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151results about How to "Improve degassing efficiency" patented technology

On-line detection system and method of trace dissolved gas in organic oil

The invention discloses an on-line detection system and method of trace dissolved gas in organic oil, characterized in that: a polymer degassing film with short oil-gas balance time is used, thus the structure is simple, and degasification speed is fast; the trace dissolved gas in organic oil is separated through the dual column chromatography, thus the number of channels of traditional chromatograph is simplified; the unique twelve-way valve structure is used, and double chromatographic columns are arranged, thus the system works respectively alternately in states of reflux and sample injection, and the problem of difficult separation of O2 and CO gas existing in the traditional chromatographic system is effectively solved; a trace flammable gas detection sensor produced by using a solidoxide fuel cell technique can simultaneously detect 7 kinds of dissolved gases in organic oil with high detection accuracy and good separating degree of different component gases, and the number of gas sensor in the system is reduced. According to the invention, an oil-gas separation, a gas separation detection unit and a control unit are combined together, thus the volume of the system device isreduced, the stability of the system is increased, and the system is convenient for installation and maintenance.
Owner:CENT SOUTH UNIV

Pure purification smelting method used for nickel-based high-temperature alloy master alloy

The invention relates to a pure purification smelting method of an alloy, in particular to a pure purification smelting method for a nickel-based high-temperature alloy master alloy, and belongs to the technical field of metal smelting. According to the method, pure purification smelting of a master alloy is completed through material distributing and alloy melting, primary refining, alloying andsecondary refining, microalloying controlling and casting. The method has the advantages that the purity of vacuum melting can be effectively improved, the element segregation can be improved, and a nickel-based high-temperature alloy prepared by the method has the advantages that the purity is high, the segregation is low, the quality is remarkably higher than that of an alloy prepared through the existing technology and method, the quality of the nickel-based high-temperature alloy is improved, and the application field is expanded; nickel-based high-temperature alloys with different gradesand marks smelted by adopting the method has good effects; vacuum induction furnaces with the furnace types of 250 kg-grade and 1.5 ton-grade are adopted; and compared with an alloy before smelting and prepared through other technologies and methods, the alloy is remarkably improved in purity and uniformity.
Owner:METALINK SPECIAL ALLOYS CORP

Aluminum melt vacuum treatment system and method

PendingCN111763831AImprove degassing conditionsImprove degassing efficiencyAluminum matrix compositesInductor
The invention discloses an aluminum melt vacuum treatment system and method. The aluminum melt vacuum treatment system comprises an aluminum melting furnace, a vacuum circulation degassing device, a permanent magnet stirring device and a feeding device, the vacuum circulation degassing device is located above the aluminum melting furnace, the top of the vacuum circulation degassing device is connected with the feeding device in a sealed mode, the vacuum circulation degassing device comprises a vacuum chamber with the side wall provided with an extraction opening and comprises a first channel and a second channel which are located at the bottom of the vacuum chamber and communicate with each other, the first channel and the second channel are inserted into the aluminum smelting furnace, aninert gas inlet is formed in the outer side wall of one of the channels, the permanent magnet stirring device is located at the bottom of the aluminum smelting furnace and comprises an inductor and afrequency converter connected with the inductor, a feeding port is formed in the top of the feeding device, a discharging port is formed in the bottom of the feeding device, and the feeding port and the discharging port can be automatically opened and closed and form an interlocking relation. When the system is used for vacuum treatment of aluminum-based alloy or aluminum-based composite materialmelt, the vacuum degassing efficiency of the aluminum melt is greatly improved, and meanwhile, uniform stirring of alloy elements in the aluminum melt can be achieved.
Owner:SHANGHAI JIAO TONG UNIV +1

Oil spraying vacuum degassing device for online monitoring of oil chromatogram and application method

