33results about How to "Improve the distillation effect" patented technology

The utility model relates to the technical field of oleic acid distillation devices, in particular to a distillation device for oleic acid production, which comprises a distillation device body, a material receiving box is mounted at the bottom of the distillation device body, an exhaust pipe is mounted on the right side of the top of the distillation device body, and a fixing pipe is mounted on the upper side of the inner wall of the exhaust pipe. An exhaust plate is mounted at the bottom end of the fixed pipe, and a fixed column is mounted at the top of the exhaust plate; the distillation device has the beneficial effects that the screw rod is driven to rotate by rotating the knob, so that the moving plate is driven to downwards extrude the spring to increase the pressure when the piston moves upwards, after adjustment is completed, when the internal pressure of the distillation device reaches a preset value, the piston is pushed to move upwards and extrude the spring, and after the internal pressure is released below the preset value, the spring pushes the piston to reset; and the exhaust plate and the exhaust hole of the fixed pipe are blocked, so that the pressure released by the exhaust pipe can be adjusted, excessive pressure release is prevented, the distillation effect of oleic acid is improved, and the use effect of the distillation device is improved.

The utility model discloses a rectification extraction device capable of improving the quality of propylene glycol, which belongs to the technical field of rectification and is characterized in that propylene glycol steam generated at high temperature is introduced into a preheating tank and is conveyed upwards along a spiral preheating structure to transfer heat to a mixed solution containing propylene glycol, which is conveyed downwards by the preheating structure, so that the quality of propylene glycol is improved. According to the multi-stage rectification device, the temperature of mixed liquid primarily entering the first rectification tower is effectively increased, propylene glycol steam after being cooled is guided into the second rectification tower to be subjected to secondary rectification after being cooled by the condenser, and the rectification effect is effectively improved through multi-stage rectification, in addition, a stirring barrel matched with a stirring shaft is additionally arranged in the first rectification tower, and the rectification efficiency is improved. Waste liquid in the second rectifying tower is guided into the stirring barrel through the second discharging pipe and mixed with preheated mixed liquid, on one hand, the waste liquid with waste heat is used for conducting secondary preheating on the mixed liquid, on the other hand, the stirring structure is additionally arranged, the heating uniformity of the mixed liquid is improved, and the heating effect is enhanced.

A dioxolame rectification device capable of efficiently removing heavy metal ions comprises a tower body, a tower base is arranged at the bottom of the tower body, a feeding port is formed in one side of the tower body, and a heavy metal ion discharging port is formed in the bottom of the tower body; the feeding hole is communicated with a feeding pipe, a spraying disc is mounted at the lower end of the feeding pipe, and the spraying disc is fixed with the tower body through a height adjusting mechanism; a condenser is arranged at the upper end of one side of the tower body, and a dioxolame discharge port is formed in the lower end of the condenser; and a reboiler is arranged at the lower end of one side of the tower body. The spraying disc is designed, so that liquid in the spraying disc can be uniformly sprayed, the feeding distribution is more uniform, and the rectification effect is improved; meanwhile, the spraying disc can be adjusted through the height adjusting mechanism and can be adjusted according to actual requirements, so that the optimal spraying effect is achieved. According to the device disclosed by the utility model, effective separation of dioxolame and heavy metal ions in a mixture and purification of dioxolame can be realized.

The present invention relates to a method for recovering organic solvents and alkaline earth metal chloride salts in aramid production waste liquid, belongs to the technical field of waste liquid treatment / recovery process, and solves at least one of the problems that the existing treatment / recovery process will cause secondary pollution, high energy consumption, and inability to simultaneously recover alkaline earth metal chloride salts. The present invention provides a method for recovering organic solvents and alkaline earth metal chloride salts in aramid production waste liquid: the recovery method includes three process sections, which are flocculation precipitation process section, azeotropic distillation process section, and "distillation + evaporation crystallization" process section, and finally obtains pure high-concentration organic solvent and alkaline earth metal chloride salt crystals. The recovery method provided by the present invention can realize the efficient recovery of organic solvents and alkaline earth metal chloride salts in aramid production waste liquid. Taking the DMAC-CaCl2 waste liquid system as an example, the recovery rate of DMAC can reach 98.3%, the recovery rate of CaCl2 can reach 94.5%, and the purity of DMAC is ≧99.99%.

