This invention relates to the field of nanoscale full-spectrum photocatalytic materials, and particularly to a method for preparing a
molybdenum selenide /
oxygen-deficient
bismuth oxybromine@gold three-phase Z-type
heterojunction photocatalyst. This method solves the problems of low
photogenerated electron-hole separation efficiency, narrow full-spectrum response range, and poor stability in existing
bismuth-based photocatalysts. The preparation method involves first preparing
oxygen-deficient BiOBr nanospheres via a solvothermal method, then directly reacting tetrachloroauric acid with
oleylamine in
toluene to prepare small-particle-size monodisperse Au nanoparticles, which are then combined with
oxygen-deficient BiOBr to prepare a BiOBr@Au nanosphere core-shell structure. Finally, a MoSe2 / oxygen-deficient BiOBr@Au three-phase
composite material is prepared via a
hydrothermal reaction. The catalyst of this invention exhibits
absorption capacity under the full spectrum of light, and simultaneously achieves a synergistic enhancement of carrier separation efficiency and strong
redox capability, demonstrating excellent photocatalytic activity and the ability to efficiently degrade pollutants and produce
hydrogen.