The invention discloses a recycling process of a methyl sulcotrione
solvent. The recycling process comprises the following steps: transferring a methyl sulcotrione
dichloroethane solution which is subjected to condensation and rearrangement and contains
triethylamine into a
triethylamine salifying kettle and adding water under the condition that the volume ratio of
dichloroethane to the water is 1 to (1-5) (v / v) (Volume Per Volume), starting stirring, slowly dripping a 80% to 91% dilute sulphuric acid solution according to the condition that the
molar ratio of the
triethylamine to the dilute sulphuric acid is 1 to (0.5-0.8) (mol / mol), regulating pH within 1 to 1.5, stirring for 15 minutes, separating out a methyl sulcotrione
dichloroethane solution at a lower layer, and carrying out reduced pressure
distillation for recycling the dichloroethane containing the water; putting a triethylamine
sulfate aqueous solution at an upper layer into a
storage tank; and simultaneously treating the obtained dichloroethane containing the water and the triethylamine
sulfate aqueous solution. According to the recycling process, an acid-base
neutralization salifying theory is adopted; the performances of
dehydration and water absorption of materials are utilized, so that the whole recycling process is low in
energy consumption, low in cost, mutually complementary, less in equipment investment and simple to operate, and is used for completely solving the problems of high cost and
high energy consumption of the
solvent separated in a
distillation recycling manner. Thus, the recycling process disclosed by the invention conforms to the ideals of
energy conservation and emission reduction in China.