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72results about How to "Dense floc" patented technology

Sulfide heavy metal chelating agent and preparation method thereof

The invention discloses a sulfide heavy metal chelating agent and a preparation method thereof; the method adopts a reaction between sodium sulfide water solution and sulfur to generate sodium polysulfide and uses aluminum sulfate, aluminium chloride and other aluminum salts as stabilizers so as to strengthen the flocculation effect and increase the catching effect on heavy metal ions. The chelating agent is used to treat the industrial wastewater containing heavy metal ions, can effectively restrain the generation of hydrogen sulfide, and reacts with all kinds of heavy metal ions quickly at room temperature to generate water insoluble sulfides precipitate, wherein, the particles of the produced sulfides is large, the floccule is dense and the settling time is reduced so that the concentrations of the heavy metal ions in wastewater are easy to be reduced below the national discharge standard, the generated residue can be used for recycling heavy metals and secondary pollution is not easy to cause; the method of the invention has simple devices, convenient operation and low cost, thus being applicable to the wastewater treatment in industries such as circuit board industry, plating industry, metal finishing industry, manufacturing industry, coal power stations, municipal or industrial waste incineration industry, battery production and the like.
Owner:南京正隆环保工程有限公司

Solid composite polymeric ferric sulfate flocculant and preparation thereof

The invention provides a solid composite polymeric ferric sulfate flocculating agent used in the treatment of high-concentration organic starch wastewater. The flocculating agent takes ferrous sulfate and sodium bentonite as raw materials and sulphuric acid and hydrogen peroxide as oxidizing agents, is obtained after oxidative polymerization, aging, concentrating and settling, and is a straw yellow solid which has stable performance and is convenient for storage and transportation; during the treatment of high-concentration organic starch wastewater, the flocculating agent ensures quick settling velocity of floc, compact floc, excellent deodorization effect, relatively high removal rate of COD and large removal value of COD, and has high use value; the flocculating agent has low energy consumption during preparation; moreover, the flocculating agent has the advantages of cheap and easily obtained raw materials, low cost, simple device and process and convenient operation, and is easy to realize industrial production.
Owner:NORTHWEST NORMAL UNIVERSITY

Environmental functional material applied to electroplating wastewater treatment

The invention discloses an environmental functional material applied to electroplating wastewater treatment; all components are as follows by mass percentage; kieselguhr, modified purified diatomite,bentonite, modified purified bentonite, attapulgite, modified purified attapulgite, kaoline and / or 20-80 percent of modified purified kaoline, 10-40 percent of humic acid and 10-40 percent of chitosan. The material has convenient usage, good treatment effect, and large and dense formed floccules, shortens settling time, and is easy to lead heavy metal ions, COD, ammonia-N, phosphorus, chromaticity and other indexes in wastewater to synchronously achieve discharge standard regulated nationally, the produced residue can recycle heavy metal, and secondary pollution is not easy to generate. Thematerial is suitable for treating wastewater in industries such as circuit boards, electro-plating, metal finishing, photographic film manufacturing, coal plants, municipal or industry waste incineration, battery production and the like.
Owner:NANJING NORMAL UNIVERSITY

Method for synthesizing composite kieselguhr coagulant from kieselguhr waste liquor

The invention relates to a method for synthesizing a composite kieselguhr coagulant, particularly a method for synthesizing a composite kieselguhr coagulant from kieselguhr waste liquor. The invention aims to solve the problems of small basicity of PAFS (polymeric aluminum ferric sulfate) or PAFC (polymeric aluminum ferric chloride) and weak bridge adsorbing function in the kieselguhr coagulant prepared by the existing method. The method comprises the following steps: 1. preparation of fine kieselguhr; 2. modification of the fine kieselguhr; and 3. synthesis of the composite kieselguhr coagulant. The composite kieselguhr coagulant synthesized by the method provided by the invention has the advantages of faovorable removal rate for turbidity and CODCr, small addition amount, wide pH applicability and low price, and enhances the economical efficiency when being used for treating wastewater; and in the composite kieselguhr coagulant preparation process, the previously modified kieselguhr is added to enhance the hydroxy polymerization degree in the PAFS or PAFC preparation process by utilizing the electropositivity on the surface of the modified kieselguhr, thereby greatly increasing the basicity of the PAFS or PAFC and enhancing the bridge adsorbing function of the coagulant.
Owner:JILIN YINDA WATER AFFAIR TECH

