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Flexible lithium ion battery black phosphorus nanosheet-graphene composite film anode, and preparation thereof

The invention belongs to the field of electrochemistry battery, and more specifically relates to a black phosphorus nanosheet-graphene composite film anode used for flexible lithium ion batteries, and a preparation method thereof. According to the preparation method, high purity and large scale black phosphorus blocks are synthesized via mineral substance assistant vapor transporting method with high efficiency; a large amount of clean and high quality black phosphorus sheets are prepared in water via ultrasound treatment; the clean and high quality black phosphorus sheets and high conductive graphene nanosheets prepared via intercalation stripping method are subjected to mixing ultrasonic dispersion; and flexible high-strength laminated composite film is prepared via vacuum filtration. The preparation process of the flexible high-strength laminated composite film is simple and controllable; large scale low cost preparation can be realized; black phosphorus nanosheets are high in capacity, graphene is high in electrical conductivity, and the black phosphorus nanosheets and graphene both possess two-dimensional structures high in flexibility and strength, so that problems the black phosphorus is poor in electrical conductivity and stability are solved, lithium ion battery capacity, cycling stability, and entire energy density are increased, and lithium ion battery electrode integrated flexible design is realized.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI +1

Construction method of long-service-life pass-through induced drainage pavement

The invention discloses a construction method of a long-service-life pass-through induced drainage pavement. The construction method comprises the following steps: 1, preparing filtering materials of the pass-through water-induced pavement, including coarse aggregate, fine aggregate and modified bituminous mixture according to the weight ratio of 58.5 to 35.85 to 5.65, wherein the modified bituminous mixture comprises slaked lime, red mud and conjugate fiber according to the weight ratio of 58.5 to 35.85 to 5.65, and the conjugate fiber comprises wood fiber and basalt fiber according to the weight ratio of 1 to 2; 2, processing a substrate of the construction pavement; 3, arranging an adhesive layer or sealing layer which has the thickness of 0.1-0.2mm and the porosity of 30%; 4, arranging a substrate filtering material layer which is 0.05-0.15mm thick between a soil layer and a gravel layer of the substrate; 5, mechanically paving; 6, treating joints; and 7, maintaining the pavement. The construction method can obviously improve the adhering force, anti-cracking performance, tensile and water-damage resistance performance and noise reducing performance of the pavement, enhance the rainstorm resistance of the pavement, and reduce the influence of long-term rain storage on stability performance of bituminous concrete.
Owner:郑州市公路工程公司

High-capacity graphene/ silicone composite negative electrode material and preparation method

The invention belongs to the field of preparation of negative electrode materials of lithium ion cells, and discloses a high-capacity graphene/ silicone composite negative electrode material and a preparation method. The method specifically comprises the following steps: preparing certain graphene oxide solution by a modified Hummer method; preparing tetraethoxysilane as a silicone source; uniformly mixing the silicone source with the graphene oxide and magnesium powder based on certain ratio; ultrasonically dispersing; drying the mixed solution into powder through a spraying drying device; reducing under high temperature in certain atmosphere; washing with diluted acid and distilled water in a plurality of times; drying; and grinding powder with certain fineness. According to the method,tetraethoxysilane is used as the silicone source which is high in compatibility; the reaction time is controllable; and moreover, silicone can be effectively wrapped with graphene, so that the electricity conductivity of the silicone can be improved; and meanwhile, the silicone expansion in charging and discharging process can be avoided. Therefore, the circulating performance and the multiplyingpower of the cell with the silicone negative electrode material can be improved.
Owner:厦门紫阳科技产业发展有限公司

Extract liquor purification treatment method for paper-making reconstituted tobacco

The invention discloses an extract liquor purification treatment method for paper-making reconstituted tobacco. The method comprises following steps: 1, putting tobacco materials containing tobacco stems, fragments and tobacco waste into an extraction tank employing water as an extraction solvent, performing solid-liquid separation after the extraction so as to obtain the solid and the extract liquor, wherein the solid is used for pulping and paper-making so as to form the paper base; 2, putting functional fibers into a hydro-pulper for pulping, and performing beating after the pulping; 3, sandwiching the beaten functional fibers between two filter screen layers to form a filter cake layer, and enabling the extract liquor to penetrate the filter cake layer; or directly adding the pulped functional fibers into the extract liquor, allowing the extract liquor to stand after the extract liquor is fully stirred, and adding guar gum into the extract liquor so as to make the functional fibers to fully and rapidly flocculate; and 4, purifying the extract liquor sequentially through a mesh screen and a horizontal screw decanter centrifuge, enabling the purified extract liquor to penetrate a condensation device for condensation, dip-coating the concentrated solution on the paper base, and drying and cutting the paper base so as to obtain the tobacco. According to the invention, the clarity degree of the extract liquor is improved by 35.23%, the color is bright, and the taste is improved.
Owner:CHINA TOBACCO JIANGSU INDAL