The invention discloses an oil spraying vacuum degassing device for online monitoring of an oil chromatogram and an application method and relates to the field of separating materials through a chromatography. The oil spraying vacuum degassing device comprises a degassing cylinder for degassing, wherein the degassing cylinder is provided with an oil feeding opening for feeding oil and an oil returning opening for discharging the oil; the oil spraying vacuum degassing device further comprises a vacuum pump for realizing negative pressure of the degassing cylinder and a circulating solenoid valve for realizing circulating oil; the oil feeding opening and the oil returning opening are connected through a pipeline provided with the circulating solenoid valve; the oil feeding opening is connected with a spraying structure. When the oil spraying vacuum degassing device is used, pressure in the degassing cylinder is pumped to a complete vacuum negative-pressure state and then transformer oilis injected; then a plurality of times of circulation are carried out and filtered gas is pumped to finish concentration detection work; finally, an oil sample is recycled. The oil spraying vacuum degassing device disclosed by the invention has the beneficial effects that the degassing efficiency is improved and the degassing time is shortened; a bottom-end side face in the degassing cylinder is set to be a reversed tapered surface, so that the volume of residual oil can be effectively reduced and a condition that impurities deposited at the bottom of the inner side of the degassing cylinder are pumped into the pipeline can be avoided.
Owner:SHANDONG WUYUE ELECTRICAL APPLIANCES

Method and apparatus for improving hydrogen utilization rate of hydrogenation equipment

The invention relates to a method and an apparatus for improving a hydrogen utilization rate of hydrogenation equipment. The method comprises the steps of implementing primary gas-liquid separation to distillate oil, a gaseous product and hydrogen after hydrogenation under high pressure through an inertial separation distributor arranged at an inlet of a thermal high pressure separator, and delivering a gas phase to a following system; feeding a liquid phase to a thermal low pressure separator, as a first step in the thermal low pressure separator, implementing primary separation through a jet flashing technology to release a part of low gas (mainly consisting of hydrogen), and settling depending on gravity to separate the gas phase and the liquid phase; under the same pressure, separating hydrogen which is still dissolved in thermal low oil and partial small bubbles through a centrifugal deaerating method in a second step; completely removing liquid drops carried in the gas phase part through cyclone separation or coalescing separation and discharging the gas phase part out of the apparatus, and delivering the distillate oil to a following facility. The method and the apparatus can improve recovery rate of the hydrogenation equipment to the hydrogen contained in the distillate oil after hydrogenation, and can be applied to other processes for recovering the hydrogen as well.
Owner:EAST CHINA UNIV OF SCI & TECH

Automatic volume displaced type vacuum degasser for transformer oil

InactiveCN101762641ASimple degassing processImprove degassing efficiencyComponent separationDegasserGas phase
The invention provides an automatic volume displaced type vacuum degasser for transformer oil. The invention is characterized in that the degasser comprises a sample oil injector, a sample gas quantitative tube, a gas transfer cylinder, a gas exchange cylinder, an oil sample degassing cylinder, an oil draining valve F1 and a plurality of electromagnetic valves; the outlet of the sample oil injector is respectively connected with the oil sample degassing cylinder, the oil draining valve F1 and a third electromagnetic valve F3 by a pipe which is provided with a second electromagnetic valve F2; the other end of the third electromagnetic valve F3 is respectively connected with the gas exchange cylinder and a fourth electromagnetic valve F4; the other end of the fourth electromagnetic valve F4 is respectively connected with the gas transfer cylinder and a fifth electromagnetic valve F5; the other end of the fifth electromagnetic valve F5 is respectively connected with the sample gas quantitative tube and a seventh electromagnetic valve F7; the other end of the seventh electromagnetic valve F7 is communicated with carrier gas; and the outlet of the sample gas quantitative tube is provided with the sixth electromagnetic valve F6. As the preposing degassing device for on-line analysis and monitoring of the oil-gas phase chromatograph of a transformer, the invention has the advantages of high degassing efficiency, quick speed and simple structure, and full-automatic degassing realization.
Owner:ZIBO ZHONGHUI INSTR

