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63results about How to "The method is simple and economical" patented technology

Preparing method for high-activity and high-stability composite catalyst for fuel cells

The invention provides a preparing method for a high-activity and high-stability composite catalyst for fuel cells and belongs to the technical field of fuel cells. The preparing method includes the steps that firstly, the surface of a Pt / C catalyst is wrapped by a layer of dopamine, and the dopamine is used for adsorbing a metal precursor through the good adsorbing performance on metal cations; secondly, silicon dioxide is used for packaging a polymer, the pyrolysis losses and heat treatment morphology conversion of a polymer precursor are controlled through morphology fixing and range limiting functions of the silicon dioxide, alloy nano particles and an N-doped carbon modified layer are further synthesized through high-temperature pyrolysis under the surface segregation effect of platinum and transition metal, and the low-platinum-nonmetal composite structure catalyst with the hollow alloy nano particles wrapped by N-doped carbon is constructed. According to the preparing method for the high-activity and high-stability composite catalyst for the fuel cells, migration agglomerating and growing in the sintering process of the catalyst are overcome, the size of the particles is effectively controlled, the catalyst has high high-activity surface area, operation is simple, industrial production is easy, and the catalyst can be widely applied to the fuel cells with proton exchange membranes serving as electrolytes.
Owner:重庆铈坦新材料技术研究院有限公司

Method for extracting and preparing lignin composite nano fibers in situ

The invention provides a method for extracting and preparing lignin composite nano fibers in situ, which takes natural lignocellulose biomasses as raw materials. The method comprises the following steps: (1) taking natural lignocellulose as the raw materials; (2) dissolving the natural lignocellulose and extracting lignin by taking a commixed electrolyte solution composed of ion liquid/an organic solvent as a solvent; (3) precipitating cellulose and semi-cellulose in the natural lignocellulose by an anti-solvent, and separating to obtain a lignin electrolyte solution; (4) adding with synthesized polymers at different parts relative to the lignin into the obtained lignin electrolyte solution to obtain a lignin-synthesized polymer electrolyte electrostatic spinning raw solution; and (5) preparing the lignin composite nano fibers by using the spinning solution through an electrostatic spinning technology. According to the method provided by the invention, all components in corn straws can be efficiently utilized; a technological process is simple and the dissolving can be recycled; the method is pollution-free and environmentally friendly, and economical and energy-saving properties are realized; and the prepared lignin-based electrostatic spinning composite fibers are uniform and continuous, have good thermal stability and can be biologically degraded.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Separation wall for carrying out in situ separation repair on pollution site and construction method thereof

The invention discloses a separation wall for carrying out in situ separation repair on a pollution site and a construction method thereof. The separation wall consists of unpolluted in situ soil and bentonite, wherein the mass ratio of the in situ soil to the bentonite is 95:5 to 85:15. The construction method of the separation wall comprises the following steps of: a first step of excavating a trough body in a region on the periphery of the pollution site, wherein soil digged out from the trough body is the unpolluted in situ soil; a second step of preparing bentonite slurry; a third step of pouring the bentonite slurry into the trough body; a fourth step of preparing back filling, i.e. adding bentonite dry powder in the unpolluted in situ soil, uniformly mixing the unpolluted in situ soil and the bentonite dry powder to form the back filling; and a fifth step of filling back the back filling mixed with the bentonite into the trough body and uniformly stirring the back filling and the bentonite slurry in the trough body. Due to the adoption of the technical scheme, the construction cost of the separation wall can be reduced, the separation response time is shortened, and the separation effect is improved. Meanwhile, the construction method is simple.
Owner:SOUTHEAST UNIV

Instant radix millettiae speciosae and preparation method and consumption method thereof

The present invention provides an instant radix millettiae speciosae and a preparation method thereof. The method comprises the following steps: 1) fresh radix millettiae speciosae is washed, the washed radix millettiae speciosae is sliced, the sliced radix millettiae speciosae is crushed, water is added, the crushd radix millettiae speciosae is subjected to a vacuum flash extraction, and the extracted radix millettiae speciosae is filtrated, wherein the vacuum flash extraction is conducted at a temperature of 60-90 DEG C and a vacuum degree of -0.08 to -0.098 MPa; 2) the radix millettiae speciosae extract is concentrated and dried to obtain a dried radix millettiae speciosae paste; and 3) the dried paste is crushed to obtain the instant radix millettiae speciosae. The vacuum flash extraction fully dissolves the various active ingredients in the radix millettiae speciosae and also solves the problem that the extraction of the radix millettiae speciosae is serious in blistering. Then a series of specific technologies are used to obtain the instant radix millettiae speciosae, so that the nutrients of the fresh radix millettiae speciosae are maximally preserved. The present invention also provides a consumption method of the instant radix millettiae speciosae.
Owner:桂林亦元生现代生物技术有限公司

