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160 results about "Slow reactions" patented technology

Slow Chemical Reactions. Slow Chemical Reactions: There are chemical reactions that are fast, but there are few that are slow and take place naturally and in the course of time the difference is notable. Few of the examples of slow chemical reactions are: Photosynthesis: Photosynthesis occurs in plants, algae and many other species of bacteria.

Liquid double reagent diagnostic reagent kit for determining content of potassium ions in serum and blood plasma

The invention relates to a liquid double reagent diagnostic reagent kit for determining the content of potassium ions in serum and blood plasma. By using the reaction principle that phosphoenolpyruvic acid (PEP) can be catalyzed by K+dependency pyruvate kinase (PK) to be converted into pyruvic acid and taking lactate dehydrogenase (LDH) as indicator enzyme by means of NADH, the reagent kit detects the reduction amount of the NADH at 340 nm and obtains the result that the change of the absorbance every minute (delta/min) is directly proportional to the content of K+, thereby establishing an enzyme coupling method for continuously determining the potassium ions. In addition, enzyme and a primer system required by slowly generating reduction type nicotinoyl coenzyme are added in a system andan enzyme-primer-coenzyme slow reaction system is formed in a reagent, so that the coenzyme can be slowly and circularly supplemented and the reagent can be stabilized when the concentration reaches a certain balance. The liquid double reagent diagnostic reagent kit is convenient and concise to use, carries out rapid detection on a common ultraviolet/visible light analyzer or a semiautomatic/fully-automatic chemical analyzer, needs no special or extra instrument and has low cost.
Owner:BEIJING STRONG BIOTECH INC

Sulfonic acid type hydrophilic chain extender and preparation method thereof

A hydrophilic chain extender of sulfonic acid type which pertains to chemical product, and preparation thereof. The invention mainly aims to solve the problems of slow reaction rate of hydrophilic chain extender used in aqueous polyurethanel industry, low content of aqueous resin, low heat resistance, low adhesion strength when applying to adhesive. The eligible product is obtained by fully dissolving multi-amine such as 0.5-1.5 parts of ethylenediamine into solvent, reacting with olefin sulfonate such as 5-9 parts of vinyl sodium sulfonate solution with about 25% of water for 4-30 hours at the temperature of 40-100 DEG C., vacuum distilling to remove solvent, dissolving with water, alcohol or ketone, vacuum distilling to remove all solvent for another time after deposition and filter. Stability treatment for storage is further carried out by adding water. The final product is slightly turbid vicous liquid in light yellow color and oil state, with density at 1.16-1.21 g/ml, pH at 11-12, content of ammonia at 6.9+-0.9g NH3/100g, effective content 40-55%. The invention can widely used into production of aqueous polyurethane of different fields, which has a fast reaction rate, high yield, highly enhanced content of solid in prepared aqueous resin, and obviously improved resistance of heat, acid, alkali, hard water, and is greatly beneficial for preparation of adhesive.
Owner:北京林氏精化新材料有限公司

Method for preparing nano hydrated calcium silicate using silican fume as siliceous materials

The invention provides a method for preparing nano hydrated calcium silicate using silican fume as siliceous materials, and solves the problems of slow reaction rate, harsh reaction conditions, low SiO2 reaction degree, low yield, unstable raw material components, and relatively large structure and performance differences of the produced hydrated calcium silicate if current siliceous materials are used as raw materials for the hydrated calcium silicate. The method comprises utilizing the silican fume as siliceous materials and calcium oxide as calcareous materials, with water being added, mixing them in a reaction vessel, and getting the nano hydrated calcium silicate through stirring, hydrothermal reacting, ultrasonic treating, centrifugally separating and vacuum drying. The silican fume used as siliceous materials provided by the invention has advantages of wide source, low price, large specific surface area, strong adsorptivity, mild reaction condition and low impurity content, and thus can be produced into high-purity nano-powder. According to the invention, calcium-silicon ratio, reaction temperature and time can be regulated to control particle sizes of products, thereby obtaining products with excellent performance.
Owner:大同煤矿集团朔州煤电宏力再生工业股份有限公司

Device and method for online measurement of dynamic chlorine demand of conditioning water

The invention belongs to the field of water supply treatment and disinfection, and particularly relates to a device and a method for online measurement of dynamic chlorine demand of conditioning water. The technical scheme disclosed by the invention is that the existing four-way stay spectrometer is improved, and an online control unit is added to form an online stay spectrum device. The method comprises the following steps: accurately measuring the concentration of residual effective chlorine of the chlorine and the conditioning water after a period of time of reaction by the online stay spectrum device on line; dividing reaction of the chlorine and the conditioning water into rapid reaction and slow reaction by linear regression fitting of a logarithmic value and reaction time of the residual effective chlorine; building a calculation formula of short-term chlorine demand on the conditioning water at the rapid reaction stage and long-term chlorine demand on the conditioning water at the slow reaction stage; and calculating the dynamic chlorine demand of the conditioning water according to the demand on a residual chlorine value at the tail end of a pipe network and the stay time, thus the pre-stage control of the fed chlorine can be achieved; the economical efficiency and the security of the fed chlorine are achieved, and water supply security is effectively guaranteed.
Owner:RES CENT FOR ECO ENVIRONMENTAL SCI THE CHINESE ACAD OF SCI

In-situ adsorption-microelectrolysis-catalytic oxidation sewage treatment equipment and method

