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34 results about "Ethyl alpha-cyanoacrylate" patented technology

Adhesive for quickly mutually sticking vulcanized silicone rubbers and preparation method of adhesive

The invention discloses an adhesive for quickly mutually sticking vulcanized silicone rubbers and a preparation method of the adhesive. The preparation method of the adhesive comprises the following steps of: adding alpha- ethyl cyanoacrylate, a thickener, a stabilizer, a plasticizer and a sticking promoter to a water-free oxygen-free reactor; mixing for 0.5 hour-4 hours at 40 DEG C-80 DEG C under the protection of a dry nitrogen gas atmosphere; cooling to room temperature and finally introducing dry sulfur dioxide gas and stirring for 0.5 hour-2 hours. On one hand, the adhesive provided by the invention can overcome the defect that the common rapid curing adhesive has poor adhesion with the vulcanized silicone rubber; on the other hand, the adhesive can overcome the defects that the room-temperature vulcanized silicone rubber (RTV) is long in curing period and low in production efficiency when used for adhering the vulcanized silicone rubber. The adhesive disclosed by the invention has the advantages of high curing speed, short curing period and high adhering strength for the vulcanized silicone rubber, and can be used for realizing in-situ forming of vulcanized silicone rubber products.
Owner:浙江凌志新材料有限公司

Anti-skid hydrophobic zebra crossing coating with long-lasting snow melting properties and preparation method of coating

The invention discloses an anti-skid hydrophobic zebra crossing coating with long-lasting snow melting properties. The coating includes a slurry and a curing agent; the slurry comprises the followingcomponents in parts by mass: 120-150 parts of a water-based acrylic emulsion, 20-30 parts of bisphenol A epoxy resin, 5-8 parts of sodium 2-ethylhexyl sulfate, 20-25 parts of titanium dioxide, 2-5 parts of a dispersant, 2-3 parts of a water-based wetting agent, 2-3 parts of a levelling agent, 5-8 parts of modified nano silicon dioxide powder, 5-8 parts of ice snow melting powder, 3-5 parts of luminous powder, 5-8 parts of quartz sand, and 20-40 parts of water; and the curing agent comprises the following components in parts by mass: 100 parts of organic silicon modified acrylic resin, 20-30 parts of ethyl alpha-cyanoacrylate, and 30-40 parts of triethylene tetramine. The zebra crossing coating provided by the invention has anti-skid, hydrophobic and snow melting properties, and can preventrain and snow from accumulating on the surface of the zebra crossing coating during rain and snow weather, thereby preventing vehicles from skidding or pedestrians from falling down when the vehiclesand the pedestrians pass a zebra crossing.
Owner:许飞扬

Adhesive for wood-plastic floor decorative paper immersion

The invention discloses an adhesive for wood-plastic floor decorative paper immersion, relating to the technical field of floor processing. The adhesive for wood-plastic floor decorative paper immersion is prepared from the following raw materials in parts by weight: 90-100 parts of ethyl alpha-cyanoacrylate, 35-40 parts of sodium carboxymethyl starch, 15-20 parts of nano clay, 15-20 parts of putty powder, 15-20 parts of palm oil, 12-18 parts of meerschaum powder, 12-18 parts of chitosan, 10-15 parts of triethyl citrate, 10-15 parts of aloe leaf, 8-12 parts of sodium alginate, 8-12 parts of maleic rosin, 6-10 parts of soybean protein glue, 6-10 parts of deodorant, 4-8 parts of sodium chloride, 80-100 parts of ethanol and 450-500 parts of water. By using the ethyl alpha-cyanoacrylate and sodium carboxymethyl starch as the main raw materials and the multiple assistants as the auxiliary materials, the prepared adhesive has the characteristics of fresh taste, high viscosity, stable properties, high safety and environment friendliness, and can not volatilize harmful gas.
Owner:安徽温禾新材料科技股份有限公司