Method for preparing oxidized form polysilicic acid ferro-aluminum coagulant

The invention discloses a method for preparing an oxidized form polysilicic acid ferro-aluminum coagulant. The method includes the following steps that (1) a sodium silicate solution is added to a dilute sulphuric acid solution under the stirring condition, the pH value is adjusted to acidity, and standing and polymerization are conducted on the mixture to obtain low-polymerization-degree activated silicic acid; (2) ferric sulfate and aluminum sulfate are added to concentrated sulfuric acid and water to prepare an acidic sulfate ferro-aluminum solution; (3) low-polymerization-degree activated silicic acid and the acidic sulfate ferro-aluminum solution are mixed and stirred, an oxidizing agent and additive are added, stirring is stopped, after standing and curing are conducted, a stabilizing agent is added, and then liquid products are obtained; (4) the liquid products are dried and grinded to obtain the powder coagulant. The products prepared from the method combine the advantages of an iron coagulant and an aluminum coagulant, the defects of polyaluminum chloride and polyferric sulfate coagulants in the using process are overcome, and the products have the advantages of capable of integrating the polysilicic acid cementation, aggregation, adsorption and bridging effects, large in aluminum salt coagulant floc, good in decoloration performance, dense in ferric salt coagulant floc, and high in settling speed.
Owner:CHINESE RES ACAD OF ENVIRONMENTAL SCI

Preparation method of sulfide heavy metal trapping agent C2H4N2S4

The invention discloses a preparation method of sulfide heavy metal trapping agent C2H4N2S4. Cyclohexanol and acetone are prepared according to a certain volume ratio and used as a mixed solvent, carbon disulfide is dissolved in the mixed solvent to obtain a carbon disulfide mixed solution, the carbon disulfide mixed solution is slowly added in hydrazine hydrate in dropwise mode under stirring state according to a certain molar ratio, reaction is performed at a certain temperature, suction filtration is performed on reaction products, a filter cake is washed through absolute ethyl alcohol, and C2H4N2S4 can be obtained. The method selects cyclohexanol to replace ethylene glycol, can greatly reduce dosage of cyclohexanol in the mixed solvent, simultaneously improves product yield, and reduces production cost of C2H4N2S4.
Owner:NANJING NORMAL UNIVERSITY

High efficiency water purification agent

The invention relates to a method for preparing high- performance water purification agent. The activated sodium silicate is polymerized with ferric sulfate, and modifies with chloride ion during process of producing polymeric ferric sulfate. It comprises following steps: adding 5- 6 units sodium silicate ((M=3.3,SiO2%=26) into autoclave, adding 20- 13 units water, stirring evenly, adding 2 units industrial concentrated sulfuric acid quickly, reacting at 40- 50 Deg. C for 0.5 hour, then adding 42- 45uints 90% ferric persulfate, 1- 2 units sodium chloride, 3- 5 units aluminum sulphate acetate, 4- 5 units industrial concentrated sulfuric acid, dropping 13- 14 units 27.5% hydrogen dioxide solution slowly, controlling temperature to be lower than 60 Deg. C, reacting for 2 hours, dissolving 1- 2 units sodium orthophosphate in 10- 7 units water and adding them into autoclave, reacting for another 0.5 hour, curing 24 hours and getting final product. The product is characterized by apparent functions of removing color, odor, oil, disinfection and removing COD and BOD.
Owner:GUANGZHOU GELONG ENVIRONMENTAL PROTECTION TECH DEV

Composite water purifying agent and preparation method and application thereof

The invention relates to the field of water treatment, in particular to a composite water purifying agent and a preparation method and application thereof. The composite water purifying agent is mainly prepared from polymeric ferric sulfate, dimethyl diallyl ammonium chloride, vinyl trimethoxy silane and polysilicic acid. The total amount of iron and the pH value of the composite water purifying agent are limited, the combination of organic components and inorganic components is closer, the flocculation capability of obtained flocculating constituents is greatly improved, and the composite water purifying agent has a good effect of removing phosphorus in water. According to the special preparation method, the combination of the organic components and the inorganic components forming the composite water purifying agent is closer, and the flocculation capability of the flocculating constituents is improved. The method is simple and easy to operate, does not produce harmful gas in the production process, and is safe and reliable. The composite water purifying agent is applied to treatment for phosphorus wastewater, has the advantages of being less in feeding amount, compact in flocculating constituents, high in sedimentation velocity, good in water-out effect, less in sludge quantity and low in treatment cost, and has significant social and economic benefits.
Owner:神美科技有限公司

