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113results about How to "Increase extraction rate" patented technology

Method for comprehensively extracting effective ingredients in tea

The invention relates to a method for comprehensively extracting effective ingredients in tea. The method comprises the following steps of: with a faintly acidic water solution as a main extraction solvent and a certain amount of organic solvent as an auxiliary extraction solvent, carrying out step-by-step extraction on water extracts to obtain four effective ingredients, namely tea polyphenol, caffeine, tea polysaccharide and theanine; and meanwhile, extracting tea protein from tea residues by using an alkali dissolution and acid deposition method. According to the method, as water is used as the main solvent, the cost is low, the reactions are mild and active ingredients are favorably preserved; as a certain amount of organic solvent is used as the auxiliary extraction solvent, the problems of overhigh cost and product pollution caused by use of a large amount of organic solvents are solved; meanwhile, five effective ingredients, namely the tea polyphenol, the tea polysaccharide, the caffeine, the theanine and the tea protein are extracted, and therefore high extraction rate, high purity and high utilization rate of tea are achieved; the solvents are recycled in the extraction process, so that the preparation cost is reduced; and no alkali and acid waste liquor is discharged in the overall process, and therefore the method is environment-friendly. The overall preparation flow is high in efficiency and low in cost, and therefore the method has a favorable application value.
Owner:TIANJIN UNIV

Method for extracting oligo proanthocyanidin from grape seeds

The invention provides a method for extracting oligo proanthocyanidin from grape seeds, which comprises the following steps: placing materials in extraction tanks, wherein the extraction solvent is water or water-containing ethanol, the using amount is 3-10 times of the volume of material mass, the temperature is 45-100 DEG C, and the time is 20-60 min; leading the content of active ingredients in extraction liquid in all the tanks to be gradually reduced by sequentially extracting the tanks, carrying out liquid discharge on the extraction liquid with the highest content of the active ingredients in all the tanks, entering into the circulating step, then carrying out residue discharge and material addition on the extraction tank which completes a plurality of times of solvent extraction of materials, adding a new solvent during the last extraction of the materials, then transferring by spacing one unit, carrying out a plurality of times of extraction and discharging liquid. The method can ensure that the materials and the solvents of all the extraction units can always keep the greater concentration difference of the active ingredients, accelerate the extraction rate, improve the concentration of the active ingredients of the final solvent and be characterized by saving the solvents, saving energy and the like under the premise of ensuring the higher extraction rate.
Owner:SUZHOU ZEDAXINGBANG MEDICAL TECH

Method for extracting anthocyanin from nitraria tangutorum peel residues

The invention provides a method for extracting anthocyanin from nitraria tangutorum peel residues. The method comprises the following steps of pretreatment, wherein the nitraria tangutorum peel residues are subjected to vacuum drying and then smashed to obtain nitraria tangutorum peel residue powder; enzymolysis, wherein the nitraria tangutorum peel residue powder and a plant cell wall degrading enzyme are mixed to be treated; extraction, wherein nitraria tangutorum peel residue enzymatic liquid and an organic solvent are mixed, and the mixture is extracted to obtain a crude nitraria tangutorum peel residue extract; purification, wherein the crude nitraria tangutorum peel residue extract is purified by adopting an adsorption chromatography method to obtain the anthocyanin. According to the method, the nitraria tangutorum peel residues are frozen at low temperature, dried through a vacuum drying method and smashed, it is effectively guaranteed that the structure of part of the anthocyanin, being sensitive to temperature, in the nitraria tangutorum peel residues is not destroyed, and therefore the finally obtained anthocyanin is more in compound variety and high in effective ingredient content. The separation efficiency of the method is high, and the anthocyanin prepared through the method is large in mass and high in purity.
Owner:QINGHAI TSINGHUA BIOTRY BIO TECH