Defoaming apparatus for high-viscosity pure-chitosan spinning solution

A degassing device for high-viscosity pure-chitosan spinning solutions having a reaction vessel and stirring device. A feed port and vacuum port are disposed at the upper part of the reaction vessel, an inner cylinder body is fixedly disposed in the center position of the reaction vessel which also has a discharge port, the upper cylinder opening of the inner cylinder body is closed and the lower cylinder opening is open, an umbrella-shaped dispersion plate is fixedly disposed at the periphery of the upper half part of the inner cylinder body, a gap is formed between the outer edge of the umbrella-shaped dispersion plate and the inner wall of the reaction vessel, and small liquid outlet holes are distributed on the part of the inner cylinder body above the umbrella-shaped dispersion plate. The stirring device has a stirring shaft with screw propeller and stirring power unit. The upper end of the stirring shaft is mounted to the stirring power unit, the stirring shaft passes through a mechanical sealing device and enters the reaction vessel with the lower end fixed on a seat-mounted bearing, the stirring shaft is superposed with the axial line of the inner cylinder body, and a gap is formed between the inner wall of the inner cylinder body and screw propeller.
Owner:HISMER BIO TECH

Coating wastewater treatment technology

The invention relates to a coating wastewater treatment technology. The technology comprises the following steps: raw water enters an equalizing tank; water in the equalizing tank enters a prepositioned filter through an elevator pump and is filtered, and the filtered raw water enters a degassing and carbonizing linkage system, wherein a carbonization membrane module is arranged in the degassing and carbonizing linkage system; water discharged from the carbonization membrane module goes through a reagent adding pool a and undergoes reagent adding, the reagent added water enters a micro-electrolysis system through a pump in order to realize treatment of high-concentration organic wastewater; water discharged from the micro-electrolysis system goes through a reagent adding pool b and undergoes reagent adding, and obtained water enters a coiled tube through a pump b and undergoes a Fenton reaction, wherein reagent adding of the reagent adding pool b is carried out to adjust the pH value and the content of hydrogen peroxide; water obtained after the Fenton reaction goes through a reagent adding pool c and undergoes reagent adding, and obtained water enters a coagulation and precipitation tank and precipitates; a clear liquid at the upper portion of the coagulation and precipitation tank enters a photocatalysis system through a pump c in order to remove organic matters in the clear liquid; and water obtained after photocatalysis is collected by an intermediate water tank, and enters an enhanced filter through a pump d, and filtered water is discharged. The technology has the advantages of reduction of the COD value of coating wastewater, simple process flow and long service life.
Owner:HUZHOU SENNUO MEMBRANE TECH ENG

High-concentration vacuum oil-gas separation device and method for online monitoring transformer oil

ActiveCN107247108AFacilitate real-time online analysisShort degassing timeComponent separationAir quality improvementAir pumpDrive motor
The invention relates to a high-concentration vacuum oil-gas separation device and method for online monitoring transformer oil. The high-concentration vacuum oil-gas separation device is provided with a quantification chamber, a gas well, an oil well, a degassing chamber, a gas collection chamber, a quantification pipe, an anti-vacuum gas pump, a driving motor and oil and gas pipelines, wherein a gas path part of a vacuum degassing machine is formed by the gas collection chamber, the anti-vacuum gas pump and the quantification pipe; the lower end of the quantification chamber is connected with an oil outlet of a transformer oil tank and the degassing chamber respectively and the upper end of the quantification chamber is connected with the gas well; the upper end of the gas well is connected with the gas collection chamber through a gas pipeline and the lower end of the gas well is connected to the upper end of the quantification chamber and the upper end of the oil well; the lower end of the oil well is connected with the degassing chamber and an oil inlet of the transformer oil tank through two branch pipelines respectively; the degassing chamber and the gas collection chamber are separated through a piston and the driving motor is connected with the piston; a gas inlet of the anti-vacuum gas pump is connected with the gas collection chamber and a gas outlet of the anti-vacuum gas pump is connected with the quantification pipe. According to the high-concentration vacuum oil-gas separation device and method provided by the invention, degassing is finished by adopting a vacuum degassing principle and real-time online analysis of dissolved gas in the transformer oil is facilitated; a manner of degassing and collecting gas for a plurality of times is adopted, so that the degassing efficiency is high and the repeatability is good.
Owner:SIFANG-TBEA INTELLIGENT ELECTRICAL CO LTD