Method for in-situ pillared modification of bentonite and algal-removing water purifying agent

The invention belongs to the field of natural fresh water environment protection and mineral processing and utilization and discloses a method for in-situ pillared modification of bentonite and an algal-removing water purifying agent prepared by using the same. Unlike the conventional pillared modification method, the method of the invention is characterized in that: Al<3+> is complexed and exchanged into an mineral inter-layer domain first through ion exchange; and microwave radiation and alkali titration are used to force the Al<3+> to undergo in-situ hydrolytic polymerization in a smectiteinterlayer domain to form Al13 pillar. The method directly uses bentonite of any quality, saves a bentonite sodium treatment process and is simple, low in cost and high in synthesis efficiency. The algal-removing water purifying agent of the invention gives an effective play to the adsorption property of the bentonite and the coagulation, electrical neutralization and other functions of Al13<7+> polycation, has obvious advantages of environmental protection, low cost, compact coagulation, quick sedimentation, removal of suspended matters such as blue-green algae, turbidity and phosphorus nitride and the like and ensures that the treated water is transparent and stable in alkalinity or acidity of the water quality.
Owner:NINGBO XINKE TEXTILE AUXILIARY

Sulfide heavy metal chelating trapping agent and preparation method thereof

The invention discloses a sulfide heavy metal chelating trapping agent. The trapping agent is prepared by a method of: dissolving 550g of mercaptoethylamine hydrochloric acid into 3L of chloroform; adding 900g of triethylamine as an acid binding agent; adding 400g of 3,3',5,5'-biphenyl 4-formyl chloride into 2L of chloroform; stirring and mixing the two kinds of solution, wherein the stirring velocity is between 30 and 100 r.min<-1>; performing a condensation reaction in an ice bath for 3 to 8 hours under protection of nitrogen; filtering the mixture, and extracting with water and the chloroform respectively; and distilling out redundant solvent with a rotary evaporator to obtain a white precipitate, namely a target product. The trapping agent fast reacts with various heavy metal ions in waste water at the normal temperature and generates a water-insoluble sulfide precipitate. The sulfide heavy metal chelating trapping agent has the advantages of simple preparation process and convenient use. The particle size of the produced sulfide precipitate is large, the floc is compact, the precipitation time is reduced, the concentration of heavy metal ions in the waste water below the national discharging standard, generated residue can be used for recycling heavy metal, and no secondary pollution is generated, The trapping agent can also be used for recycling precious metal in aqueous solution.
Owner:南京正隆环保工程有限公司

Magnetic flocculating agent and application method thereof

The invention relates to a magnetic flocculating agent applied to the field of sewage treatment. The magnetic flocculating agent consists of ferroferric oxide magnetic powder, gamma-amino acid propyl triethoxy silane and glutaraldehyde. The ferroferric oxide magnetic powder surface of the prepared magnetic flocculating agent is coated with an organic functional film in a chemical monomolecular layer coating mode, and the magnetic flocculating agent removes pollutants by utilizing absorption, agglomeration, coprecipitation and other effects of functional groups and the pollutants. Fish protein is recovered by utilizing the magnetic flocculating agent, the protein recovery rate can be improved, recovered materials do not contain chemical agents, the used magnetic flocculating agent can be recycled, and operation cost is saved. The magnetic flocculating agent can be widely applied to treatment of inorganic waste water containing phosphorus, heavy metal ions and the like and treatment of high-turbidity organic waste water with suspended matter of enterprises in the industries of papermaking, food processing, cultivation, petrochemical engineering and the like.
Owner:河南汇思原环保科技有限公司

Nano magnetic cationic flocculant and preparation method thereof

The invention relates to a nano magnetic cationic flocculant and a preparation method thereof, and is applied to the field of sewage and sludge treatment. The nano magnetic cationic flocculant is prepared by the following steps: carrying out graft copolymerization and cationization on gelatinized starch, building an electrolytic tank, carrying out a co-precipitation reaction to generate nano Fe3O4particles, and finally combining the starch graft with the magnetic fluid. The nano magnetic cationic flocculant prepared by the invention has good adsorption and flocculation effects on suspended matter in sewage and sludge, the flocculation sedimentation speed can be accelerated through action of an external magnetic field, and recycling of the flocculating agent in later stage is also facilitated. The nano magnetic flocculant is suitable for treating sewage and sludge of enterprises in papermaking industry, petrochemical industry and the like.
Owner:UNIV OF SHANGHAI FOR SCI & TECH

