160 to 180 DEG C for 2 to 3 hours; then the non-reactant is removed through vacuum distillation and the reactant is decolorized through depigmenting agent so as to obtain C21 dicarboxylic acid monomethyl ester. The second step: 1 mol of C21 dicarboxylic acid monomethyl ester obtained from the first step is added drop by drop into 1.5-2 mol of polyamine which is of 140 DEG C within 0.5 hour, then the mixture liquid is processed with amidation at 170 to 200 DEG C for 3 to 6 hours; later, water and free amine are removed through vacuum distillation, so the C21 dicarboxylates polyamide epoxy curing agent is obtained. The methyl eleostearate of the invention has an 85% yield, high reactivity and low energy consumption needed in the reactions; the prepared C21 dicarboxylates polyamide epoxy curing agent and the epoxy solid products have high strength and modulus and good heat-resistant performance.
Owner:INST OF CHEM IND OF FOREST PROD CHINESE ACAD OF FORESTRY

Waterproof packing cardboard and producing method thereof

The present invention relates to a waterproof and antirust packaging paperboard and a manufacturing method thereof. Said method comprises coating one side of a waterproof paperboard with a layer of surface water-resistance agent, wherein said waterproof paperboard is made of a paper board containing a composite water-resistance agent prepared by mixing alkyl ketene dimmer and polyamide epoxy resin with a proportion of 4-6:1 by weight. The beneficial effects in accordance with the present invention are as follows: 1, the waterproof paperboard manufactured by a multi-layer recombination not only exhibit better intensity, tenacity and impact resistance, but also has excellent waterproof and damp proof insulation performances, and further exhibits better antirust performance after being coated with a vapor phase inhibitor, then said paperboard has excellent packaging performances which is stable, and the packaging requests and outdoor storage requests can be satisfied by packaging steel (coil) sheet materials with the waterproof paperboard in accordance with the present invention; 2, the manufacturing cost is low ans the source of the raw material is extensive; 3, said waterproof paperboard can be recovered and recycled easily, and is naturally degradable, and then is environment-friendly.
Owner:武汉市江夏区江南实业有限公司 +1

Thiourea modified polyamide epoxy curing agent and preparation method

The invention discloses a thiourea modified polyamide epoxy curing agent and a preparation method thereof. The thiourea modified polyamide epoxy curing agent is prepared from polyamide and thiourea. The thiourea modified polyamide epoxy curing agent disclosed by the invention is prepared through an optimal raw material ratio screened by a lot of experiments. According to the preparation method, polyamide is prepared firstly through an optimum scheme and the thiourea modified polyamide epoxy curing agent with an excellent performance is prepared by taking the polyamide and thiourea at a preferable ratio to react. An experiment result shows that the thiourea modified polyamide epoxy curing agent prepared by the preparation method enables epoxy resin to be rapidly cured at low temperature of -10 DEG C and an epoxy resin cured thin film has excellent toughness and adhesive force; the surface of the film does not easily absorb moisture and the corrosion-resisting and drug-resisting performances are excellent; requirements on application of low-temperature environment epoxy heavy-duty anticorrosive paint can be met. Compared with other curing agents, the thiourea modified polyamide epoxy curing agent has more excellent performances and very good technical effects are obtained.
Owner:江苏三木化工股份有限公司 +1

Emulsified asphalt cold-recycling layer interface bonding material as well as preparation method and application thereof

The invention relates to an emulsified asphalt cold-recycling layer interface bonding material which is prepared from the following raw materials: a component A, a component B, a component C, a component D and a component E. The component A is waterborne epoxy resin; the component B is a polyamide epoxy curing agent; the component C is formed by mixing a stabilizer and water; the component D is formed by mixing solid SBS, xylene, a compound emulsifier, a defoaming agent and water; the component E is formed by mixing asphalt, a medium-crack emulsifier, phosphoric acid and water; the emulsifiedasphalt cold-recycling layer interface bonding material comprises following components in parts by mass: 3-25 parts of the component A, 3-25 parts of the component B, 3-15 parts of the component C, 5-10 parts of the component D and 40-90 parts of the component E, the interface bonding performance between the emulsified asphalt cold-recycling layer and the upper layer is improved, the water damageresistance and the durability of the pavement are improved, and the product is non-toxic, high in stability, high in bonding strength, high in shear strength, good in waterproof performance and good in durability.
Owner:山西工程科技职业大学 +1
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