The invention discloses in-situ adsorption-microelectrolysis-catalytic oxidation sewage treatment equipment and method, belonging to the technical field of sewage treatment in environment engineering. The in-situ adsorption-microelectrolysis-catalytic oxidation sewage treatment equipment is characterized in that adsorption equipment, electrolysis equipment and catalytic oxidation equipment are integrated so as to gather enable pollutants to be gathered from a low-concentration water phase onto an adsorbent; by using the favorable electric conductivity, the adsorbent is used as a complexly polarized three-dimensional electrode to form countless micro electrolytic baths, so that the organic pollutants are electrolyzed while organic matters are adsorbed, and adsorption active sites are continuously regenerated; and by utilizing an electric insulation material, the three-dimensional electrode is complexly polarized and has a high-class oxidation catalyst function at the same time, so that a gas oxidant dissolved in water and an oxidant generated by side reaction of the electrode form a high-class oxidant to efficiently remove the organic pollutants. According to the equipment and the method, the problems of slow reaction speed, low space-time efficiency, low current efficiency and low pollutant degradation efficiency in the conventional electrolytic reactors are solved, and an excellent market prospect is provided.
Owner:DALIAN UNIV OF TECH

Preparation of beta-dione

The invention relates to a preparation method of beta-diketone; Claisen condensation reaction is adopted; the chemical general expression of the beta-diketone is R1COCH2COR2, wherein, R1 is C6-C12 alkyl, and R2 is phenyl or alkylphenyl; the method comprises the following steps: ester, phenyl ketone and partial solvent are pre-mixed for spare; a condensating agent and remaining solvent are added in a reactor, and the temperature is raised under nitrogen atmosphere; during the period when the temperature of the reactor is raised to the needed temperature of the condensation reaction, the pre-mixed material is dropwise added in the reactor for carrying out the condensation reaction with a system which is composed of the condensating agent and the remaining solvent under an infinite reflux condition; after the pre-mixed material is dropwise added, heat-preserving condensation reaction is carried out continuously under the infinite reflux condition. The ester and the condensating agent in the raw material are contacted when the reacting condition is achieved, and acylation reaction is slow reaction, relative to the Claisen condensation reaction, thus being capable of better solving the acidylation problem of the ester, and reducing the effect of the acylation reaction to the minimum; the yield of the beta-diketone is more than or equal to 90 percent.
Owner:KUNSHAN CITY BANMING ELECTRONICS SCI & TECH

Static cracking agent expansion pressure and temperature testing integrated device and testing method thereof

The invention provides a static cracking agent expansion pressure and temperature testing integrated device. The static cracking agent expansion pressure and temperature testing integrated device comprises supporting legs, a base, a hydraulic jack, a left stand column, a right stand column, a top seat, a guide rod, an upper fixing plate, an upper sealing piston, a pressure cell, a supporting limiting nut, a cylinder barrel and a pressure gauge; exhaust passages communicated with the interior of the cylinder barrel are arranged in the upper sealing piston and the upper fixing plate, sealing bolts are arranged at the outer ports of the exhaust passages, a mounting hole is formed in the side part of the cylinder barrel in a radial direction, and a thermometer is arranged in the mounting hole.The invention further discloses a testing method of the static cracking agent expansion pressure and temperature testing integrated device. The device can achieve the purpose of testing the expansionpressure and temperature in the hydration process of static cracking agents with different properties, is easy to carry, high in testing efficiency and testing speed and low in testing cost, can be used repeatedly, can be applied to different environments, and is suitable for testing the expansion pressure and temperature of the static cracking agents in different fast and common slow reactions.
Owner:LULIANG UNIV

Solder convex point connected metal layer in microelectronic package and use thereof

The invention relates to the micro-interconnecting technology in the field of microelectronic encapsulation, in particular to an iron-nickel coating layer with good weldability taken as a solder ball bump connecting metalizing (transition) layer in the microelectronic encapsulation and the application thereof. The invention can be widely applied to the industry of microelectronic encapsulation, is particularly suitable for the BGA and other types of high-density micro-interconnecting technology, and in particular can be taken as a base plate or a bonding pad metalizing layer on a printing circuit board and a ball bump lower metal layer in the flip chip interconnection, and the like. The invention plates an iron-nickel alloy layer on a copper (or a nickel) layer by adopting the plating method; the weight percentage of iron is 5 to 80 percent; and the thickness of the coating layer and the content of an iron element can be adjusted according to the requirements. The coating layer has good weldability, antioxygenic property and very slow reaction rate in the liquid reaction of a solder ball bump. Under the condition of higher temperature, a very thin and smooth compound layer is generated between the coating layer and a solder; and the connecting interface of the coating layer and the solder ball bump has better mechanic reliability.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Preparation method of polysilicate aluminum-titanium and chitosan composite flocculant

The invention discloses a polysilicate aluminum-titanium and chitosan composite flocculant. The polysilicate aluminum-titanium and chitosan composite flocculant is characterized by comprising an environment-friendly chitosan solution and a polysilicate aluminum-titanium solution, so that the environment-friendly and high-efficiency effects are realized. The polysilicate aluminum-titanium and chitosan composite flocculant is prepared by the following steps of (1) acidifying sodium silicate by sulfuric acid with certain concentration, stirring by water bath, aging, and the like, so as to prepare polysilicate; (2) preparing an aluminum salt solution, a titanium salt solution and a chitosan acetate solution; (3) blending with the polysilicate according to certain ratio, so as to prepare polysilicate aluminum-titanium salt; (4) adding the chitosan acetate solution, and aging, so as to obtain polysilicate aluminum-titanium and chitosan; (5) drying, and crushing. The polysilicate aluminum-titanium and chitosan composite flocculant provided by the invention has the advantages that by comprising the natural organic matter of chitosan and the polysilicate aluminum-titanium solution, the preparation method is simple, the property is stable, the problems of large usage amount of inorganic flocculant, poor bridging action, slower reaction speed of organic flocculant and high agent cost are solved, and the application prospect is broad.
Owner:JILIN INST OF CHEM TECH
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