Preparation method of natural plant dye

InactiveCN105086505AHas antibacterial and antivirus effectsGood adhesionNatural dyesAnti virusCavitation
The invention provides a preparation method of natural plant dye. The method comprises the first step of cleaning, the second step of mixing, the third step of ultrasonic extraction, the fourth step of distillation and the fifth step of filtration. According to the preparation method of the natural plant dye, by means of multi-frequency ultrasonic extraction operation, the mechanical effect, the cavitation effect and the thermal effect of the dye can be greatly enhanced; compared with single-frequency acoustic extraction, the extraction time can be shortened by 40% to 60%, the extraction temperature can be declined by 15 DEG C to 20 DEG C, damage to natural pigments and effective components caused by the temperature is reduced, therefore, the extraction rate is increased, and the quality is improved; due to the fact that optimum induction frequencies of different plant cells are different, according to the preparation method of the natural plant dye, different frequencies can be appropriately adjusted and combined, coextraction of various plants with similar hues can be achieved, the energy sources are saved, and the efficiency is improved. The prepared plant dye is stronger in adhesion effect and pure and elegant in color, the antibacterial and anti-virus effects are achieved, and the plane dye is safe, harmless, natural and environmentally friendly.
Owner:界首市波菲特服饰有限公司

Process for extracting elemental aluminium by coal gangue acidification

The invention belongs to the technical field of coal gangue extraction equipment, and particularly relates to a process for extracting elemental aluminium by coal gangue acidification. According to the process, through arranging a microwave generator and an ultrasonic generator, through controlling the microwave power to be between 780 and 820W and through setting the microwave generation time tobe 1 hour, an extraction ratio of the elemental aluminium in the coal gangue can reach 95%; an extracting speed of the coal gangue is accelerated through the ultrasonic generator; a coal gangue acidification treatment kiln used in the process comprises a kiln body which is internally provided with a squeezing plate, wherein the squeezing plate is designed in an annular shape; a filter plate is arranged below a drive cabin, a grinding groove is formed in the filter plate and grinding balls are arranged in the grinding groove; four stirring rods are uniformly and fixedly connected to the surfaceof a third airbag; an aeration tank is arranged in push plates; and aeration holes are uniformly formed in the surfaces of the push plates and communicate with the aeration tank. The coal gangue acidification treatment kiln is simple in structure and can sufficiently crush the coal gangue, and in addition, the coal gangue can be evenly stirred and mixed and the acidification rate is high.
Owner:李静娴

Clay mineral loaded nanometer zero valent iron, and preparation method and use thereof

The invention belongs to the technical field of environmental chemistry, and particularly relates to a clay mineral loaded nanometer zero valent iron, and a preparation method and use thereof. According to the clay mineral loaded nanometer zero valent iron, and the preparation method and the use thereof, tobacco stems and walnut green seedcases are used for preparing plant extracts, high toxicityand expensive sodium borohydride is replaced as reducing agents, and the clay mineral loaded nanometer zero valent iron is prepared; at the same time, the fact that the clay mineral loaded nanometer zero valent iron can effectively remove residues of anabasin pesticides in water is found for the first time, and the degradation effect is better than that of clay mineral, nanometer zero valent ironand clay mineral loaded nanometer zero valent iron prepared by conventional methods; and degradation conditions of the anabasin pesticides on the clay minerals loaded nanometer zero valent iron are optimized. According to the clay mineral loaded nanometer zero valent iron, and the preparation method and the use thereof, preparation conditions and the degradation conditions of the clay mineral loaded nanometer zero valent iron are optimized, great significance to diversified utilization of agricultural production wastes, reduction of production costs and reduction of environmental pollution areprovided; and at the same time, the reaction process is simple, and good market prospects in remediation and treatment of anabasine pesticide pollution environments are provided.
Owner:LIUYANG BRANCH OF CHANGSHA COMPANY OF HUNAN TOBACCO +1

Preparation method of edible packaging film based on diatom polysaccharide

The invention discloses a preparation method of an edible packaging film based on diatom polysaccharide. The preparation method specifically comprises the following steps: degreasing diatom powder, concretely adding a chloroform methanol mixed solution into the diatom powder, carrying out degreasing, suction filtration, and drying to obtain degreased diatom powder; preparing the diatom polysaccharide, concretely uniformly mixing the degreased diatom powder with water, then adding 8-chlorotheophylline, and carrying out ultrahigh-pressure extraction and suction filtration, wherein the obtained filtrate is the water extracted crude polysaccharide; and preparing the edible packaging film, concretely taking the following components in parts by weight: the diatom polysaccharide, glycerol, gelatin, tea polyphenol and water, dissolving the components to prepare a film liquid, carrying out degassing, then uniformly pouring the degassed film liquid into a mold, and carrying out drying for forming a film, so as to obtain the edible packaging film. The preparation method disclosed by the invention has the beneficial effects that the preparation method is simple and feasible, the time consumption is low, the energy consumption is low, the utilization rate of the raw materials can be improved, and the degradable pollution-free packaging film with good performance can be formed. The surface of the packaging film is smooth and compact, the film is easy to uncover, and the packaging film is edible, is easy for industrial scale production and has good application value and market potential.
Owner:金华市铁骑士生物科技有限公司

