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41results about How to "Regulation uniformity" patented technology

New method for preparing nanometer-structure composite ultra-filtration membrane

The invention discloses a new method for preparing a nanometer-structure composite ultra-filtration membrane. According to the new method, in the prior art, the defect that the interception adsorption performance of an electro-spinning fiber membrane is low is overcome. The new method in the technical scheme includes the following steps that (1) polymer materials are dissolved in a solvent to be prepared into an electrostatic spinning solution for preparing a fiber membrane, and the fiber membrane serves as a base layer of the composite membrane; (2) a hydrophilic polymer is dissolved in the solvent, then a plasticizer and a pore-forming agent are added into the mixture, the mixture is heated, dissolved, subjected to standing and defoamed, a coating solution is formed, and the base layer is coated with the coating solution; (3) when the coating solution is gelatinous, porous functional materials are evenly sprayed and pressed to the surface of the base layer with the air-spraying-pressing method. The nanometer-structure composite membrane is prepared with the soaking-pore-opening method, and using of a traditional chemical cross-linking agent is avoided; the new method is simple in preparing process, and has the high adsorption capacity for organic pollutants, heavy metal ions and the like.
Owner:CHANGZHOU UNIV

Titanium dioxide-metal organic framework array with uniformly and continuously coated nuclear-sheath structure, and preparation method and application of titanium dioxide-metal organic framework array

The invention discloses a titanium dioxide-metal organic framework array with a uniformly and continuously coated nuclear-sheath structure, and a preparation method and application of the titanium dioxide-metal organic framework array. The titanium dioxide-metal organic framework array is provided with the uniformly and continuously coated core-sheath structure, wherein titanium dioxide is used asa core, and a metal organic framework is used as a sheath layer; the titanium dioxide is titanium dioxide nanowires, and the metal organic framework is a Ti-based bdc-(NH2)x, wherein the x is 0, 1 or2. The number of amino groups in the titanium dioxide-metal organic framework array can be regulated and controlled, and the thickness and uniformity of the metal organic framework which is used as the sheath layer can also be regulated and controlled. Performance of the array structure can be changed through the regulation and control of the thickness and uniformity of the metal organic framework which is used as the sheath layer, and through the regulation and control of the number of amino groups contained in ligands in the metal organic framework which is used as the sheath layer, the change of performance of the metal organic framework can be influenced by regulating the visible light absorption capacity of the metal organic framework.
Owner:FUJIAN INST OF RES ON THE STRUCTURE OF MATTER CHINESE ACAD OF SCI

Strontium titanate-titanium dioxide composite nanotube array film and preparation method and application thereof

The invention relates to a strontium titanate-titanium dioxide composite nanotube array film and a preparation method and application thereof. The film is obtained through direct growth on a conductive glass substrate with a three-step hydrothermal method; hydrothermal synthesis of titanium dioxide nanorods is carried out in the first step, the titanium dioxide nanorods are etched to generate titanium dioxide nanotubes in the second step of hydrothermal treatment, strontium hydroxide serves as a strontium source in the third step of hydrothermal reaction, and finally the composite film with perovskite type strontium titanate nanoparticles uniformly distributed on the surface of the titanium dioxide nanotube array is obtained, wherein the titanium dioxide nanotubes are vertically arrayed on the conductive glass substrate. The composite film can serve as an anode material of solar cells or serve as a photocatalyst for degradation treatment of photolysis water or organic matter. The three-step hydrothermal method is adopted for in-situ synthesis, the preparation process and needed equipment are simple, the controllability is high, and production is safe, free of toxin and environmentally friendly; by assembling the film into solar cells, the sunlight capturing capability of photoanodes can be improved, and the photoelectric conversion efficiency can be improved.
Owner:QINGDAO UNIV OF SCI & TECH