The present invention discloses a device and method for extracting plant essence for cosmetics, and belongs to the field of plant essence extraction. A device for extracting plant essence for cosmetics includes an extraction tank, and also includes: a distillation plate fixed at the lower part of the inner wall of the extraction tank, on which a distillation part for providing steam to the inside of the extraction tank is arranged; wherein a cutting shaft is rotatably connected to the top of the inner cavity of the extraction tank; the present invention drives the cutting blade to rotate in the cutting barrel through the cutting shaft to achieve crushing and cutting of plant raw materials, which is convenient for the essence liquid inside to flow out and for subsequent comprehensive and thorough extraction; and the cutting shaft also drives the scraping plate to rotate, so that the reciprocating screw rod and the sliding block and stirring brush that reciprocate thereon turn over the plant raw materials accumulated on the surface of the distillation plate, so that it can be more comprehensively contacted with high-temperature water vapor, effectively improving the distillation effect, and realizing the extraction of essence liquid efficiently and comprehensively.

The utility model discloses a negative pressure methyl silicone oil rectifying still which comprises a working table, the surface of the working table is rotatably connected with a still body in a penetrating mode, the outer surface of the still body is fixedly connected with a fixed gear ring, and the lower surface of the working table is connected with a movable rack meshed with the fixed gear ring in a sliding mode. According to the utility model, the threaded rod is rotated, so that the threaded block drives the lifting pipe to ascend, the water spraying holes are exposed from adaptive ports, then the water suction pump is started, the water suction pump pumps clean water into the lifting pipe, then the clean water is sprayed out through the plurality of water spraying holes to wash the inner wall of the kettle body, and meanwhile, the servo motor is started; an output shaft of the servo motor drives a rotating gear to rotate, so that a mounting gear ring drives a rotating pipe, and the rotating pipe drives a lifting pipe to rotate, so that rotary flushing is performed, and the flushing effect is improved.

The utility model relates to acetic acid rectification energy -conserving separation device technical field, and disclose acetic acid rectification energy -conserving separation device, including rectifying tank, the right side of rectifying tank places the heat preservation box, the outer wall of rectifying tank is penetrated respectively with air inlet pipe and pressure reducing pipe, the one end of air inlet pipe is equipped with igniter in rectifying tank inside, the top of rectifying tank is penetrated respectively with feeding pipe and reflux tube. This acetic acid rectification energy -conserving separation device, through setting up rectifying tank, pressure reducing pipe, gas pipe, reflux tube, heat preservation layer, solenoid pressure reducing valve structure, make the device in the operation process, high temperature and high pressure air will be through the opening of solenoid pressure reducing valve and be arranged into the heat preservation interlayer, thereby guarantee the safety of the device in the operation process, and in the subsequent heating process, high temperature and high pressure air in the heat preservation interlayer is directly arranged into rectifying tank through reflux tube again, to this reduces the combustion and use of carbon monoxide, and further improves the energy -conserving effect of the device.

The application provides a metal organic framework rectification filler, a preparation method and application thereof in treatment of deuterium-containing wastewater and tritium-containing wastewater, and belongs to the field of chemical industry. The application is based on metal organic framework materials (MOFs), excellent MOF materials are synthesized by selection of metal centers and organic ligands, and the MOF materials are applied to the treatment process of deuterium-containing wastewater and tritium-containing wastewater in a granulation mode; meanwhile, due to the unique crystal properties of the MOF materials, the MOF materials are endowed with unique separation properties, and the theoretical plate number can be effectively improved. The application introduces the metal organic framework materials into the field of tritium-containing wastewater rectification, thereby expanding the material types in the field, and providing a brand-new vision and method for research and development of a new tritium-containing wastewater filler.