Method used for extracting sea-buckthorn active polypeptides with supersonic wave

The invention discloses a method used for extracting sea-buckthorn active polypeptides with supersonic wave. The method comprises following steps: glucopyranose and galactopyranose are added into sea-buckthorn seeds, and primary crushing and superfine grinding are carried out so as to obtain sea-buckthorn ultra-fine powder; distilled water, cellulase, phytase, and tannase are added into the sea-buckthorn ultra-fine powder, hydrolysis, enzyme deactivation, and centrifugation are carried out, a precipitate is collected, and is dried; distilled water, alkali protease, neutral protease, and left lateral vitamin C are added into sea-buckthorn powder, ultrasonic-assisted extraction and enzyme deactivation are carried out, an obtained enzymatic hydrolysate is cooled, and is subjected to ultrafiltration so as to obtain a sea-buckthorn active polypeptide crude solution; the sea-buckthorn active polypeptide crude solution is introduced into a chromatographic column for elution with double distilled water, an obtained eluate is introduced into a macroporous resin column for elution with double distilled water and an ethanol solution successively, an obtained elution solution is dried so as toobtain the sea-buckthorn active polypeptides. The method is simple and practical; pretreatment time is short; the purity of the sea-buckthorn active polypeptides is high; extraction rate is high; andthe obtained sea-buckthorn active polypeptides possess antibacterial performance and water retention capacity.
Owner:磐安县派普特生物科技有限公司

Method for purifying capsicine in hot pepper

The invention belongs to the field of natural organic chemistry, and relates to a method for purifying capsicine in hot pepper by using microwave countercurrent extraction-membrane filtration technologies in a combined way. The method is characterized in that: microwave countercurrent extraction and membrane filtration are performed in sequence, so that the extraction time is shortened, the extraction speed is increased, the extraction rate is increased by dozens of times, and the extraction period is shortened greatly. Meanwhile, the content of active ingredients is increased, medicinal materials and energy consumption are saved, and the defects of relatively low conventional extraction rate and low extraction purity are overcome. Furthermore, the content of active ingredients is increased, the extraction purity is high, and a final capsicine product of which the content is over 98 percent can be obtained. Due to the adoption of the method for using microwave countercurrent extraction-membrane filtration technologies in a combined way, an organic solvent is extracted completely, the membrane filtration technology is safe and reliable, the microwave technology has a high extraction speed, pollution is avoided, environment-friendly engineering is adopted, a production line has a simple constitution, a processing process is simple and contributes to saving medicinal materials and lowering energy consumption, and the defects of relatively low conventional extraction rate and low extraction purity are overcome.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD

Clay mineral supported nano zero-valent iron as well as preparation method and application thereof

The invention belongs to the technical field of environment chemicals and in particular relates to clay mineral supported nano zero-valent iron as well as a preparation method and application thereof.According to the preparation method, tobacco stems and green walnut peel are adopted to prepare plant extracts to replace sodium borohydride as a reducing agent which is large in toxicity and high inprice in a common preparation method, and thus the clay mineral supported nano zero-valent iron is prepared; meanwhile, the effect that the clay mineral supported nano zero-valent iron is capable ofefficiently removing residues of anabasine pesticides in a water body is found for a first time, and the clay mineral supported nano zero-valent iron has a degradation effect prior to those of a claymineral, nano zero-valent iron and clay mineral supported nano zero-valent iron which is prepared by using a common method; degradation conditions of the clay mineral supported nano zero-valent iron upon the anabasine pesticides are optimized; preparation conditions and degradation conditions of the clay mineral supported nano zero-valent iron are optimized, and great significances are achieved for diversely utilizing agricultural production wastes, lowering the production cost and reducing environment pollution; and meanwhile, the clay mineral supported nano zero-valent iron is simple in reaction process and has very good market prospects in repairing treatment on anabasine pesticide polluted environments.
Owner:LIUYANG BRANCH OF CHANGSHA COMPANY OF HUNAN TOBACCO +1
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