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30results about How to "Reduce the degree of decomposition" patented technology

Device for continuously destructing radiative waste organic solvent

The invention belongs to the technical field of the spent fuel reprocessing and discloses a device for continuously destructing a radiative waste organic solvent. The device comprises a constant-temperature tank and an electrochemical oxidation destruction container located in the constant-temperature tank; the container is mainly composed of an anode chamber, a cathode chamber and a clarifying chamber; the radiative waste organic solvent goes into the clarifying chamber by use of a waste organic solvent feeding pipe; when the solvent is higher than a separator between the clarifying chamber and the anode chamber, the solvent goes into the anode chamber. The non-destructed waste organic solvent is mixed with water into a mixed solution which goes into the clarifying chamber by use of a liquid flow channel between the anode chamber and the clarifying chamber, the separation of the organic phase and the water phase is realized in the clarifying chamber, and the water phase located below contains redionuclides and is charged by use of a water phase drainage pipe at a certain rate; besides, the organic phase located at top is mixed with the waste organic solvent added by use of the waste organic solvent feeding pipe and then the mixture flows into the anode chamber by use of the upper channel of the separator. The device is capable of meeting the requirements on improving the current effectively and realizing continuous destruction of waste organic solvents.
Owner:CHINA INSTITUTE OF ATOMIC ENERGY

Determination method for OCPs in environmental sample

The invention discloses a determination method for OCPs in an environmental sample, which belongs to the field of detection of OCPs. The determination method comprises the following steps: carrying out Soxhlet extraction on a to-be-determined environmental sample so as to obtain a liquid extract containing OCPs; carrying out separation and purification, i.e., concentrating the liquid extract to a constant volume, adding an aqueous solution of tetrabutyl ammonium sulfite and isopropanol, carrying out oscillation until a solid residue is generated after repeated shaking every time, discarding a lower layer, retaining an organic phase, washing the organic phase, removing water by using anhydrous sodium sulfate, carrying out purification by using a Florisil column so as to obtain an eluate, concentrating the eluate to a constant volume and dividing the concentrated eluate into two groups which are used as samples for subsequent detection, wherein one of the groups is a sample of OCPs stable in sulfuric acid and is purified by using a sulfuric acid silica gel column so as to obtain a purified sample, and the other of the groups is a sample of OCPs instable in sulfuric acid and is purified by using an Envi-carb SPE small column so as to obtain a purified sample; and carrying out determination, i.e., respectively analyzing and determining the two groups of purified samples by using an HRGC-HRMS apparatus so as to obtain determination results of the content of OCPs in the two groups of purified samples. The determination method provided by the invention enables accuracy and sensitivity of determination to be improved.
Owner:CSD IDEA BEIJING INST OF ENVIRONMENTAL INNOVATION

Pleurotus eryngii cultivation material containing pleurotus eryngii residues and preparation method thereof

The invention discloses a pleurotus eryngii cultivation material containing pleurotus eryngii residues and a preparation method thereof, and belongs to the field of edible fungus cultivation materials and preparation methods thereof. The cultivation material is prepared from the following raw materials in parts by mass: 55.0-65.0 parts of a fermented main material, 8.0-12.0 parts of soybean meal, 6.0-9.0 parts of corn meal, 18.0-22.0 parts of wheat bran, 1.0-3.0 parts of lime and 1.0-3.0 parts of light calcium carbonate. The fermented main material is mainly prepared by mixing and fermenting bagasse, mushroom residues, corncobs and saw dust in a mass ratio of 1 to 1.1 to 2 to 2. The preparation method comprises the following steps: A, cleaning pleurotus eryngii residues; B, screening the pleurotus eryngii residues; C, prewetting; D, mixing, composting and fermenting the bagasse, residues, corncobs and saw dust; E, turning; F, screening the mixed material; and E, adding the soybean meal, corn meal and other auxiliaries. According to the cultivation material, the raw material cost can be remarkably reduced, and the cultivated pleurotus eryngii has the advantages of high yield, high quality, small budding amount, low pollution and improved biological efficiency.
Owner:HUNAN YUXIU BIOLOGICAL TECHN

Method for preparing nafcillin acid

The invention discloses a method for preparing nafcillin acid. The method includes the following steps: 1) performing chlorination on 2-ethyoxyl naphthoic acid and excessive thionyl chloride to obtain acyl chloride liquid, steaming in a decompression mode to remove thionyl chloride, and dissolving the residue through dichloromethane to obtain solution A; 2) adding triethylamine and dichloromethane in 6-aminopenicillanic acid, and stirring until the solution is clear to obtain solution B; 3) dropwise adding the solution A into the solution B to perform condensation reaction, and preserving the temperature for 30-90mins to react after the dropwise adding is finished to obtain solution C; 4) adding buffer agent into the solution C to obtain solution D; and 5) acidizing the solution D to separate an organic layer, washing, drying, steaming in a decompression mode to remove dichloromethane, and performing recrystallization on the obtained solid through alcohols solvents to obtain the nafcillin acid. The method for preparing the nafcillin acid is easy and simple to operate, simple in aftertreatment and high in yield.
Owner:GUILIN PHARMA