Degasser

The invention discloses a degasser, which belongs to the comprehensive logging and gas logging equipment and relates to a device for performing online degassing on the slurry extracted from oil exploration drilling. The degasser is provided with a tank body for containing the slurry and a stirring body, wherein the stirring body is used for extending into the tank body to stir the slurry; the tank body is provided with a slurry inlet and a slurry outlet; the inner cavity of the tank body is set as a level-by-level stirring cavity; the level-by-level stirring cavity is divided into classification chambers by a slurry blocking component in the tank body; the slurry blocking component comprises a first slurry blocking sheet and a second slurry blocking sheet; the first slurry blocking sheet is provided with an outer edge that can be closely combined with the inner wall of the tank body and a channel hole; the outer edge is combined with the tank body; and the channel hole is used for forming a channel of the leakage slurry. The tank body of the degasser is set as a drawer type chamber capable of stirring level by level; and by combining the reasonable configuration of the slurry blocking component, the degasser enables the slurry to be stirred more sufficiently in the stirring chamber of the level so as to realize level-by-level sufficient stirring and level-by-level sufficient degassing.
Owner:天津开发区利达科技发展有限公司

Online transformer oil chromatography monitoring system based on vacuum stirrer

The invention discloses an online transformer oil chromatography monitoring system based on a vacuum stirrer. The system comprises a data acquisition unit and a master control computer data processing and fault diagnosis system, wherein the data acquisition unit comprises an oil-gas separator, a chromatographic column, a gas sensor and a CPU (central processing unit), wherein a sampling end of the oil-gas separator is connected with a transformer, an output end of the oil-gas separator is connected to the chromatographic column through a cold trap, an output end of the chromatographic column is connected to the gas sensor, and an output end of the gas sensor is connected to the CPU; the data acquisition unit is connected to the master control computer data processing and fault diagnosis system through a communication network; a vacuum mixing and vibrating degassing device is arranged in the oil-gas separator; a carrier gas generating module is arranged in the data acquisition unit. According to the online transformer oil chromatography monitoring system, a conventional carrier-gas cylinder is replaced with the carrier gas generating module, stable carrier gas is provided for the monitoring system, the data accuracy of the monitoring system is guaranteed, frequent replacement of the carrier-gas cylinder is avoided, and the use is very convenient.
Owner:云南电网有限责任公司文山供电局

Method for removing hydrogen sulfide of food-grade phosphoric acid

The invention discloses a method for removing hydrogen sulfide of food-grade phosphoric acid. The method comprises the following steps of: vacuumizing at a tower top of a hydrogen sulfide removing tower, enabling clean gas to move from a tower bottom to the tower top, conveying industrial arsenic-removed phosphoric acid to the tower top via a circulating pump, evenly distributing the phosphoric acid via a filler layer of the hydrogen sulfide removing tower and subsequently heating hydrogen sulfide in the phosphoric acid to fully contact with rising gas flow, blowing off the hydrogen sulfide to enable the hydrogen sulfide to enter an arsenic-removing reactor from the tower top, enabling the sulfuretted hydrogen-removed phosphoric acid to fall to the tower bottom, and conveying the sulfuretted hydrogen-removed phosphoric acid to the tower top via the circulating pump for continuously removing hydrogen sulfide or conveying the sulfuretted hydrogen-removed phosphoric acid to a finished product tank to obtain the food-grade phosphoric acid according to the detection situation of the removing effect of the hydrogen sulfide. Through the method, the hydrogen sulfide in the phosphoric acid can be accelerated to fully contact with the rising gas flow, the hydrogen sulfide gas in the phosphoric acid is efficiently removed, the problems of time consumption and energy consumption while repeatedly degassing the sulfuretted hydrogen-removed phosphoric acid via the traditional hydrogen sulfide removing device are solved, the circulation time of the process of removing the hydrogen sulfide is shortened and the degassing efficiency and the production continuity of the food-grade phosphoric acid are enhanced.
Owner:GUANGXI MINGLI CHEM

