The invention discloses a recycling process of a methyl sulcotrione 
solvent. The recycling process comprises the following steps: transferring a methyl sulcotrione 
dichloroethane solution which is subjected to condensation and rearrangement and contains 
triethylamine into a 
triethylamine salifying kettle and adding water under the condition that the volume ratio of 
dichloroethane to the water is 1 to (1-5) (v / v) (Volume Per Volume), starting stirring, slowly dripping a 80% to 91% dilute sulphuric acid solution according to the condition that the 
molar ratio of the 
triethylamine to the dilute sulphuric acid is 1 to (0.5-0.8) (mol / mol), regulating pH within 1 to 1.5, stirring for 15 minutes, separating out a methyl sulcotrione 
dichloroethane solution at a lower layer, and carrying out reduced pressure 
distillation for recycling the dichloroethane containing the water; putting a triethylamine 
sulfate aqueous solution at an upper layer into a 
storage tank; and simultaneously treating the obtained dichloroethane containing the water and the triethylamine 
sulfate aqueous solution. According to the recycling process, an acid-base 
neutralization salifying theory is adopted; the performances of 
dehydration and water absorption of materials are utilized, so that the whole recycling process is low in 
energy consumption, low in cost, mutually complementary, less in equipment investment and simple to operate, and is used for completely solving the problems of high cost and 
high energy consumption of the 
solvent separated in a 
distillation recycling manner. Thus, the recycling process disclosed by the invention conforms to the ideals of 
energy conservation and emission reduction in China.