The invention discloses a preparation method of an adsorbent for removing
heavy metals in municipal
sludge. The method comprises the synthesis and modification processes of the adsorbent. The preparation method comprises the following steps: firstly, preparing an adsorbent precursor, preparing a
mixed solution according to the ratio of a
calcium source to a
silicon source to
sodium hydroxide to water being 4: (5-6): (11-40): (72-175), then transferring the obtained
mixed solution into a
hydrothermal reaction kettle with a
polytetrafluoroethylene lining, and reacting for 10-12 hours under the conditions of 180-190 DEG C and 0.8-1.0 MPa; after the reaction is finished, washing,
drying and
grinding to obtain an adsorbent precursor; and then preparing the heavy
metal adsorbent: mixing
cerium chloride and water according to a
mass ratio of 1: (30-50), and stirring for 30-60 minutes in a
room temperature environment. The
mass ratio of the adsorbent precursor to the
cerium chloride solution is 1: (20-25), stirring at
room temperature for 2-4 hours, standing for 1-2 hours, alternately washing with
ethanol and deionized water for 3-5 times, and finally
drying to obtain the adsorbent. The prepared adsorbent can be used for removing the
heavy metals in the municipal
sludge, the amount ratio of the adsorbent to the municipal
sludge is 1: (200-250) when the adsorbent is used, and the highest value of the removal efficiency of each group after the reaction is carried out for 50-70 minutes at the temperature of 25-50 DEG C reaches 90% or above. The method effectively improves the removal effect of the
heavy metals in the municipal sludge, and provides a solution for reducing the content of the heavy metals in the municipal sludge.