Production process for alpha-cyanoethyl acrylate adhesive

The invention provides a production process for an alpha-cyanoethyl acrylate adhesive. The production process comprises the following steps: under the action of a catalyst, subjecting ethyl cyanoacetate, solid formaldehyde and an organic solvent to condensation polymerization in a reaction vessel so as to obtain a reaction system; then adding an organic solvent into the reaction system from the bottom of the reaction vessel and then carrying out condensation, reflux and dehydration; and finally, adding an auxiliary agent into the reaction system obtained in the previous step and carrying out a cracking reaction so as to obtain the alpha-cyanoethyl acrylate adhesive. The production process employs specific reaction steps, so yield is further improved, and production cost is reduced; and in particular, after completion of condensation polymerization and synthesis reaction of materials, the organic solvent is added from the bottom of reaction vessel and an external reflux and dehydration manner is employed, so dehydration is more thorough, removal of a trace amount of moisture is much easier, stability of the adhesive is improved, and the shelf-life of the adhesive is further prolonged.
Owner:湖南浩森胶业有限公司

Plastic adhesive

The invention discloses a plastic adhesive. The adhesive is prepared in steps as follows: a, asphalt and n-heptane are mixed, treated in an airtight reaction kettle at the temperature of 100-150 DEG C for 1-12 h and filtered, and filtrate is obtained; b, the filtrate is dried in the nitrogen fluid state at the temperature of 100-150 DEG C for 1-10 h, solids are obtained, finely ground, sieved by a 50-120-mesh sieve and then dispersed in ethyl alpha cyanoacrylate to be stirred for 10-30 min, ethyl carbamate glycol, 2,4,4-trimethyl-1,6-hexamethylene diamine, ethylene carbonate, dichloro-hexylidene diisocyanate, melamino-formaldehyde resin, epoxy resin, vinyl chloride-vinyl acetate resin, an expanding agent, desulfurized gypsum and a curing agent are added, and the plastic adhesive is obtained. The provided plastic adhesive can powerfully bond a wood material and plastic, and no harmful organic substances are produced.
Owner:GUANGDONG YUCHEN YUANCHUANG ENERGY SAVING ENVIRONMENTAL PROTECTION TECH CO LTD

Silver conductive adhesive as well as preparation method and application thereof

The invention provides a silver conductive adhesive, comprising a basic resin, a curing agent, a curing accelerator and a conductive material, wherein the basic resin is epoxy resin, the curing agent is binary aliphatic ether amine and versamid, the curing accelerator is 2,4,6-tri-(dimethylaminomethyl)-phenol, and the conductive material is silver powder. The silver conductive adhesive is characterized by furthering comprising alpha-cyan ethyl acrylate and polyether. The invention further provides a preparation method and application of the silver conductive adhesive. The silver conductive adhesive prepared in the invention can be completely cured within 5-15min at room temperature (25 DEG C) and has good cohesiveness and conductivity.
Owner:BYD CO LTD

Two-component quick-drying glue and preparation method thereof

The invention relates to two-component quick-drying glue and a preparation method thereof. The two-component quick-drying gel comprises a component A and a component B. The component A comprises ethylalpha-cyanoacrylate, an ethyl alpha-cyanoacrylate solution containing 1000 ppm of boron trifluoride, phosphoric acid with a concentration of 85%, lithium tetrafluoroborate and vinyl chloride-vinyl acetate resin. The component B comprises an epoxy resin, a toughening agent, an accelerator, ABS high rubber powder and fumed silica. The two-component quick-drying glue realizes rapid curing at the room temperature and has good toughness and impact resistance. The two-component quick-drying glue is suitable for bonding metals and most of plastic and rubber, has adhesion to plastic than that of epoxy glue and toughness and high temperature resistance better than those of the cyanoacrylate and is suitable for a high temperature and high humidity environment.
Owner:烟台长盈电子科技有限公司

Nano particle of enwrapping water-soluble active ingredient, and preparation method

