The invention relates to the technical field of 
organic synthesis, in particular to a preparation method of azacyclo-
sulfide and a purification method of same. The preparation method comprises the steps of 
raw material extraction, substrate expansion, nucleophilic preparation, oxidation modification, vibration, standing and purification. A reaction tank comprises a tank body, a reaction vessel anda 
burette; a plurality of 
layers of reaction vessels are arranged in the tank body; the 
burette pipeline comprises a 
titration disc and a shunt 
pipe; because the dispersion degrees of the substratesin the 
mixed solution are different and the speed of adding the substrates into the reaction tank is changed, the purity effect of the required azacyclo-
sulfide extraction can be influenced; therefore, according to the invention, the reaction vessel and the 
titration disc are correspondingly arranged in the reaction tank; the reaction vessel is provided with the inclined reaction tank, the speed of a substrate solution entering the 
titration disc is balanced by matching with the shunt 
pipe inclined to the titration disc, and the 
servo motor drives the inclined reaction tank to rotate, so thatthe substrate added into the reaction vessel uniformly covers the surface of the reaction vessel, and the preparation purity of the azacyclo-
sulfide is improved.