Flexible polyimide foam and preparation method and applications thereof

ActiveCN109593199AProtection against excessive volatilizationUniform pore sizeFoaming agentMicrometer
The present invention relates to flexible polyimide foam and a preparation method and applications thereof. The flexible polyimide foam is obtained by foaming a block/plate-shaped polyimide foam precursor containing slow-release components of a foaming agent; and the flexible polyimide foam has the average density of 14.7-47.7 kg/m<3> and the pore size of 130-530 micrometers. The flexible polyimide foam disclosed by the invention has the beneficial effects that by adopting a foaming form of a polyimide (PI) precursor block/plate, the problem of large density deviation in the thickness direction, of a polyimide precursor powder foaming method, can be effectively solved and the product yield of the foam made from the prepolymerized powder is improved; by adopting the PI precursor containingthe slow-release components and by regulating and controlling the type and the using amount of the slow-release components of the foaming agent, the density of the PI flexible foam can be adjusted andcontrolled, so that the foaming process window is wider and the pore size of the foam is more uniform; and meanwhile, by adopting the polyimide precursor plate, the water absorption rate can be effectively reduced and the storage time of the material is prolonged in the preservation process, so that the quality stability of the final foam product is improved.
Owner:INST OF CHEM CHINESE ACAD OF SCI

Preparing method and application of cobalt tantalum zirconium alloy target material

The invention discloses a preparing method and application of a cobalt tantalum zirconium alloy target material, and belongs to the technical field of preparation of special materials. The preparing method comprises the steps of component design, high-vacuum vertical sintering and high-vacuum electron beam melting, three-dimensional isothermal hot forging cogging, angle-varying controlled rollingand the like. In this way, the organization structure of the alloy and the performance of the target material are controlled, and the high-quality cobalt tantalum zirconium alloy target material is prepared. The oxygen content of the cobalt tantalum zirconium alloy target material is smaller than or equal to 15 ppm, the average grain size of the cobalt tantalum zirconium alloy target material is 5-20 micrometers, the phase distribution of the target material is uniform, the magnetic permeability is larger than 40%, and the heterogeneity of magnetic permeability is smaller than 2%. By means ofthe designed process, the oxygen content, organization structure heterogeneity and magnetic performance of the finished product target material can be effectively controlled, and a raw material guarantee is provided for sputtering high-quality thin films by means of the preparing method.
Owner:CENT SOUTH UNIV

A kind of soft polyimide foam, its preparation method and its application

ActiveCN109593199BSolve the problem of large thickness control deviationUniform pore sizeImidePolymer science
The present invention relates to flexible polyimide foam and a preparation method and applications thereof. The flexible polyimide foam is obtained by foaming a block / plate-shaped polyimide foam precursor containing slow-release components of a foaming agent; and the flexible polyimide foam has the average density of 14.7-47.7 kg / m<3> and the pore size of 130-530 micrometers. The flexible polyimide foam disclosed by the invention has the beneficial effects that by adopting a foaming form of a polyimide (PI) precursor block / plate, the problem of large density deviation in the thickness direction, of a polyimide precursor powder foaming method, can be effectively solved and the product yield of the foam made from the prepolymerized powder is improved; by adopting the PI precursor containingthe slow-release components and by regulating and controlling the type and the using amount of the slow-release components of the foaming agent, the density of the PI flexible foam can be adjusted andcontrolled, so that the foaming process window is wider and the pore size of the foam is more uniform; and meanwhile, by adopting the polyimide precursor plate, the water absorption rate can be effectively reduced and the storage time of the material is prolonged in the preservation process, so that the quality stability of the final foam product is improved.
Owner:INST OF CHEM CHINESE ACAD OF SCI

Zinc layer trivalent chromium iridescent passivation treating fluid used under normal temperature and usage method thereof

The invention relates to the technical field of metal surface passivating treatment, in particular to a zinc layer trivalent chromium iridescent passivation treating fluid used under normal temperature and a usage method thereof. Based on calculation per liter, the zinc layer trivalent chromium iridescent passivation treating fluid consists of 15-20g of chromium trichloride, 5-10g of sodium nitrate, 8-15g of propane diacid, 15-20g of citric acid, 5-10g of sodium dihydrogen phosphate, 8-15g of thiourea, 0.8-1.5g of ferrous sulfate, 0.6-1.0g of cerium sulfate and the balance of deionized water.Under a continuous stirring condition, the chromium trichloride is dissolved in a part of the deionized water, the sodium nitrate, the propane diacid, the citric acid, the sodium dihydrogen phosphateand the thiourea are sequentially added and fully dissolved, the cerium sulfate is added and stirred to completely dissolve, the ferrous sulfate and the remaining deionized water are added, and the zinc layer trivalent chromium iridescent passivation treating fluid is obtained after standing. The zinc layer trivalent chromium iridescent passivation treating fluid has the characteristics of being capable of performing normal temperature treatment, simple and convenient, easy to control, stable and the like, and a colored passive film bright, uniform and compact, and good in corrosion resistancecan be obtained by passivating an encapsulated galvanized sample under the condition that PH (potential of hydrogen) value is 2.2 in a laboratory.
Owner:NORTHEASTERN UNIV