The invention belongs to the technical field of electric power image-text large models, and discloses an electric power image-text large model device and a hierarchical deployment method thereof. The electric power image-text large model device comprises an edge model used for being deployed on an edge device and a cloud model used for being deployed on a cloud. The edge model comprises a post-distillation visual coding layer obtained after knowledge distillation is carried out on a visual coding layer of the original electric power image-text large model, and a head layer added to the post-distillation visual coding layer; the cloud model comprises a text coding layer and a modal interaction layer in the original electric power image-text large model. According to the technical scheme, the potential of a cloud large model can be further exerted, and the recognition capability of complex scenes is improved; besides, the calculation complexity of the model can be reduced, and the core performance can be ensured, so that the model can be efficiently deployed and operated on edge equipment with limited calculation capability, and a series of technical problems caused by frequent data transmission can be solved.

The utility model belongs to the technical field of liquid oxygen production, and particularly relates to liquid oxygen preparation distillation equipment which comprises a distillation box, a feeding hole formed in the top of the distillation box, a motor fixedly mounted at the top of the distillation box, a rotating rod arranged at one end of the motor, a stirring rod fixedly mounted on the rotating rod, and a heating pipe fixedly mounted on the inner wall of the distillation box, a temperature sensor is fixedly mounted on the inner wall of the distillation box, a first collecting mechanism is arranged on one side of the distillation box, a second collecting mechanism is arranged on the other side of the distillation box, and a thermal insulation layer is arranged on the inner wall of the distillation box. According to the device disclosed by the utility model, the motor, the rotating rod and the stirring rod are matched for use, and the rotating rod can be rotated to drive the stirring rod to rotate by driving the motor to work, so that liquid air in the device can be heated more sufficiently and uniformly, and the distillation effect can be improved; the internal temperature can be conveniently detected in real time, and liquid gas with different boiling points can be conveniently distilled.

The device comprises a distillation barrel with an open top, a barrel cover is arranged at the top of the distillation barrel, a tray is erected in the distillation barrel, a vertical rod is arranged in the distillation barrel, the tray comprises an inner ring and an outer ring, an elastic net is arranged between the inner ring and the outer ring, the inner ring sleeves the outer side of the vertical rod, the vertical rod can move downwards, and the inner ring can move downwards along with the vertical rod; a limiting structure is arranged on the inner side wall of the distillation barrel, the bottom of the outer ring abuts against the limiting structure, and the limiting structure can prevent the outer ring from moving downwards. The area of the tray can be increased in the wine steaming process, so that the contact between steam and fermented grains is increased, and the distillation effect of tail wine is improved.

The present invention belongs to the technical field of agricultural detection equipment, especially an agricultural detection equipment, and the following scheme is proposed, including a bottom plate and a cooling cover, the top outer wall of the bottom plate is fixedly connected to a motor, and the output shaft of the motor is fixedly connected to a rotating shaft through a coupling, the outer wall of the rotating shaft near the top is fixedly connected to a fixing frame, the outer wall of the fixing frame is fixedly connected to a storage cylinder, and the outer wall of the storage cylinder near the bottom is provided with a connecting hole. The present invention is provided with a juice extraction component, when the agricultural detection equipment is used, the pulp is placed in the juice extraction cylinder, and the hydraulic cylinder is adjusted to drive the cutting blade to move downward, so as to cut the pulp placed in the juice extraction cylinder into multiple parts, and then the hydraulic rod is adjusted to drive the squeezing plate to squeeze and juice the pulp on each part, and the squeezing sheet on the squeezing plate performs secondary cutting on the pulp. This juicing method improves the juice extraction rate of each pulp and at the same time improves the efficiency of single juicing.

The utility model belongs to the technical field of alpha-acetyl-gamma-butyrolactone production equipment, and particularly relates to alpha-acetyl-gamma-butyrolactone rectification equipment which comprises a tower body, a feed pipe fixedly connected to the top of the outer wall of the tower body, a discharge pipe fixedly connected to the bottom of the outer wall of the tower body, an air inlet pipe fixedly connected to the top of the tower body, and an air outlet pipe fixedly connected to the bottom of the outer wall of the tower body. A reheater is installed at the water outlet end of the discharging pipe, an air injection assembly is installed between the tower body and the reheater, an installation hole is formed in the top of the tower body, an air inlet pipe is installed in the installation hole, a condenser is fixedly installed at the top of the air inlet pipe, a backflow assembly is installed between the tower body and the condenser, and a plurality of tower plates are installed in the tower body. The four tower plates are sequentially distributed in a staggered mode, baffles are fixedly connected to the tops of the tower plates, and the air injection assembly comprises a first air pipe and a second air pipe. According to the utility model, the heat of steam is fully utilized to vaporize the solvent on each layer of tower plate, and the refluxed condensate can be uniformly sprayed to the top of each tower plate, so that the rectification effect is improved.