High-efficiency sewage treating agent

The invention discloses a high-efficiency sewage treating agent which comprises the following components in parts by weight: 15-80 parts of polysilicate aluminum ferric, 8-25 parts of active aluminum oxide, 8-18 parts of bleaching powder, 1-12 parts of organic phosphonium salt scale inhibitor, 2-10 parts of organic corrosion inhibitor and 2-12 parts of acetic acid. The high-efficiency sewage treating agent comprises a flocculant, an adsorbent, a bactericide, a scale inhibitor, a corrosion inhibitor and an antiscaling agent, and can comprehensively treat water. Compared with the prior art, the high-efficiency sewage treating agent has the advantages of wide treatment range, obviously higher removal ratio, favorable treatment effect, high removal ratio of suspended substances (up to 90% above), low raw material price, wide sources, low consumption, low cost and no toxicity or harm, and is easy to store; and the high-efficiency sewage treating agent is easy for sludge dewatering: since the material is unique, the floccule is compact, the precipitation speed is high, and the generated sludge can be easily dewatered.
Owner:WUXI EPIC TECH

Composite coagulant used for treating printing and dyeing waste water and preparing method thereof

The invention relates to a preparing method of a composite coagulant used for treating printing and dyeing waste water.The method comprises the steps that an industrial by-product waste hydrochloric acid and aluminum profile industry aluminum-containing waste residues are added into a reaction kettle sequentially, stirring is carried out in a heat-preserving mode at normal pressure, and aluminum residue water with AlCl3 as an effective ingredient is obtained; a liquid heavy metal capture agent is put into the aluminum residue water, stirring is carried out, and plate-frame pressure filtration is carried out to obtain faint yellow clear aluminum-containing liquid; industrial-grade CaCl2 is put into the aluminum-containing liquid, and stirring is carried out; the stirring reaction is carried out in a heat-preserving mode at the normal pressure, and supernatant liquid subjected to natural sedimentation is the liquid composite coagulant.The preparing method has the advantages that the preparation technology of the composite coagulant is simple, the raw materials are wide in source, and cost is low; the product performance is stable, the added amount of chemical is small, floc is compact, and the sedimentation speed is high; the composite coagulant has good decoloration performance and a high COD removal rate, and the actual printing and dyeing waste water chroma removing rate and the COD removal rate can be 10-15% higher than those of PAC sold in the market.
Owner:CHANGZHOU WUJIN YOUBANG WATER PURIFICATION MATERIALS

Mixed type foundry waste sand wet reclamation wastewater processing method

ActiveCN103351065ASolve the disadvantages of being difficult to effectively dehydrateGuaranteed uptimeMultistage water/sewage treatmentWater useFoundry
The invention provides a mixed type foundry waste sand wet reclamation wastewater processing method. Firstly, wastewater is demulsified, and large suspended matters in the wastewater are flocculated in a spiral flocculating tank by virtue of an inorganic flocculating agent; then small suspended matters are flocculated by virtue of an organic flocculating agent; through standing sedimentation in an inclined tube sedimentation tank, a flocculation layer forming at the bottom in a condensed manner is extracted through a sludge pump at the bottom of the sedimentation tank; the organic flocculating agent is secondarily used, and finally, a band type concentration-vacuum-filter pressing all-in-one machine is used for treatment, so that the water content of sludge discharged at an outlet of a filter cake of the band type concentration-vacuum-filter pressing all-in-one machine is less than 40%; therefore, supernate overflowing from the inclined tube sedimentation tank and clear water from a clear water outlet of the band type concentration-vacuum-filter pressing all-in-one machine can achieve the requirement for production cycle water and the standard for direct discharge.
Owner:广西兰科资源再生利用有限公司

Complex coagulant for advanced treatment of biochemical tail water, and its preparation method and application

