The invention relates to a triazinone preparation method, which comprises: carrying out a
hydrolysis reaction on 1-chloropinacolone at a temperature of 80-140 DEG C under the actions of a
solvent andan alkali to obtain a compound I, wherein the
solvent is water; carrying out an oxidation reaction on the compound I in the presence of
oxygen by using Pt as a catalyst under a neutral or weakly basiccondition to obtain a compound II; and carrying out a ring closure reaction on the compound II and thiocarbohydrazide under the
catalysis of an acid to obtain triazinone, wherein the structure formula of the compound I is defined in the specification, and the structure formula of the compound II is defined in the specification. According to the present invention, 1-chloropinacolone is used as theraw material, and the water is used as the
solvent, such that the generation of high salt
wastewater can be avoided; Pt is used as the catalyst, and
oxygen is used as the oxidant, such that the use of
hydrogen peroxide can be avoided, and the catalyst can be recycled so as to reduce the
raw material cost; and the production method is simple, meets the
environmentally friendly requirement, and issuitable for industrial production, and the yield and the content of the final product are high.