The present invention discloses a method for data set distillation and lightweighting using GAN prior enhancement in depth, including: sending the initialized mean noise into the GAN network to obtain a hidden code; converting the hidden code into a real picture through the GAN network; calculating the distillation loss of the generated data set and the real data set according to the combination of the real pictures; optimizing the hidden code through an optimizer, and selecting a preset hidden code according to the calculated feature distance; evaluating all data sets generated using the preset hidden code of the intermediate layer, and selecting the data set that meets the conditions as the solution. The present invention uses a layer-by-layer search of the intermediate layer space of GAN, realizes the optimization of the generated data set using the multi-level guidance information of GAN, and automatically selects the generated data set corresponding to the optimal layer as the result, thereby improving the performance of data set distillation.

The present application relates to a kind of for aromatic hydrocarbon combined plant adsorption separation unit extract partition wall rectification system, including partition wall rectification tower, toluene separation flow path, p-xylene separation flow path and p-diethylbenzene separation flow path;Partition wall rectification tower includes the partition wall being arranged in tower interior, one end of partition wall is fixed in tower bottom, the other end of partition wall extends upwards and is kept a certain distance from tower top, and partition wall separates the space in tower interior into first separation chamber and second separation chamber being arranged left and right, and common rectification chamber being located above partition wall, first separation chamber, second separation chamber and common rectification chamber are in fluid communication;Toluene separation flow path is connected with the top of common rectification chamber;P-diethylbenzene separation flow path is connected with the bottom of first separation chamber;P-xylene separation flow path is connected with the bottom of second separation chamber.Compared with double-tower rectification process, investment is greatly reduced, tower top gas cooling load is less, system waste heat is fully recycled, energy consumption and cost are reduced, and economic benefit is generated.

This invention relates to a method for predicting the thermal storage performance of materials based on multi-source domain knowledge distillation. First, the crystal structure of a first sample is obtained, and its thermal storage performance parameters are calculated using first-principles calculations to construct a target dataset. Second, the crystal structure and various readily available physicochemical properties of a second sample are searched, and multiple source domain pre-training datasets are constructed by grouping according to different parameters. Next, isomorphic second models are trained using each source domain dataset, with each model predicting one physicochemical property parameter, and its second intermediate layer feature representation is extracted. Then, a first model with the same structure as the first sample is trained to predict the thermal storage performance parameters, and knowledge distillation is introduced during training: the intermediate layer features of each second model are fused using learnable weighted methods to generate reference features. The difference between these reference features and the first intermediate layer features of the first model is calculated, and the model is optimized by combining the error of the predicted values. Finally, the crystal structure of the sample to be predicted is input into the trained first model to obtain the predicted thermal storage performance parameters. This method is suitable for small-sample scenarios with limited thermal storage performance label data and can provide rational guidance for the design of thermal storage materials.

The utility model discloses a plant active ingredient steam distillation device which comprises a distillation cylinder and an electric heating wire arranged on the inner wall of the bottom end, a discharging box is arranged in the distillation cylinder, a closing cover is rotatably arranged at the upper end of the discharging box, and a fastening knob is arranged on one side of the upper end of the closing cover. A turning structure is arranged on one side of the distillation cylinder and comprises a motor, a storage groove is formed in the side, close to the motor, of the discharging box, a connecting block is arranged in the storage groove, a connecting piece is installed at the output end of the motor, and the connecting piece is connected with the turning structure. The connecting piece enters the clamping groove in one side of the connecting block. According to the plant active ingredient steam distillation device, two ends of a plant can be distilled, and the effects of turning over the plant and accelerating distillation are achieved.