The invention discloses a complex coagulant for advanced treatment of biochemical tail water, and its preparation method and application. The complex coagulant is characterized in that the complex coagulant is an inorganic polymer complex coagulant prepared form industrial waste or nonmetallic mineral materials as main materials under heating conditions through the processes of alkaline hydrolysis, acid leaching oxidation, hydrolyzation and polymerization; and the complex coagulant prepared by the preparation method contains 20 to 35% of silicon, 15 to 25% of aluminum, 6 to 11% of iron and 3 to 6% of boron. Compared with the prior arts, the preparation method has the advantages of easy acquirement of raw materials, simple process, and good economical efficiency and applicability. The inorganic polymer complex coagulant prepared by the preparation method has the advantages of good performances of adsorption and bridging, charge neutrality, bonding and gathering, and decoloration, big flocs, fast sedimentation velocity of flocs, and low use amount. The complex coagulant can be widely utilized for the field of wastewater treatment, and is especially suitable for advanced treatment ofbiochemical tail water.
Owner:CHINA PETROLEUM & CHEM CORP +1

Polymer emulsion for polymer-containing sewage treatment and preparation method thereof

InactiveCN101831028AFast separationSolve the problems existing in the treatment of poly-containing sewageWaste water treatment from quariesWater contaminantsKeroseneOxygen
The invention relates to a polymer emulsion for polymer-containing sewage treatment, which is used for processing oil field sewage and a preparation method thereof. The polymer emulsion can have strong adsorptive capacity on colloidal particles and oil droplets in sewage so that the oil droplets are inverted and rapidly copolymerized. Acrylamide and acryloyloxy ethyl trimethyl ammonium chloride are adopted as cationic monomers, fatty alcohol-polyoxyethylene ethers MOA-3 and MOA-9 are adopted as emulsifying agents, tasteless kerosene is adopted as a continuous phase, water is adopted as a dispersed phase and 2,2'-azodissobutyl amidinodihydrochloride is adopted as an initiating agent; and the solid content of the obtained emulsion is 40-50 percent, the cationic degree of a polymer is 50-70 percent, and the characteristic viscosity number of the polymer is 1,026-1,378ml / g. The preparation method comprises the steps of: adding the raw materials into a reactor and stirring to form emulsion; and raising the temperature and introducing nitrogen for removing oxygen, and adding the initiating agent to react at constant temperature for five hours to obtain the polymer emulsion. The emulsion for treating polymer-containing sewage has the advantages of less medicament dosage, high oil and water separating speed, compact flocculating body, obvious water purifying effect, and the like, and can be used for treating the polymer-containing sewage of an oil field.
Owner:SOUTHWEST PETROLEUM UNIV

Heavy metal chelating trapping sulfide agent hexasulfoguanidinoformic acid or salt thereof, and preparation method and application thereof

The invention discloses a heavy metal chelating trapping sulfide agent, and a preparation method and an application thereof. The heavy metal chelating trapping sulfide agent is hexasulfoguanidinoformic acid having a structure represented by formula I, or a water-soluble salt thereof. The preparation method of the heavy metal chelating trapping sulfide agent comprises the following steps: reacting an aqueous solution of guanidine hydrochloride or guanidine nitrate with an excess amount of an alkali to generate free guanidine, reacting the free guanidine with carbon disulfide under the action of a proper amount of an inorganic phosphate to obtain a heavy metal chelating trapping sulfide agent hexasulfoguanidinoformate, and adding a proper amount of an acid for neutralization to obtain hexasulfoguanidinoformic acid. The heavy metal chelating trapping sulfide agent can be used for removing or trapping heavy metal ions in water, and forms a heavy metal sulfide precipitate having a network structure together with the heavy metal ions in water through a chelating effect, so the relative molecular mass of a chelate is improved, the settling time is shortened, and the stability of the chelate formed by the agent and the heavy metals is increased. The formula I is shown in the specification.
Owner:NANJING NORMAL UNIVERSITY

Harvesting method of selenium-enriched chlorella product via diatomite-based positively charged green flocculant

The invention provides a harvesting method of a selenium-enriched chlorella product via a diatomite-based positively charged green flocculant. The method is characterized by comprising the following steps: cultivating chlorella pyrenoidosa in a culture solution containing selenite, so that chlorella liquid undergoing selenium-enriched culture is obtained; and adding the diatomite-based positivelycharged green flocculant to the chlorella liquid undergoing selenium-enriched culture, standing by, discarding supernatant liquid and harvesting the selenium-enriched chlorella. According to the method, by harvesting and cultivating the selenium-enriched chlorella, the finished product that an organic selenium content reaches 73% or above can be obtained, and the method is simple in culture steps,low in cost and convenient to operate. In addition, the selenium-enriched chlorella product that the algae flocculant which is free from toxins and harm is adopted is simple in preparation method, green-going and free from pollution, and a chlorella harvesting rate can reach 90-97%. The method is applicable to large-scale production; and moreover, the obtained product is applicable to the fieldsof food health care and medicine, and a certain economic value is created.
Owner:DONGHUA UNIV

