The invention relates to the technical field of
electrolyte additives, in particular to a preparation method of a
silane modified
zirconium phosphate electrolyte additive, which comprises the following steps: S1, introducing a
zirconium source and a
phosphorus source into a high-pressure synthesis kettle, fully stirring and mixing, and carrying out
hydrothermal reaction to obtain nano
zirconium phosphate; s2, dispersing the nano
zirconium phosphate of the adjusting mechanism obtained in S1 into absolute ethyl
alcohol, then introducing into a main chamber of a
surface modification device, and adding a
silane coupling agent into the main chamber of the adjusting mechanism, so that the
mixed solution is preliminarily mixed in the main chamber of the adjusting mechanism; s3, after preliminary mixing, modifying the
mixed solution at the bottom of the main chamber of the adjusting mechanism in an acoustoelectric
coupling module of the adjusting mechanism under the combined action of an
electric field and
ultrasound; s4, after modification is completed, the
silane modified
zirconium phosphate electrolyte additive is obtained. The preparation method provided by the invention can efficiently and stably obtain silane modified
zirconium phosphate of which the surface hydroxyl coverage rate is greatly reduced, and has good application value.