This invention discloses a method for preparing nanoparticles containing water-soluble active component. The cores are composed of water-soluble active component, and the shells are composed of polymer of alkyl alpha-cyanoacrylate monomer. The average diameter of the nanoparticles at 25 deg.C is 100-500 nm. The water-soluble active component is one or more of vitamin C, vitamin B, hyaluronic acid and hyaluronic acid derivatives. The alkyl alpha-cyanoacrylate monomer is ethyl alpha-cyanoacrylate monomer or butyl alpha-cyanoacrylate monomer. The carrier material has such advantages as high biocompatibility, and high safety in cosmetic field. The method has such advantages as simple operation and high stability. The obtained nanoparticles have such advantages as small and uniform sizes, high permeability to skin, high drug loading rate, and stable protection of sensitive active substances.
Owner:SHANGHAI INST OF TECH

Preparation dedicated binder of microbeam analysis standard sample and blending method thereof

The invention provides a preparation dedicated binder of a microbeam analysis standard sample. The preparation dedicated binder of a microbeam analysis standard sample comprises components with the following volume fraction: alpha-ethyl cyanoacrylate, the volume fraction of the alpha-ethyl cyanoacrylate is more than 50%, tackifier, the volume fraction of the tackifier is 1-5%; stabilizer, the volume fraction of the stabilizer is 1-5%, flexibilizer, the volume fraction of the flexibilizer is 1-5%, and polymerization inhibitor, the volume fraction of the polymerization inhibitor is 1-5%. Simultaneously, the invention further provides a blending method of the preparation dedicated binder of a microbeam analysis standard sample, a throwing sequence is as following: the alpha- ethyl cyanoacrylate, the polymerization inhibitor, the stabilizer, the flexibilizer, and the tackifier, blended using time is controlled within one tenth of a binder solidification time. The preparation dedicated binder of the microbeam analysis standard sample possesses appropriate liquidity, solidification speed, and good electroconductibility in the meantime, solves an embedding problem of the microbeam analysis standard sample in the preparation process, so that an embedding rate of finished products is effectively improved.
Owner:BAOSHAN IRON & STEEL CO LTD

Environment-friendly low-whitening instant adhesive

The invention discloses an environment-friendly low-whitening instant adhesive. The instant adhesive is composed of the following materials: cage silsesquioxane / acrylate copolymer-modified ethyl alpha-cyanoacrylate, hydrophilic modified n-octyl alpha-cyanoacrylate, n-butyl alpha-cyanoacrylate and additives at a mass ratio of (1-10):(1-10):(80-95):(0.5-5). Through the instant adhesive, the technical problems of poor heat resistance, poor aging resistance, large irritating odor and easy whitening phenomena of a traditional instant adhesive are solved, and the use effect of the instant adhesive is improved through modification treatment and reasonable compounding of the different components.
Owner:浙江派菲特新材料科技有限公司

Square liquid-state aluminum electrolytic capacitor with flexible package and manufacturing process thereof

The invention discloses a square liquid-state aluminum electrolytic capacitor with flexible package, comprising a flexible shell and a flat elliptoid capacitor core bag, wherein the capacitor core bag is sealed in the flexible shell and comprises an anode foil, a cathode foil, electrolytic paper, a positive lead and a negative lead; the electrolytic paper is placed between the anode foil and the cathode foil; the positive lead and the negative lead are respectively connected to the anode foil and the cathode foil in a riveting way; the aluminum stems of the positive lead and the negative lead are in sealed connection with the flexible shell through PP glue (mainly comprising ethyl-alpha-cyanoacrylate). The square liquid-state aluminum electrolytic capacitor with flexible package can bear bending to some extent in the process of installation and use since the shell is of flexible package; moreover, due to use of the flexible package design, the rubber plug design of the traditional aluminum electrolytic capacitor is omitted and therefore the cost is saved. With adoption of the square liquid-state aluminum electrolytic capacitor, the conductivity of a conducting polymer is high, the equivalent series resistance and impedance of the capacitor are relatively low and loss is low; the ripple resistance is strong.
Owner:HUNAN AIHUA GRP