Water purifying agent for rapid treatment of industrial wastewater and preparation method thereof

The invention relates to a water purifying agent for rapid treatment of industrial wastewater and a preparation method thereof, wherein the water purifying agent comprises the following components inparts by weight: 20-35 parts of a nano diatomite powder / cellulose composite material, 5-10 parts of alkyl glycoside or derivative surfactant thereof, 60-75 parts of a flocculating agent and 2-6 partsof nitrifying bacteria. The water purifying agent prepared by the invention is simple in components and reasonable in proportion, does not contain heavy metal components in the formula, is mostly a natural compound, is an environment-friendly water purifying agent, and avoids secondary pollution to a water body; cellulose and diatomite powder are subjected to nanocrystallization and compounding, have huge specific surface area, can adsorb a large number of polluting organic matters, are fully mixed with specific contents of raw material components, and have the effects of rapid sedimentation,decolorization and COD removal; and alkyl glycoside or derivatives thereof are added, so that the water purifying agent has sterilization and disinfection effects on the water body, can effectively kill bacteria and microorganisms in the water body, and avoids water body pollution caused by mass propagation.
Owner:江苏建霖环保科技有限公司

Water treatment filler and preparation method thereof

The invention discloses a water treatment filler and a preparation method thereof. The water treatment filler includes an embedding carrier and an embedding content. The embedding carrier comprises 20-30 parts of montmorillonite, 90-110 parts of garbage burning fly ash, 15-25 parts of carbon fiber beams, 3-5 parts of gelatin, 5-8 parts of modified chitosan, and 20-30 parts of agricultural and forestry waste. The embedding content comprises 5-8 parts of vitamin E, 7-9 parts of lysine, 3-5 parts of 6-benzyladenine, 15-18 parts of iron, 15-17 parts of zinc, 5-8 parts of manganese, 6-7 parts of cobalt, and 20-30 parts of glucose. Anaerobic fermentation is carried out on the agriculture and forestry waste to obtain a fermentation product. The raw materials are added into the fermentation product for roasting to obtain the carrier. The embedding carrier and the embedding content are coated to obtain the water treatment filler. The filler of the invention can meet the requirements of good biocompatibility, large specific surface area and difficult blocking.
Owner:JILIN JIANZHU UNIVERSITY

High-performance polymeric aluminium and preparation method thereof

The invention discloses high-performance polymeric aluminium. The high-performance polymeric aluminium is prepared from the following main raw materials in parts by weight: 40-50 parts of modified polymeric aluminium, 15-20 parts of sodium chlorate, 10-16 parts of industrial salt, 6-9 parts of zinc chloride, 20-30 parts of 36% industrial hydrochloric acid, 10-15 parts of sodium silicate, 80-100 parts of ammonia-free distilled water and 18-25 parts of a NaHCO3 solution; and the invention further discloses a preparation method of the high-performance polymeric aluminium. According to the invention, the modified polymeric aluminium is used as a main body, and is copolymerized with the zinc chloride and polysilicic acid in a preparation process, so that a polymer combining aluminium salt, magnesium salt and zinc salt is obtained; and the sodium chlorate and the industrial salt are added, so that the high-performance polymeric aluminium is obtained; when the high-performance polymeric aluminium is used in a wastewater treatment process, the sedimentation speed of wastes is faster; the algae removal effect is good; flocs are large and dense; the sedimentation speed is fast; the adding amount is low; the cost can be effectively reduced; and therefore, the high-performance polymeric aluminium has a great significance for guaranteeing the water supply quality quality and lowering waterproduction cost.
Owner:江苏蓝遥净水剂有限公司

Water purifying agent for treatment process of polymer-containing sewage pipeline of offshore oil field and application of water purifying agent

