The invention discloses a synthesis method of
phosphate. The method comprises the following steps: (1) adding organic
alcohol into a reaction kettle; (2) proportionally adding
phosphorus pentoxide into a feeding box, and setting the rotating speed of the feeding box, wherein the adding time of
phosphorus pentoxide is controlled to be 1-3 h, a
circulating pump is started in the feeding process, thespeed of circulating liquid is controlled, a plurality of small holes are formed in the
surface layer of the feeding box,
phosphorus pentoxide overflows from the small holes through the rotation of abox body and enters the reaction kettle to react with organic
alcohol; and (3) after addition of the
phosphorus pentoxide is finished, raising the temperature of the reaction kettle to 70-90 DEG C, and continuing reacting for 5-7 hours to obtain a
phosphate product. According to the invention,
phosphate is prepared by adopting a
solvent-free method; the adding amount and quality of
phosphorus pentoxide are guaranteed by controlling the adding mode of
phosphorus pentoxide and setting a material circulating device; heat generated by the reaction is discharged in time, so reaction stability is guaranteed, and the prepared
phosphate product is stable and high in esterification rate; and the formed
system is colorless and transparent, decoloration is not needed, and the product does not contain any decolorizing agent.