The present invention belongs to the technical field of bamboo wood pyrolysis, and particularly relates to a bamboo vinegar preparation distillation apparatus, which comprises: a distillation kettle, which is provided with a material inlet, a thermometer and a liquid level meter; the condensation mechanism is arranged at the top of the distillation kettle and is communicated with the interior of the distillation kettle; the main heating device is arranged at the bottom of the distillation kettle; the liquid discharge pipe is arranged at the bottom of the distillation kettle, and a precipitation cavity is formed in the bottom of the liquid discharge pipe; the circulating pipe is arranged on one side of the distillation kettle, one end of the circulating pipe is communicated with the interior of the distillation kettle, the other end of the circulating pipe is communicated with the liquid discharging pipe, and a gas-liquid pump is arranged on the circulating pipe in series; the ozone generation unit is connected with the gas-liquid pump; the auxiliary heating device is arranged on the distillation kettle and is used for assisting in heating the bamboo vinegar; compared with the prior art, the bamboo vinegar distillation device has the advantages that industrial production is facilitated, and the bamboo vinegar distillation efficiency and production efficiency are improved.

The present application relates to wastewater distillation technical field, especially to a kind of chemical raw material intermediate wastewater distillation equipment and distillation method thereof.It includes primary distillation unit and condensing unit, the bottom of the primary distillation unit is connected with secondary distillation unit, the primary distillation unit includes distillation ball of spherical structure, first rotating rod is rotatably connected in the distillation ball, the periphery of the first rotating rod is annular array distribution with several groups of first scraping mechanism;The secondary distillation unit includes distillation kettle with hemispherical structure at bottom.The present application carries out secondary distillation in the form of hierarchical intensity, not only save energy consumption, but also improve distillation effect and harmful substance separation effect.At the same time, distillation ball and distillation kettle are respectively set as spherical and hemispherical, reduce bottom area, reduce precipitation probability, and use first scraping mechanism and second scraping mechanism to respectively stir and scrape wall of the inner wall of both, also reduce the residue of waste residue.

The utility model relates to the technical field of distillation equipment, and discloses distillation equipment for a degreasing agent, which comprises a distillation retort and a cooling box, a filtering mechanism is arranged on the right side of the upper surface of the distillation retort, a stirring mechanism is arranged in the distillation retort, and the right side of the upper surface of the distillation retort is communicated with a conveying pipe. The end, away from the distillation retort, of the conveying pipe communicates with the upper surface of the cooling box, and the right side of the input pipe communicates with a spiral condensation pipe. According to the distillation equipment for the degreasing agent, the distillation equipment can be opened from the outer side of the top end of the feeding barrel by twisting a sealing cover, then materials needing to be distilled can be poured into the feeding barrel, the distilled materials flow into the filtering barrel, impurities in the distilled materials can be filtered through a filtering net fixed in the filtering barrel, and the filtering effect is good. The filtered distillation material flows into the distillation retort, and impurities stay in the filter cartridge, so that the impurities in the distilled material can be filtered, and the distillation efficiency is improved.

The present invention relates to the technical field of ethane recovery and natural gas liquefaction, and specifically to a method for multi-stage separation of ethane recovery and co-production of large-volume liquefied natural gas. The natural gas liquefaction process and the ethane recovery process are independent of each other, and two independent refrigeration systems are used, first ethane recovery is performed, and then natural gas liquefaction is performed, and energy consumption accounts for a large proportion. In view of the above problems, the present invention provides a method for multi-stage separation of ethane recovery and co-production of large-volume liquefied natural gas, which includes a multi-stage separation ethane recovery unit, a liquefied natural gas unit, a mixed refrigerant refrigeration cycle unit and a propane refrigeration cycle unit. The natural gas liquefaction process and the ethane recovery process, the mixed refrigerant refrigeration cycle unit and the propane refrigeration cycle unit share a set of device systems, which can realize ethane recovery and natural gas liquefaction. The mixed refrigerant refrigeration cycle unit and the propane refrigeration cycle unit are used in combination, which can reduce investment and operation and maintenance costs, and can also improve the adaptability of the device to the processing volume and gas quality, so as to realize the resource integration and benefit maximization of the upstream and downstream of the oil and gas field natural gas processing.