The invention discloses a water purifying agent for a treatment process of a polymer-containing sewage pipeline mixer of an offshore oil field and application of the water purifying agent. The water purifying agent comprises the following components by weight percent: 15.0%-20.0% of poly-silicate aluminum ferrum (PSAF), 10.0%-15.0% of poly-aluminum chloride (PAC), 5.0%-10.0% of poly-dimethyl diallyl ammonium chloride (PDA with a molecular weight of 4*10<5>g / mol-5*10<5>g / mol), 0.5%-1.0% of sodium carboxymethyl starch (CMS) and the balance of deionized water. The preparation method comprises the steps of adding poly-aluminum chloride, poly-silicate aluminum ferrum and sodium carboxymethyl starch into water, after the components are completely dissolved, adding poly-dimethyl diallyl ammonium chloride, uniformly stirring at the rotation speed of 100rpm-150rpm, so as to obtain the water purifying agent. The water purifying agent has the characteristics that flocs are compact, are rapidly formed and are high in settling velocity, a water body is strong in adaptability, effects of removing suspended solids and oil are good, the polymer-containing sewage with high content of oil field suspended solids can be effectively treated, and the reaction speed is suitable for the enhanced coagulation treatment process of the pipeline mixture.
Owner:CNOOC TIANJIN CHEM RES & DESIGN INST +1

Polymer emulsion for polymer-containing sewage treatment and preparation method thereof

InactiveCN101831028BFast separationSolve the problems existing in the treatment of poly-containing sewageWaste water treatment from quariesWater contaminantsKeroseneOxygen
The invention relates to a polymer emulsion for polymer-containing sewage treatment, which is used for processing oil field sewage and a preparation method thereof. The polymer emulsion can have strong adsorptive capacity on colloidal particles and oil droplets in sewage so that the oil droplets are inverted and rapidly copolymerized. Acrylamide and acryloyloxy ethyl trimethyl ammonium chloride are adopted as cationic monomers, fatty alcohol-polyoxyethylene ethers MOA-3 and MOA-9 are adopted as emulsifying agents, tasteless kerosene is adopted as a continuous phase, water is adopted as a dispersed phase and 2,2'-azodissobutyl amidinodihydrochloride is adopted as an initiating agent; and the solid content of the obtained emulsion is 40-50 percent, the cationic degree of a polymer is 50-70 percent, and the characteristic viscosity number of the polymer is 1,026-1,378ml / g. The preparation method comprises the steps of: adding the raw materials into a reactor and stirring to form emulsion; and raising the temperature and introducing nitrogen for removing oxygen, and adding the initiating agent to react at constant temperature for five hours to obtain the polymer emulsion. The emulsionfor treating polymer-containing sewage has the advantages of less medicament dosage, high oil and water separating speed, compact flocculating body, obvious water purifying effect, and the like, and can be used for treating the polymer-containing sewage of an oil field.
Owner:SOUTHWEST PETROLEUM UNIV

Composite coagulant for advanced treatment of biochemical tail water, as well as preparation method and application thereof

The invention relates to a composite coagulant for advanced treatment of biochemical tail water, as well as a preparation method and application thereof. The inorganic polymer composite coagulant containing boron, silicon, aluminum and iron, which is prepared by adopting an iron source, a boron source and a silicon-aluminum source as raw materials, is applied to coagulation purification processing coagulant of all kinds of waste water, and is particularly applied to advanced treatment of the biochemical tail water. The iron source, the boron source and the silicon-aluminum source are adopted as the raw materials; the inorganic polymer composite coagulant is prepared through alkaline hydrolysis, acid leaching oxidation, hydrolysis and polymerization under heating; and the prepared composite coagulant contains 20 percent-35 percent of silicon, 15 percent-25 percent of aluminum, 6 percent-11 percent of iron, and 3 percent-6 percent of boron. The coagulant has easy-to-get raw materials and concise process, and is economic and applicable. The obtained inorganic polymer composite coagulant has good capacities of absorption and bridging, charge neutrality, bonding aggregation and decoloration, and less dosage, and is widely applied to waste water treatment field, in particular to advanced treatment of the biochemical tail water; and the flocs are big and are fast in sedimentation velocity.
Owner:CHINA PETROLEUM & CHEM CORP +1

Composite flocculating agent for treating oil sand deposit tailings, and treating method for cured fine tailings

The invention provides a composite flocculating agent for treating oil sand deposit tailings, and a treating method for cured fine tailings. The composite flocculating agent comprises 30-70% of polyacrylamide, 5-30% of poly(dimethyldiallyl ammonium chloride), 2-20% of a calcium-containing material and 1-20% of an adsorbent, wherein the calcium-containing material is one or more selected from the group consisting of calcium carbonate and calcium oxide, and the adsorbent is one or more selected from the group consisting of diatomite and activated carbon. The composite flocculating agent has a rapid sedimentation speed; after solid-liquid separation, liquid supernatant is clear, the content of suspended matters is low, and turbidity is small; flocs formed after flocculation are dense, and thesolid content of bottom mud is high; and the composite flocculating agent has good temperature adaptability. The composite flocculating agent has good solubility, and can be directly added as dry powder in virtue of an appropriate dosing device, thereby eliminating a flocculating agent dissolving device and reducing investment. The composite flocculating agent of the invention can be used for treating cured fine tailings; and the composite flocculating agent can also be used for secondary dewatering of bottom mud, and after the composite flocculating agent is added into the bottom mud, capillary suction time is short, yield stress is moderate, and a dehydration rate is high.
Owner:CHINA SPECIAL EQUIP INSPECTION & RES INST