Degasser and tank body and stirring body thereof

The invention discloses a degasser and a tank body and a stirring body thereof, relating to a device for on-line degassing of slurry extracted from oil exploration drilling. The degasser is provided with the tank body for accommodating the slurry and the stirring body; the stirring body is used for stretching into the tank body to stir the slurry; the tank body is provided with a slurry inlet anda slurry outlet, wherein the tank body is also provided with a seat body; one end of the seat body connected with an installation plate is provided with a gas collecting chamber; the tank body has anairtight structure; and the airtight structure is composed of a slurry outlet structure and the slurry inlet structure and an induced draught exhaust port. The stirring body is composed of a stirringbody central shaft and a plurality of stirring rods; the stirring body central shaft is connected with a transmission shaft; the stirring rods are fixedly arranged on the stirring body central shaft at a preset interval, and the adjacent stirring rods are vertical to each other. An inner chamber of the tank body is arranged into a stepwise stirring chamber, and the stepwise stirring chamber is partitioned into graded chambers by a slurry blocking assembly arranged in the tank body; and the slurry blocking assembly consists of a first slurry blocking piece and a second slurry blocking piece.
Owner:天津开发区利达科技发展有限公司

Integrated gas-liquid-solid continuous separation device

The invention discloses an integrated gas-liquid-solid continuous separation device. The device comprises an upper sealing cover, an outer cylinder and a lower sealing cover, and the upper sealing cover, the outer cylinder and the lower sealing cover are connected into a whole through flanges. An upper layer, a middle layer and a lower layer are formed in an inner cavity of the outer cylinder, theupper layer is used for storing oil and gas after primary separation, the middle layer is used for storing oil after secondary separation, the lower layer is used for storing sand and water which arefinally separated, and all the layers are separated through perforated sieve plates and oil absorption felts. Mixed incoming liquid is accelerated to enter a cyclone for primary separation through atangential inlet and a spiral pipe type acceleration flow channel, and then is subjected to secondary separation by oleophylic and hydrophobic oil absorption felts, and continuous separation of a multiphase medium is realized. Multi-stage continuous separation is realized based on the combined action of cyclone separation, settling separation and membrane separation, and high-precision continuousseparation of oil-water-sand-gas four-phase media can be achieved in one device.
Owner:NORTHEAST GASOLINEEUM UNIV

Degassing technology in synthetic process of neoprene

InactiveCN102120789AThe amount of non-condensable gas decreasesImprove heat transfer efficiencyLiquid degasificationNeopreneToluene
The invention discloses a degassing technology in the synthetic process of neoprene. The technology comprises the following steps: neoprene latex with chloroprene monomer enters a first-stage degassing pipe; under the vacuum condition, steam and neoprene latex enter a first-stage separator after steam stripping to obtain first-stage separated gas and first-stage separated neoprene latex; the first-stage separated gas enters a second-stage separator to obtain second-stage separated gas and second-stage separated neoprene latex, the second-stage separated gas enters a third-stage separator to obtain third-stage separated gas and third-stage separated neoprene latex, the third-stage separated gas passes through a water condenser, a chloroprene recycling condenser and a tail gas condenser so that water, chloroprene monomer and toluene are condensed, tail gas is sucked in a first-stage ejector, the ejector is emptied; the first-stage separated neoprene latex, the second-stage separated neoprene latex and the third-stage separated neoprene latex are mixed to enter a second-stage degassing pipe, the mixed gas is flashed under high vacuum degree and then performs first-stage separation twice to obtain final neoprene latex and twice separated gas; the twice separated gas enter first-stage separation twice to obtain final separated gas and final neoprene latex; and the final separated gas is cooled, is sucked by a second-stage ejector and enters a third-stage separator. The process disclosed by the invention has high degree of degassing and high monomer recovery rate which can be more than 90%, the process has low energy consumption; and by adopting the process, the quality of the neoprene product can be increased.
Owner:SEDIN ENG