The invention discloses a preparation method of tetracyclododecene, which comprises the following steps: mixing crude dicyclopentadiene, a norbornene solution and ethylene as raw materials, carrying out Diels-Alder reaction, and carrying out three-section rectification on the generated product to obtain a high-purity tetracyclododecene product and a heavy oil byproduct. Compared with the prior art, the method has the advantages that the dicyclopentadiene with the impurity content of less than or equal to 15% can be used as a raw material, so that high-purity dicyclopentadiene does not need to be purchased or crude dicyclopentadiene does not need to be refined. In addition, three-section rectification is used in the rectification section, so that the cost and the energy consumption can be effectively reduced.

The utility model belongs to the technical field of high-softening-point resin production, and particularly relates to a distillation device for high-softening-point resin production, which comprises an operation table and supporting columns, the supporting columns are fixedly mounted at four corners of the bottom surface of the operation table, and supporting bases are fixedly mounted on the bottom surfaces of the supporting columns. A distillation device is arranged on the upper surface of the operation table and comprises a steam generation unit, a distillation stirring unit, a condensation unit and a collection unit, the steam generation unit comprises a steam generator and a steam conveying pipe, and the steam generator is fixedly installed on one side of the upper surface of the operation table; and the steam conveying pipe is fixedly mounted on the upper surface of the steam generator. According to the distillation device for high-softening-point resin production, by arranging the stirring shaft and the stirring rods, raw materials can be stirred during distillation, distillation is accelerated, the distillation effect is improved, and meanwhile the connecting rods drive the scraping plates to rotate to scrape the raw materials attached to the inner wall of the distillation retort so that the raw materials can better participate in distillation.

The utility model provides a methacrylic acid distillation device, which belongs to the field of methacrylic acid distillation and comprises a distillation tower, the distillation tower is divided into an upper cavity and a lower cavity, a heating component is connected in the cavity at the bottom of the distillation tower, and the heating component is used for distilling methacrylic acid; a collecting mechanism is arranged in the chamber at the top of the distillation tower and is used for collecting a methacrylic acid solution; the collecting mechanism comprises a top plate arranged at the top of the distillation tower, a water tank is formed in the bottom of the top plate, the bottom of the water tank is connected with a gas circulating pipe, and the gas circulating pipe is used for guiding out the gasified methacrylic acid material; according to the utility model, the distillation tower is connected with the collecting mechanism, so that gasified methacrylic acid can be cooled and collected in time, and steam loss and insufficient condensation are avoided.

The invention provides a production method for recovering glacial acetic acid through negative pressure distillation, and belongs to the technical field of glacial acetic acid recovery. The method comprises the following steps of: preheating dilute acetic acid obtained by a reaction in a previous working section in a preheater, feeding the preheated dilute acetic acid into a concentration tower, injecting butyl acetate into the concentration tower, concentrating, feeding the concentrated acetic acid into a distillation tower, distilling, feeding a distilled gas phase into a condenser through heat exchange, and condensing to obtain liquid acetic acid, and transferring into a receiving tank to obtain crude acetic acid. By changing the positive pressure of the distillation system into the negative pressure for production, online switching and distillation online cleaning are realized, the distillation effect of the distillation tower is improved, the steam consumption is reduced, the resistance of the concentration system is reduced, the acid content in wastewater is reduced, the wastewater amount of system cleaning is reduced, the operation period of the concentration tower is prolonged, and the production cost is reduced. Therefore, the effects of saving energy, reducing emission and reducing consumption are achieved.

This utility model relates to the field of evaporation equipment technology, specifically to an evaporation device for the distillation process of R-(+)tetrahydrofuran carboxylic acid. The device includes an inner wall of an evaporation sleeve, an evaporation sleeve jacket, a discharge assembly, an upper end cap, a stirring shaft, a stirring shaft mounting assembly, a stirring blade assembly, a feed pipe, a feed sleeve flange, a dispersion disc, a discharge pipe, a thermometer sleeve, a sight glass, a condenser assembly, and a receiving vessel assembly. The feed pipe controls the amount of material entering the distillation device via a valve. After the material is fed into the inner wall of the evaporation sleeve, it is evenly dispersed by the dispersion disc. Utilizing the motor, stirring shaft, and stirring blade assembly, the material forms a film on the inner wall of the evaporation sleeve during the stirring process. The rapidly vaporized material is condensed in the condenser and then received in the receiving vessel, thus improving the distillation effect and preventing localized overheating of the material, which could lead to quality problems.

