The invention discloses a preparation method and low-temperature application of a Te-doped
tungsten niobium oxide /
molybdenum niobium oxide heterojunction, and belongs to the technical field of secondary batteries. The preparation method specifically comprises the following steps: carrying out high-energy ball milling and alloying on WO3, Nb2O5 and Te2O5 to obtain amorphous Te-doped
tungsten niobium oxide; the preparation method comprises the following steps: carrying out high-energy ball milling and alloying on MoO3, Nb2O5 and Te2O5 to obtain amorphous Te doped
molybdenum niobium oxide; uniformly mixing and compacting the amorphous Te doped
tungsten niobium oxide and the amorphous Te doped
molybdenum niobium oxide, and performing
discharge plasma sintering in an
inert atmosphere to obtain the
ceramic crystal Te doped tungsten niobium oxide / molybdenum niobium oxide
heterojunction material. The Te-doped tungsten niobium oxide / molybdenum niobium oxide two-phase
heterojunction material designed by the invention is relatively short in synthesis time, the
synthesis period is shortened, the size of
crystal grains is convenient to regulate and control, the
crystallinity of the material is very good, the
diffusion rate of
lithium ions is greatly promoted by a heterojunction interface, the
electron conductivity is improved by cooperating with Te
doping, and the performance of the Te-doped tungsten niobium oxide / molybdenum niobium oxide two-phase heterojunction material is improved. The material can be used as a
lithium ion negative
electrode material with
fast charging characteristic and good low-temperature performance.