High-viscosity environment-friendly glue

The invention discloses high-viscosity environment-friendly glue. The high-viscosity environment-friendly glue is prepared from, by mass, 15-18 parts of polyvinyl alcohol, 8-12 parts of aluminum silicate ceramic fiber, 12-15 parts of sodium benzoate, 7-9 parts of methacrylate, 6-10 parts of salicylic acid, 7-13 parts of trimethylolpropane, 5-9 parts of butanediol, 12-16 parts of rosin, 7-12 parts of ethyl Alpha-cyanoacrylate, 9-16 parts of latex and 13-15 parts of styrene. The high-viscosity environment-friendly glue is high in viscosity, strong in cohesive force, good in environmental protection and low in manufacturing cost and does not easily shed.
Owner:QINGDAO YUXING INTELLIGENT TECH DEV CO LTD

Quick blocking agent and preparation method thereof

InactiveCN102399532AHigh bonding strengthSatisfy the needs of adding plugging operationsOther chemical processesAnilineEthyl acetate
The invention discloses a quick blocking agent. The blocking agent comprises a component A and a component B in a ratio of 37: 62, wherein the component A comprises 80 to 100 weight parts of alpha-cyan ethyl acrylate and 5 weight parts of fumed silica; and the component B comprises 2.5 weight parts of zinc oxide, 1 weight part of aniline anti-aging agent, 2 weight parts of magnesium oxide, 40 weight parts of ethyl acetate, 20 weight parts of gasoline, 20 weight parts of chloroprene rubber, 10 weight parts of ethane solution and 5 weight parts of carborundum. The invention also discloses a preparation method for the quick blocking agent. The component A and the component B are quickly mixed and stirred in a ratio of 37: 62 and placed at the position to be blocked, and the blocking agent can be quickly cured for blocking; and the blocking agent has high adhesive strength, and completely can meet the requirement of quick and effective blocking operation.
Owner:BAOSHAN IRON & STEEL CO LTD

Butterfly specimen making method

The invention discloses a butterfly specimen making method and relates to the technical field of specimen making. The butterfly specimen making method comprises the steps of 1) applying ethyl Alpha-cyanoacrylate to a whole butterfly, and setting wings of the butterfly to shape for 5-10 min to obtain a butterfly sample with fixed shape; 2) pouring epoxy resin structural adhesive and acrylate structural adhesive into a container, stirring to obtain mixed adhesive, heating the mixed adhesive to 40 DEG C, and pouring part of the mixed adhesive into a lower portion of a mold; 3) placing the butterfly specimen in the mold above the mixed adhesive, pouring the rest of the mixed adhesive until the mold is full, and cooling for 30 min to obtain gel; 4) taking the gel out of the mold to obtain the butterfly specimen. The problems are solved that an existing butterfly specimen damages easily, observation angles are limited, and the existing butterfly specimen has poor ornamental value, takes space for storage and is inconvenient to carry.
Owner:广西柳州中嘉知识产权服务有限公司

Road zebra crossing coating

The invention provides road zebra crossing coating. The road zebra crossing coating comprises the following raw materials in parts by weight: 20-25 parts of polyester acrylate, 15-25 parts of organosilicone-modified acrylic resin, 10-15 parts of ethyl alpha-cyanoacrylate, 4-7 parts of butyl acetate cellulose, 5- 6 parts of a dispersant, 4-6 parts of metal silicon, 2-4 parts of a leveling agent, 4-5 parts of zinc borate, 6-8 parts of luminous powder, 3-5 parts of quartz sand, 2-3 parts of a defoamer, 2-3 parts of an antioxidant and 8-12 parts of water. The road zebra crossing coating has excellent heat resistance, adhesion and aging resistance and has a self-luminous function; and at night, the boundary position of a zebra crossing can be clearly observed in the distance, so that vehicles are reminded of decelerating in advance and stopping accurately, and thus the traffic safety passage rate is increased.
Owner:朱晶霞

Method for sealing tenon on instrument shell

The invention provides a method for sealing a tenon on an instrument shell. According to the method, a quick dry adhesive with Alpha-ethyl cyanoacrylate as a main component is applied into a gap between a flight parameter recorder shell and the tenon so as to achieve the aims of sealing and preventing liquid wax from flowing out. After the method is adopted, even if burning happens, since an adhesive layer in the gap is rapidly carbonized to form a solid blockage, the sealing function does not fail, so that electronic elements are effectively protected; the adhesive layer is not corroded when being soaked in seawater, therefore the protection time is prolonged and consequently the precious time is prolonged for search and rescue work.
Owner:SHAANXI BAOCHENG AVIATION INSTR