The utility model relates to the technical field of hydrogenation reaction, and discloses a hydrogenation device which comprises a feeding end, a feeding heat exchange mechanism, a de-heavy tower, a reflux mechanism and a discharging end which are connected in sequence, the feeding end and the backflow mechanism are each provided with a polymerization inhibitor injection port. The device has the following technical effects: 1, the reflux mechanism is arranged between the heavy component removal tower and the discharge end, so that part of materials rectified by the heavy component removal tower can be conveyed back into the heavy component removal tower through the reflux mechanism to be rectified again, the yield of light components is improved, and the quality of finished products is improved; and 2, a polymerization inhibitor injection port is arranged at the feeding end and the reflux mechanism, and a polymerization inhibitor is added into a material to be rectified, so that the colloid content of light components is effectively reduced, the yield of finished products is improved, the service life of a hydrogenation device is prolonged, and the maintenance cost is reduced.

The utility model provides a glass-lined distillation kettle with high distillation efficiency, which relates to the technical field of distillation kettles and comprises a distillation kettle body, a top cover is arranged at the top end of the distillation kettle body, and a filtering and stirring mechanism is arranged at the top end of the top cover; the filtering and stirring mechanism comprises a rack, a motor is fixedly mounted at the top end of the rack, a first rotating rod is arranged on an output shaft of the motor, a driving wheel is arranged on the outer surface wall of the first rotating rod, a second rotating rod is rotationally connected to the top end of the top cover, a driven wheel is arranged on the outer surface wall of the second rotating rod, and belts are arranged on the outer surface walls of the driving wheel and the driven wheel; an output shaft of the second rotating rod penetrates through the top cover to be fixedly provided with a filter cartridge, the filter cartridge can filter impurity solid particles in the mixed liquid, in order to improve the filtering rate of the filter cartridge, a motor is started to drive the first rotating rod to rotate, and the first rotating rod drives the filter cartridge to rotate through a belt; centrifugal force is generated in the rotating process of the filter cartridge, so that the filtering speed of the mixed liquid is increased.

This invention provides a distillation system for degassing carboxylated styrene-butadiene latex, comprising a polymerization kettle, a distillation column, a condenser, a buffer tank, a mixed-phase feed pump, a conditioning tank, and a vibrating screen. The outlet of the polymerization kettle is connected to the inlet on the side wall of the distillation column. The vapor phase outlet of the distillation column is sequentially connected to the inlet of the polymerization kettle via the condenser, the buffer tank, and the mixed-phase feed pump. The liquid phase outlet of the distillation column is connected to the inlet of the conditioning tank, and the outlet of the conditioning tank is connected to the inlet of the vibrating screen. A fractionation device is provided in the distillation column, comprising several trays. Each tray has multiple valve tubes evenly distributed through it, and each valve tube contains a Tesla valve. A sliding float valve structure is provided at the top of each valve tube. This high-efficiency distillation system can effectively disperse the vapor phase during distillation, allowing for more thorough countercurrent contact between the vapor and liquid phases and more complete interphase mass transfer, thereby further improving the distillation effect and efficiency while reducing energy consumption.

The utility model discloses a distillation device for detecting traditional Chinese medicine chemicals, which relates to the technical field of distillation devices, and adopts the technical scheme that the distillation device comprises a box body, a heater is fixedly connected to the inner side of the box body, a distillation flask is movably connected to the outside of the heater, a feed port is fixedly connected to the outside of the distillation flask, and a stirring rod is rotatably connected to the inside of the distillation flask; a first bevel gear is fixedly connected to the exterior of the end, located outside the distillation flask, of the stirring rod, a rotating rod is rotationally connected to the exterior of the box body, a second bevel gear is fixedly connected to the end, close to the first bevel gear, of the rotating rod, the second bevel gear is meshed with the first bevel gear, and an overturning assembly is arranged outside the box body and comprises an L-shaped push plate and a material containing bag; by arranging the motor, the material containing bag is driven to obliquely discharge, the discharge speed is well controlled, the motor drives the stirring rod in the distillation bottle to operate while traditional Chinese medicine chemical medicine powder is poured, and stirring and heating are performed while discharging is performed, so that the powder is quickly dissolved, and the distillation efficiency and effect can be improved.