Barrier device with function of easily adjusting size for engineering blasting

The invention discloses a barrier device with a function of easily adjusting the size for engineering blasting. The barrier device comprises fixing rods, barrier plates and a base, wherein the fixingrods are uniformly installed on the top of the base, supporting corner brackets are installed at the positions where the bottoms of the fixing rods are connected with the base respectively, fixing sleeves are arranged on the fixing rods respectively, and the barrier plates are arranged on one sides of the fixing sleeves respectively. Fixing bases are uniformly installed on one sides of the barrierplates respectively, the fixing bases are fixedly connected with the fixing sleeves, and shock-absorption plates are arranged on the sides, away from the fixing bases, of the barrier plates respectively. According to the barrier device with the function of easily adjusting the size for engineering blasting, by arranging water-penetration membranes and water-absorption sponge, when stones spattered in the blasting process squeeze the shock-absorption plates and the barrier plates, water absorbed in the water-absorption sponge easily seeps out of the water-penetration membranes after being squeezed and overflows through water outlets, dust generated during blasting is effectively wrapped, less dust rises, and therefore, the pollution of the dust to the environment is reduced.
Owner:GUIZHOU UNIV

Adjustable jetting support for dust control of comprehensive mechanized excavation surface of mine

An adjustable jetting support for dust control of a comprehensive mechanized excavation surface of a mine comprises a support plate and a plurality of connecting lugs. A plurality of input port through holes are disposed in the middle of the support plate at intervals, delivery pipes penetrate through the input port through holes, strip-shaped holes are disposed on two sides of each input port through hole, an elongated bolt is arranged in each strip-shaped hole, a sprayer mounting branch pipe connected with a corresponding input pipe is disposed at the front of each input port through hole of the support plate, branch pipe fixing lugs are arranged on the upper side and the lower side of each sprayer mounting branch pipe and are respectively sleeved on the corresponding elongated bolts, each elongated bolt is provided with an adjusting nut used for fixing and adjusting the distance from the corresponding sprayer mounting branch pipe to the support plate, and a plurality of sprayers are disposed on the sprayer mounting branch pipes. The adjustable jetting support is applicable to treating high-concentration dust by the aid of dust falling media such as water mist, foam and the like when an underground coal mine comprehensive mechanized heading machine cuts and crushes coal rocks, dust falling efficiency and utilization rate of the dust falling media are increased, and the adjustable jetting support is simple in structure, simple and convenient in operation and easy to repair and replace.
Owner:CHINA UNIV OF MINING & TECH

Metformin hydrochloride sustained-release tablet and preparation method thereof

The invention relates to a metformin hydrochloride sustained-release tablet and a preparation method thereof, and belongs to the technical field of medicine. The metformin hydrochloride sustained-release tablet is composed of sustained-release granules, sustained-release microcapsules and a lubricant, and is prepared through tabletting, wherein the weight ratio of the metformin hydrochloride in the sustained-release granules and the metformin hydrochloride in the sustained-release microcapsules is (3:7)-(6:4), and the lubricant is selected from superfine silica powder or magnesium stearate. According to the preparation method, a traditional spray drying method is improved, by combining a dry granulation process, the sustained-release microcapsules and sustained-release granules of different processes are prepared, tabletting is further carried out to prepare the metformin hydrochloride sustained-release tablet, the specific ratio of the sustained-release microcapsules prepared by the spray drying process to the sustained-release granules prepared by the dry granulation process is explored, and the metformin hydrochloride sustained-release tablet of which the inner portion has the structure of the sustained-release microcapsules and the sustained-release granules is finally obtained. The metformin hydrochloride sustained-release tablet and the preparation method thereof achievea good release behavior of the sustained-release tablet, overcome the shortcomings of sudden release and incomplete release, obtain a better release curve, and also greatly reduce the impurity content.
Owner:CSPC OUYI PHARM CO LTD
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