Vamp sticker

The invention discloses a vamp sticker which comprises a flower layer and an adhesive layer. The adhesive layer is a flat sealing bag. Alpha-cyan ethyl acrylate pasty adhesive is packaged into the sealing bag. The thickness of the adhesive layer is 0.1-5 mm and pasted below the flower layer. The vamp sticker is convenient to use, is bonded firmly, can be used for repairing a vamp with flowers falling off, and avoids waste, original flowers of the vamp can be replaced according to the personal preference, and the attractiveness of shoes is improved.
Owner:海宁经开产业园区开发建设有限公司

High-strength wood chip adhesive

The invention discloses a high-strength wood chip adhesive. The adhesive is prepared from the following raw materials in parts by weight: 30-50 parts of urea-formaldehyde resin, 1-5 parts of borax, 1-3 parts of caustic soda flakes, 10-20 parts of magnesium oxide, 15-25 parts of starch, 15-20 parts of ethyl alpha-cyanoacrylate, 9-11 parts of talc powder, 22-26 parts of acetone, 5-7 parts of propanol, 1-2 parts of lignin and 4-12 parts of collagen fiber. The high-strength wood chip adhesive has high adhesive capability, is suitable for the manufacture process of wood boards by wood chip adhesion, and has filling and adhesion effects on gaps between wood chips.
Owner:定远县嘉恒木业有限公司

Method for gluing hair elastic ring

The invention relates to a method for gluing a hair elastic ring. The method comprises the following steps of: 1) rinsing the elastic band provided with an ornament layer on the outer layer of a rubber band by using 5 to 10 weight percent aqueous solution of sodium chloride, then cleaning the rinsed elastic band by using 1 to 5 weight percent polyvinyl alcohol or by using 5 to 25 weight percent of triethanolamine, and drying the cleaned elastic band at room temperature; 2) cutting the elastic band with an elastic material thermal cutting machine, performing a circle of ironing on a cutting position for the elastic band by using a heating cutter at the temperature of 200 to 300 DEG C in a twist way, leaving a pressing mark on the ornament layer of the elastic band and performing cutting atthe pressing mark by using a cutter; and 3) wetting two cross sections of the elastic band by spraying 60 to 85 weight percent alcohol, coating glue containing alpha-ethyl cyanoacrylate on the two cross sections and jointing and bonding the two cross sections to form the hair elastic ring. The method for gluing the hair elastic ring discards the conventional way for connecting the elastic band bya metal connecting piece, so that the hair elastic ring becomes a hair ornament which is safe and environmentally-friendly and difficult to be broken and has nice appearance.
Owner:ZHANGZHOU BEITE COSTUME

Preparation dedicated binder of microbeam analysis standard sample and blending method thereof

The invention provides a preparation dedicated binder of a microbeam analysis standard sample. The preparation dedicated binder of a microbeam analysis standard sample comprises components with the following volume fraction: alpha-ethyl cyanoacrylate, the volume fraction of the alpha-ethyl cyanoacrylate is more than 50%, tackifier, the volume fraction of the tackifier is 1-5%; stabilizer, the volume fraction of the stabilizer is 1-5%, flexibilizer, the volume fraction of the flexibilizer is 1-5%, and polymerization inhibitor, the volume fraction of the polymerization inhibitor is 1-5%. Simultaneously, the invention further provides a blending method of the preparation dedicated binder of a microbeam analysis standard sample, a throwing sequence is as following: the alpha- ethyl cyanoacrylate, the polymerization inhibitor, the stabilizer, the flexibilizer, and the tackifier, blended using time is controlled within one tenth of a binder solidification time. The preparation dedicated binder of the microbeam analysis standard sample possesses appropriate liquidity, solidification speed, and good electroconductibility in the meantime, solves an embedding problem of the microbeam analysis standard sample in the preparation process, so that an embedding rate of finished products is effectively improved.
Owner:BAOSHAN IRON & STEEL CO LTD