Compound and efficient flocculating agent, preparation method and application thereof

The invention relates to a compound and efficient flocculating agent. The flocculating agent comprises the following materials in percent by volume: 45 to 47 percent of a ferrous sulfate solution, 18to 20 percent of industrial sulphuric acid, and 33 to 35 percent of an aluminum chloride solution, wherein the mass concentration of the ferrous sulfate solution is 25 to 30 percent; the mass concentration of the aluminum chloride solution is 5 to 8 percent. The flocculating agent is brown yellow to yellow brown, the density is within a range of 1.2 to 1.45g / mL, and the pH of a solution is 2.2 to2.6 after the flocculating agent is diluted for 100 times. The flocculating agent can be applied to a deep treatment unit for pharmaceutical and chemical wastewater subjected to biochemical treatment,has the purpose of removing insoluble COD in wastewater, and has the advantages that the removal effect is good, discharged water is clear, formed alum floc is dense, and the settling velocity is high.
Owner:华夏碧水环保科技股份有限公司

A kind of composite iron salt coagulant and its preparation method and application

The invention relates to a composite iron salt coagulating agent, which is prepared from the following components in parts by weight: 100 parts of iron-containing waste hydrochloric acid, 10 to 30 parts of aluminum-containing sludge, 1 to 5 parts of silicic acid and 0.4 to 2 parts of sodium chlorate. A preparation method comprises the following steps of adding the iron-containing waste hydrochloric acid into a reaction kettle, adding the sodium chlorate into the reaction kettle, and agitating an obtained mixture for reaction; adding the aluminum-containing sludge into the reaction kettle, and agitating a newly obtained mixture for reaction; dropwise adding the silicic acid into the reaction kettle, and agitating a finally obtained mixture for reaction, to obtain the composite iron salt coagulating agent. The composite iron salt coagulating agent has the beneficial effects that (1), the composite coagulating agent is simple in preparation process, wide in sources of raw materials and low in cost; (2), the product performance is stable, the dosage of an agent is less, and a flocculating constituent is compact and is further quick in sedimentation rate; (3), the composite iron salt coagulating agent has favorable decoloration performance and a higher COD (Chemical Oxygen Demand) removal rate, and is wider in pH (potential of hydrogen) serviceable range.
Owner:CHANGZHOU WUJIN YOUBANG WATER PURIFICATION MATERIALS

Polyaluminum silicate-acrylamide copolymer composite flocculant and preparation method thereof

The invention discloses a polyaluminum silicate iron-acrylamide copolymer composite flocculant and a preparation method thereof, which is characterized in that 20 parts of Na2SiO3 are added to 250 parts of deionized water, the pH value is 2 to 5, and the reaction is carried out at room temperature for 2 to 3 hours. Prepare activated silicic acid; use aluminum-containing waste, iron-containing waste hydrochloric acid and industrial hydrochloric acid to obtain mixed crystals of AlCl3 and FeCl2; add 1.2 to 25.0 parts of mixed crystals to 25 parts of activated silicic acid, react, stand and mature, and obtain poly Aluminum iron silicate PAFSI; add 20 parts of acrylamide, 75-450 parts of deionized water, 5-20 parts of ionic monomer, and 0.3-6 parts of macromonomer into the reaction bottle, stir, pH value 5-9, pass N2 , add 0.008-0.4 parts of potassium persulfate at 40-70°C, react for 12-36 hours, and prepare the copolymer PAME; add 100 parts of 5 g / L PAME solution into the reaction bottle, and add 12-350 parts under rapid stirring 100 g / L PAFSI solution, pH value 1-4, react at 30-40°C for 2-3 hours, then react at 50-75°C for 2-4 hours, and mature for 24 hours to prepare PAFSI-PAME composite flocculant.
Owner:CHENGDU UNIVERSITY OF TECHNOLOGY
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