Household ozone generator

The invention discloses a household ozone generator, and belongs to the technical field of ozone generators. The household ozone generator comprises an outer frame, the left side surface of the outerframe is fixedly connected with the right side surface of a support frame, the lower surface of the inner wall of the support frame is fixedly connected with the lower surface of a first water tank, the right side surface of the first water tank communicates with the left end of a filter, and the filter is clamped on the left side surface of the inner wall of the outer frame. According to the household ozone generator, the first water tank, a water inlet pipe, a water outlet pipe, a first connecting pipe, a second connecting pipe, a water injection frame, the outer frame and the supporting frame are arranged, so that the flow velocity of air around the first water tank is increased, and then water flow in the water injection frame takes away heat on the surface of an electrolysis ozone generator main body. According to the device, the cooling process of water flow on the electrolysis ozone generator main body can be realized while water is added for electrolysis to prepare ozone, the probability of temperature rise is reduced, the degree of ozone decomposition caused by heat in the working process can be reduced to a certain extent, and the ideal ozone preparation efficiency of thedevice is ensured.
Owner:常州市艾诺电子科技有限公司

Medicinal preparation and preparation method and application thereof

The invention relates to the field of medicaments, and particularly relates to a medicinal preparation and a preparation method and application thereof. The medicinal preparation is prepared from benzoyl peroxide with specific particle size distribution, and when the medicinal preparation is prepared into a mixed preparation together with clindamycin phosphate, the stability of the medicinal preparation can be sufficiently improved, the decomposing degree of two effective components, namely, benzoyl peroxide and clindamycin phosphate, is greatly reduced, and the problem of poor stability of apreparation with the two effective components, namely, benzoyl peroxide and clindamycin phosphate, in long-term storage is solved. The preparation method of the medicinal preparation is simple in process, convenient in operation, short in production cycle, and suitable for large-scale industrialized production. The medicinal preparation disclosed by the invention is applicable to preparation of external medicaments, preferably applicable to preparation of a medicine for treating acne, can effectively inhibit the decomposition of two effective components, namely benzoyl peroxide and clindamycinphosphate, can be stably stored for a long time and can keep efficacy for a long time.
Owner:SHANGHAI MEDICILON INC

A device for continuously destroying radioactive waste organic solvents

The invention belongs to the technical field of the spent fuel reprocessing and discloses a device for continuously destructing a radiative waste organic solvent. The device comprises a constant-temperature tank and an electrochemical oxidation destruction container located in the constant-temperature tank; the container is mainly composed of an anode chamber, a cathode chamber and a clarifying chamber; the radiative waste organic solvent goes into the clarifying chamber by use of a waste organic solvent feeding pipe; when the solvent is higher than a separator between the clarifying chamber and the anode chamber, the solvent goes into the anode chamber. The non-destructed waste organic solvent is mixed with water into a mixed solution which goes into the clarifying chamber by use of a liquid flow channel between the anode chamber and the clarifying chamber, the separation of the organic phase and the water phase is realized in the clarifying chamber, and the water phase located below contains redionuclides and is charged by use of a water phase drainage pipe at a certain rate; besides, the organic phase located at top is mixed with the waste organic solvent added by use of the waste organic solvent feeding pipe and then the mixture flows into the anode chamber by use of the upper channel of the separator. The device is capable of meeting the requirements on improving the current effectively and realizing continuous destruction of waste organic solvents.
Owner:CHINA INSTITUTE OF ATOMIC ENERGY

A kind of polypropylene consumables for 3D printing and preparation method thereof

The invention relates to the technical field of polymer materials, in particular to a polypropylene consumable for 3D printing and a preparation method thereof. The polypropylene consumables for 3D printing of the present invention are composed of polypropylene, thermoplastic elastomer, talcum powder masterbatch, maleic anhydride grafted polypropylene, antioxidant, lubricant, hyperdispersant and color masterbatch. In the present invention, thermoplastic elastomer is added to polypropylene to increase the toughness of the composite material; talcum powder masterbatch is added to reduce product cost and crystallization and shrinkage of matrix resin, and improve the forming precision of 3D printing; adding maleic anhydride grafted polypropylene to improve matrix resin The binding force with talcum powder; adding compound antioxidants can reduce the aging and decomposition of materials during the extrusion process, prolong the service life of the product, and interact with each auxiliary material to reduce shrinkage and improve anti-aging ability at the same time The result is that the obtained polypropylene consumables for 3D printing are not easy to crystallize, have good toughness, small shrinkage after molding, and strong anti-aging ability.
Owner:GUIZHOU AEROSPACE TIANMA ELECTRICAL TECH

Determination method for OCPs in environmental sample

The invention discloses a determination method for OCPs in an environmental sample, which belongs to the field of detection of OCPs. The determination method comprises the following steps: carrying out Soxhlet extraction on a to-be-determined environmental sample so as to obtain a liquid extract containing OCPs; carrying out separation and purification, i.e., concentrating the liquid extract to a constant volume, adding an aqueous solution of tetrabutyl ammonium sulfite and isopropanol, carrying out oscillation until a solid residue is generated after repeated shaking every time, discarding a lower layer, retaining an organic phase, washing the organic phase, removing water by using anhydrous sodium sulfate, carrying out purification by using a Florisil column so as to obtain an eluate, concentrating the eluate to a constant volume and dividing the concentrated eluate into two groups which are used as samples for subsequent detection, wherein one of the groups is a sample of OCPs stable in sulfuric acid and is purified by using a sulfuric acid silica gel column so as to obtain a purified sample, and the other of the groups is a sample of OCPs instable in sulfuric acid and is purified by using an Envi-carb SPE small column so as to obtain a purified sample; and carrying out determination, i.e., respectively analyzing and determining the two groups of purified samples by using an HRGC-HRMS apparatus so as to obtain determination results of the content of OCPs in the two groups of purified samples. The determination method provided by the invention enables accuracy and sensitivity of determination to be improved.
Owner:CSD IDEA BEIJING INST OF ENVIRONMENTAL INNOVATION
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