A kind of preparation method of nanostructure composite ultrafiltration membrane

The invention discloses a new method for preparing a nanometer-structure composite ultra-filtration membrane. According to the new method, in the prior art, the defect that the interception adsorption performance of an electro-spinning fiber membrane is low is overcome. The new method in the technical scheme includes the following steps that (1) polymer materials are dissolved in a solvent to be prepared into an electrostatic spinning solution for preparing a fiber membrane, and the fiber membrane serves as a base layer of the composite membrane; (2) a hydrophilic polymer is dissolved in the solvent, then a plasticizer and a pore-forming agent are added into the mixture, the mixture is heated, dissolved, subjected to standing and defoamed, a coating solution is formed, and the base layer is coated with the coating solution; (3) when the coating solution is gelatinous, porous functional materials are evenly sprayed and pressed to the surface of the base layer with the air-spraying-pressing method. The nanometer-structure composite membrane is prepared with the soaking-pore-opening method, and using of a traditional chemical cross-linking agent is avoided; the new method is simple in preparing process, and has the high adsorption capacity for organic pollutants, heavy metal ions and the like.
Owner:CHANGZHOU UNIV

Roll type strip filamentation system

The invention provides a roll-type strip filamentation system. The roll-type strip filamentation system is characterized by comprising a feeding trolley for transferring strip rolls; the unwinding machine is connected with the feeding trolley in a matched mode and controls the strip coil to unwind the strip; the threading mechanism is connected with the unreeling machine in a matched mode and controls threading of the strip; the traction mechanism is connected with the threading mechanism in a matched mode and controls the strip to move; the moisture regaining and/or feeding mechanism is used for regaining moisture and feeding the front and back surfaces of the strip during traction; the fixed-width slitting mechanism is connected with the traction mechanism in a matched mode and controls the strips to be slit into tows in a fixed-width mode; the tow gathering mechanism is connected with the fixed-width slitting mechanism in a matched mode and controls gathering of the fixed-width slitting tows; the fixed-length slitting mechanism is connected with the tow gathering mechanism in a matched mode and controls the tows to be slit into tow sections in a fixed-length mode. Double-sided moisture regaining and/or feeding, fixed-width slitting, tow gathering and fixed-length slitting into tow sections with the width of 0.5 mm are completed, and the filling rate and sensory quality of cigarettes are improved.
Owner:云南烟草机械有限责任公司 +1

Nano tungsten powder doped with metal oxide nanoparticles and preparation method thereof

The invention discloses a method for preparing nano-tungsten powder doped with metal oxide nanoparticles. The method comprises: 1. dispersing tungsten trioxide or blue tungsten and drying to obtain pretreated tungsten source powder; 2. oxidizing the metal The ultrafine / nano-droplets obtained by ultrasonic atomization of the aqueous solution of the precursor salt of the substance are sprayed on the pretreated tungsten source powder to obtain the doped tungsten source powder; 3. The doped tungsten source powder is mixed with carbon nanoparticles and then heated and kept warm The pre-reduction powder is obtained; 4. The pre-reduction powder is reduced by hydrogen to obtain nano-tungsten powder doped with metal oxide nanoparticles; the invention also discloses the nano-tungsten powder doped with metal oxide nanoparticles prepared by the above method. In the present invention, carbon nanoparticles and doped metal oxide nanoparticles are used respectively to increase the nucleation rate of the corresponding reduction products, refine the particle size of the corresponding reduction products, and realize the control of the particle size of the metal oxide nanoparticles and tungsten powder , to obtain nano-tungsten powder uniformly doped with metal oxide nanoparticles.
Owner:西安稀有金属材料研究院有限公司
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