Office superglue

The invention discloses office superglue which contains the following raw materials (by weight): 25-30 parts of formaldehyde, 8-12 parts of ethyl alpha-cyanoacrylate, 6-8 parts of polyvinyl alcohol, 5-7 parts of aniline, 10-12 parts of an aqueous acrylic emulsion, 2-4 parts of propyl alcohol, 1-3 parts of water glass, 3.2-4.3 parts of citric acid, and 8-11 parts of alkylphenoxy polyoxyethylenepolyoxypropylene. The office superglue of the invention has strong binding power, has a good waterproof effect, is not easy to fall off, has long bonding period, has a good bonding effect, and is low-cost.
Owner:QINGDAO DAFANG WISDOM NETWORK TECH CO LTD

Carbon nanotube-polytetrafluoroethylene valve sealing ring filled with modified mullite powder

The invention discloses a carbon nanotube-polytetrafluoroethylene valve sealing ring filled with modified mullite powder. The valve sealing ring is prepared from the following components: polytetrafluoroethylene, polyphenylene sulfide, carbon nanotubes, phenol, p-toluylic acid, bentonite, diphenyl ether, butyl titanate, sodium hypochlorite with a concentration of 60 to 70%, EDTA, ammonia water, absolute ethyl alcohol, mullite, hydrogen peroxide with a concentration of 10 to 15%, deionized water, 2,4,6-trisphenol, ethyl alpha-cyanoacrylate, a cross-linking agent TAC, molybdenum disulfide, a silane coupling agent KH550, ammonium chloride, urea and water. The sealing ring provided by the invention has good sealing performance, high hardness, small thermal expansion coefficient, high refractoriness, stable thermo-chemical performance and other excellent performance.
Owner:ANHUI RONGDA VALVE

Conductive adhesive

The invention relates to a conductive adhesive. The conductive adhesive is characterized by being prepared from raw material components in parts by weight as follows: 1-24 parts of acrylic rubber, 2-14 parts of an emulsifier, 5-21 parts of triethanolamine, 3-19 parts of diatomite, 2-19 parts of talc, 3-30 parts of acetone, 7-19 parts of sodium bisulfite, 8-10 parts of hydroxypropyl methylcellulose, 11-20 parts of conductive powder, 9-13 parts of polyethylene glycol, 3-7 parts of a dispersant, 6-12 parts of a binder, 8-12 parts of a coupling agent, 6-10 parts of triphenyl phosphate, 9-11 partsof ethyl alpha-cyanoacrylate, 6-8 parts of 4,4'-diphenylmethane diisocyanate and 3-5 parts of water. The provided conductive adhesive has good electrical conductivity, excellent flame retardant effect, excellent flexing resistance and high temperature resistance, and can be used in various environments.
Owner:NANTONG HUAXING OIL EQUIP

A square liquid aluminum electrolytic capacitor with flexible packaging and its manufacturing process

The invention discloses a square liquid-state aluminum electrolytic capacitor with flexible package, comprising a flexible shell and a flat elliptoid capacitor core bag, wherein the capacitor core bag is sealed in the flexible shell and comprises an anode foil, a cathode foil, electrolytic paper, a positive lead and a negative lead; the electrolytic paper is placed between the anode foil and the cathode foil; the positive lead and the negative lead are respectively connected to the anode foil and the cathode foil in a riveting way; the aluminum stems of the positive lead and the negative lead are in sealed connection with the flexible shell through PP glue (mainly comprising ethyl-alpha-cyanoacrylate). The square liquid-state aluminum electrolytic capacitor with flexible package can bear bending to some extent in the process of installation and use since the shell is of flexible package; moreover, due to use of the flexible package design, the rubber plug design of the traditional aluminum electrolytic capacitor is omitted and therefore the cost is saved. With adoption of the square liquid-state aluminum electrolytic capacitor, the conductivity of a conducting polymer is high, the equivalent series resistance and impedance of the capacitor are relatively low and loss is low; the ripple resistance is strong.
Owner:HUNAN AIHUA GRP
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