Method for determining rare earth elements in super-based rock by ICP-MS

The invention provides a method for determining rare earth elements in a super-based rock by ICP-MS. The method comprises the following steps: accurately weighing a powder sample and putting the powder sample into a sample dissolving bomb; adding high-purity nitric acid and high-purity hydrofluoric acid in sequence; putting the sample dissolving bomb into a steel sleeve, screwing and putting the sample dissolving bomb into a drying oven for heating; after the sample dissolving bomb is cooled and the cover is opened, putting the sample dissolving bomb on an electric heating plate and evaporating to dryness; adding nitric acid and evaporating to dryness again; adding high-purity nitric acid and ultrapure water; putting the sample dissolving bomb into the steel sleeve, screwing and putting the sample dissolving bomb into the drying oven for heating; putting the sample dissolving bomb on the electric heating plate and evaporating to dryness; adding hydrochloric acid and evaporating to dryness again; adding hydrochloric acid and dissolving; centrifuging the sample by utilizing a centrifugal machine; taking supernatant and putting the supernatant on a column; adding hydrochloric acid towash the column and adding hydrochloric acid to connect the sample; after evaporating the sample to dryness, adding nitric acid; after evaporating to dryness again, adding nitric acid and fixing the volume; finally, determining the content of the rare earth elements in the sample by ICP-MS. According to the method provided by the invention, the ultralow-low-content rare earth elements in the super-based rock can be effectively detected; an obtained rare earth partition curve is smooth in distribution and a detection result is accurate and reliable.
Owner:武汉上谱分析科技有限责任公司

Method for producing ceramic die core

The invention provides a method for producing a ceramic die core. The method comprises the following steps of (1) producing a ceramic die core blank; (2) pre-treating a filler for the shaping of the ceramic die core, specifically adding the filler to be treated into a nonmetal material hopper with de-ionized water, continuously stirring slurry obtained by mixing powder and de-ionized water, continuously dropwise adding analytically pure hydrochloric acid to adjust the pH value of the slurry to 4 to 6, stopping adding analytically pure hydrochloric acid when the pH value is changed by less than or equal to 0.2 within 5 minutes, continuing stirring the slurry for 10 to 60 minutes, standing and settling the slurry for 4 to 12 hours, pouring an upper-layer solution, washing settled powder for 1 to 3 times by using de-ionized water until the pH value of an obtained solution is 6 to 8, drying the powder finally sinking to the bottom at 100 to 140 DEG C, calcining the powder for 4 to 6 hours at 1200 to 1500 DEG C, and crushing and sieving the powder; (3) performing shaping calcination; (4) performing reinforcement reconditioning. The method is simple, economical and low in time consumption, manpower is saved, energy consumption is eliminated, the production efficiency of the ceramic die core is greatly improved, and the quality of the ceramic die core is improved.
Owner:DONGFANG TURBINE CO LTD

Construction method for large-span cast-in-situ beam slab support system of plant

InactiveCN101929244BRealize measurable and controllablePlay a supporting roleForms/shuttering/falseworksShoresSupporting systemFalsework
The invention relates to a construction method for a large-span cast-in-situ beam slab support system of a plant, which is characterized in that a middle part and an upper part of a shear wall are respectively buried with I-shaped steel to stretch over a room, and a pull ring 9 is welded on the one-third, a cross part, of the middle I-shaped steel 1 for obliquely drawing a steel wire rope 7 between wall bodies, a roof full scaffold is supported on two layers of the I-shaped steel 1 to unload the I-shaped steel 1 through obliquely drawing the I-shaped steel 1 and the steel wire rope 7 between the shear walls with a turnbuckle 8, and the forced deformation of the support system is measured and controlled by measuring the deformation of the I-shaped steel 1 in the concrete casting and loading process. The embodiment scheme of the construction method is that the settlement deformation of the I-shaped steel 1 in different loading stages can be measured through a leveling instrument in the process of the concrete casting and loading process, if the deformation exceeds a preset limit value, the I-shaped steel is unloaded through fastening the turnbuckle 8 to strain the steel wire rope 7,so as to prevent the deformation from exceeding the preset limit value, and the loading deformation value of the support system can be continuously kept in the limit value range through circulating operation, thereby achieving the effective measureable and controllable effect.
Owner:中国人民解放军63926部队
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