Degassing and dehydrating miniature device for transformer oil

The invention relates to a degassing and dehydrating miniature device for transformer oil. An oil storage tank is connected with a telescopic degassing tank through a three-way electromagnetic valve and a single-pass electromagnetic value B. The telescopic degassing tank is connected with a vacuum buffer tank through a single-pass electromagnetic valve C. The vacuum buffer tank is connected with a vacuum pump through a single-pass electromagnetic valve D. A sampler is connected with the three-way electromagnetic valve through the single-pass electromagnetic valve A and a thin-film filter. An ultrasonic vibrator is fixed at the lower part of a base of the telescopic degassing tank. The telescopic degassing tank is placed in a temperature-controllable air bath. The upper part of the telescopic degassing tank is connected with an electrical repeated propeller through a connection rod. A pressure sensor is installed on a connection pipe of the telescopic degassing tank and the single-pass electronic valve B. A temperature sensor is installed in the air bath. A vacuum pressure sensor is installed on the vacuum buffer tank. The degassing and dehydrating miniature device for the transformer oil uses combination of the electrical repeated propeller, the telescopic degassing tank and the ultrasonic vibration to perform vacuum degassing and dehydration on samples so that degassing efficiency is improved and degassing speed is high.
Owner:PETROCHINA CO LTD

Preparation method of poly(p-phenylene benzobisoxazole) fibers

The invention belongs to the field of high-performance fibers, and particularly relates to a preparation method of poly(p-phenylene benzobisoxazole) fibers. The preparation method comprises the following steps of taking frozen polyphosphoric acid powder, phosphorus pentoxide, 4,6-diaminoresorcinol hydrochloride and terephthalic acid as raw materials, putting the phosphorus pentoxide into a reaction system step by step in a reasonable proportion in a proper time period, and detecting and regulating the apparent viscosity of the materials in real time in a prepolymerization process to ensure that a prepolymer with uniform apparent viscosity is obtained; performing post-polymerization to obtain PBO spinning slurry; and performing dry-jet wet spinning and post-spinning to obtain the finished PBO fibers. The method overcomes the defects that traditional solid raw materials are poor in solvent mixing and dispersing effect, easy to agglomerate and incapable of uniformly reacting, ensures the consistency of a prepolymerization reaction end point, and reduces the process errors. The intrinsic viscosity of the polymer in the same batch in different time periods is small in change and high, the mechanical property of the fibers can be obviously improved, and the quality stability is also improved.
Owner:SHANDONG NON METALLIC MATERIAL RES INST

Air removal device for water tunnels

InactiveCN104174188AAvoid Cavitation Cavitation HazardsImprove degassing efficiencyLiquid degasificationPumping vacuumWater use
The invention discloses an air removal device for water tunnels, which increases the flow velocity of water and reduces the pressure of water through gravity settling and vacuumizing and by using an orifice air removal generator, so that air dissolved in the water is expanded into bubbles from air cores at low pressure, and the bubbles dissolved in the water quickly emerge from the water, thereby achieving air-liquid separation. Upper and lower barrel bodies are connected by a flange plate, a cover plate is fixedly connected with the upper barrel body, the cover plate is provided with a water inlet pipe communicated with a sleeve, the sleeve is fixed at the middle position of the downside of the cover plate, a first-level orifice is arranged at the bottom of the sleeve, a second-level orifice and a three-level orifice are fixed below the sleeve, a cleaning tube and a vacuumizing tube are located on both sides of the water inlet pipe and communicated with the upper barrel body, a discharge pipe is arranged on a chassis, and a water outlet pipe is located on one side of the lower barrel body. The air removal device can quickly carry out air removal on a large amount of experimental water for water tunnels, thereby avoiding cavitation and erosion hazards caused by air contained in the water in the process of experiments. The air removal device can be applied to the removal of air contained in oil and the air removal of water for air conditioning circulation.
Owner:NORTHWESTERN POLYTECHNICAL UNIV
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