The invention discloses a continuous preparation method of
ethylene glycol dimethacrylate, and aims to provide a continuous preparation method of
ethylene glycol dimethacrylate, which is high in
reaction rate and high in product yield, and is characterized in that
methacrylic acid and
ethylene glycol are used as raw materials, and
continuous production is realized through
reactive distillation; the technical scheme comprises the following steps; the method comprises the following steps: 1, filling a
reactive distillation tower with a filler, putting
methacrylic acid,
ethylene glycol, a
polymerization inhibitor and
sodium hydrogen sulfate into a feeding tank, and uniformly stirring to obtain a reaction
raw material; 2, turning on a main power supply, starting a
reaction control system, starting a cyclic heating device, and controlling the temperature of the rectifying column to be 100-120 DEG C; starting a circulating condensing device, and controlling the temperature of
condensed water to be 0-10 DEG C; 3, starting a
peristaltic pump to pump the reaction raw materials in the feeding tank into the reaction rectifying
tower, starting an
air pump to introduce air, collecting condensate water at the top of the rectifying
tower at the beginning of reaction, and obtaining a crude
ethylene glycol dimethacrylate product at the bottom of the rectifying tower; and 4, timely transferring water and
methacrylic acid collected at the tower top to a tower top
liquid storage tank through a pipeline, and timely transferring an
ethylene glycol dimethacrylate crude product collected at a tower kettle to an
ethylene glycol dimethacrylate crude product
storage tank through a pipeline.