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32results about How to "Improve sintering density" patented technology

High-temperature X8R type ceramic-capacitor dielectric material and preparation method thereof

The invention belongs to the technical field of ceramic-capacitor dielectric materials and particularly relates to a high-temperature X8R type ceramic-capacitor dielectric material. The high-temperature X8R type ceramic-capacitor dielectric material is characterized in that a co-fusion content of barium titanate and sodium bismuth titanate barium is taken as the main material, a co-fusion content of niobium manganese and oxide of A, a silicon lithium co-fusion content, a barium metaborate co-fusion content and Re2O3 are added, the element A is one or more of cobalt, nickel, zinc, bismuth and the like, and the element Re is one or more of rare-earth elements of praseodymium, samarium, gadolinium, dysprosium and the like. A capacitor made from the high-temperature X8R type ceramic-capacitor dielectric material is high in dielectric constant and high-temperature stability, medium-temperature sintering can be realized since the high-temperature X8R type ceramic-capacitor dielectric material can be matched with a medium and low-temperature sintered 30Pd-70Ag inner electrode in production of a multilayer ceramic dielectric fixed capacitor, application in high-temperature environment is realized, and high industrial prospects and industrial application value are achieved.
Owner:FUJIAN TORCH ELECTRON TECH CO LTD

Ultralow dielectric constant microwave dielectric ceramic material and preparation method thereof

The invention discloses an ultralow dielectric constant microwave dielectric ceramic material. The material is prepared by sintering, by mass, 93-95% of fused silica powder, 2-4% of nanometer silica powder, 0.5-2.5% of CaF2 and 0.5-2.5% of MnO2, and the principal phase of the ultralow dielectric constant microwave dielectric ceramic material is crystalline state SiO2. The invention further discloses a preparation method of the ultralow dielectric constant microwave dielectric ceramic material. The method comprises the steps that S1, CaF2 and MnO2 powder are ground and mixed; S2, the fused silica powder and the nanometer silica powder are mixed, the CaF2 and MnO2 mixed powder obtained in step 1 is added, and wet process ball milling is performed to obtain a mixture; S3, the mixture obtainedin step 2 is dried, granulation and pressing are performed to obtain a perform body, and the perform body is sintered to obtain the ceramic material. The ultralow dielectric constant microwave dielectric ceramic material is wide in raw material source, the preparation method is simple and convenient to implement, practical application and production are facilitated, the obtained ceramic materialis low in dielectric constant, the temperature coefficient of resonance frequency approaches to zero, and the ultralow dielectric constant microwave dielectric ceramic material can be widely applied to manufacturing microwave devices such as a microwave substrate and a missile radome.
Owner:CHANGSHU INSTITUTE OF TECHNOLOGY

Preparing method for magnesium synthetic material

The invention discloses a preparing method for a magnesium synthetic material. The preparing method comprises the following steps that light roasting magnesium calcium powder is subjected to sufficient fine grinding, light roasting calcium magnesium fine powder is obtained, and in addition, iron oxide red is subjected to sufficient fine grinding; the obtained fine powder and finely ground iron oxide red are subjected to co-grinding, and activated nano calcium carbonate is evenly added in the co-grinding process; water is added in the co-grinding fine powder, the mixture is placed in a rolling machine to be subjected to stirring and wheel rolling, stirring is uniform, and the press heating temperature is larger than or equal to 40 DEG C; wet powder is added in a ball pressing machine to be compacted, and ball blanks are manufactured in the ball pressing process; the obtained ball blanks are naturally dried; and the obtained dry blanks are placed in a kiln to be fired, the firing temperature ranges from 1,600 DEG C to 1,700 DEG C, heat preservation is conducted for 2-6 h, and the magnesium synthetic material is obtained. According to the preparing method, the magnesium synthetic material can be manufactured at the relatively low firing temperature and the short firing time, coal consumption is effectively reduced, the production cost is controlled, sufficient sintering of the magnesium synthetic material is guaranteed as well, and the firing compactness of the magnesium synthetic material is improved.
Owner:北京利尔高温材料股份有限公司

Method for preparing titanium subgroup carbonitride solid solution composite ceramic material by sintering

The invention relates to a method for preparing a titanium subgroup carbonitride solid solution composite ceramic material by sintering. The invention belongs to the field of multiphase ceramic materials. The invention aims to solve the technical problems of poor sinterability and fracture toughness of the existing multiphase ceramic. The method comprises the following steps: step 1, mixing titanium subgroup carbide powder and titanium subgroup carbonitride powder or adding titanium subgroup carbonitride powder, ball-milling, mixing and sieving to obtain mixed powder; and step 2, carrying out spark plasma sintering or hot pressed sintering on the mixed powder obtained in the step 1 to obtain the titanium subgroup carbonitride solid solution composite ceramic material. According to the preparation method disclosed by the invention, elements in the same family are mutually used as sintering aids according to solid solution characteristics, so that the phase boundary can be enriched, the sintering performance of the titanium subfamily ceramic is improved, and the solid solution strengthening effect is achieved. Besides, after the titanium subgroup hydride is added, heat preservation is carried out in the initial stage in the sintering process, vacancy is introduced, and the density is remarkably improved.
Owner:HARBIN UNIV OF SCI & TECH

A kind of thin dielectric material for x5r type multilayer ceramic capacitor and its preparation method

The invention provides a thin dielectric material for X5R multilayer ceramic capacitors. The thin dielectric material for X5R multilayer ceramic capacitors is composed of a main component and an auxiliary additive, wherein the main component is BaTi(1-x)CrxO3 (0.005<x<=0.05); on the basis of 100mol of the main component, the addition amount of the auxiliary additive is 0.32-5.6mol; and the auxiliary additive is composed of acetates, transition metal oxides and glass powder. The dielectric material provided by the invention has the advantages of favorable temperature stability and high reliability. By using the chromium barium titanate as the main component, the additive introduced into the formula mostly adopts water-soluble acetates, thereby being more beneficial to the mixing of the additive and main component on the atom level. The thin dielectric material solves the problem of poor product reliability since the oxides used as the main additive and the main component can not be mixed uniformly in the existing dielectric material. The glass powder added into the formula can effectively lower the sintering temperature of the product and enhance the sintering compactness of the product. The introduced rare earth element can enhance the reduction resistance of the dielectric material.
Owner:SHANDONG SINOCERA FUNCTIONAL MATERIAL CO LTD

A kind of ultra-low dielectric constant microwave dielectric ceramic material and preparation method thereof

The invention discloses an ultralow dielectric constant microwave dielectric ceramic material. The material is prepared by sintering, by mass, 93-95% of fused silica powder, 2-4% of nanometer silica powder, 0.5-2.5% of CaF2 and 0.5-2.5% of MnO2, and the principal phase of the ultralow dielectric constant microwave dielectric ceramic material is crystalline state SiO2. The invention further discloses a preparation method of the ultralow dielectric constant microwave dielectric ceramic material. The method comprises the steps that S1, CaF2 and MnO2 powder are ground and mixed; S2, the fused silica powder and the nanometer silica powder are mixed, the CaF2 and MnO2 mixed powder obtained in step 1 is added, and wet process ball milling is performed to obtain a mixture; S3, the mixture obtainedin step 2 is dried, granulation and pressing are performed to obtain a perform body, and the perform body is sintered to obtain the ceramic material. The ultralow dielectric constant microwave dielectric ceramic material is wide in raw material source, the preparation method is simple and convenient to implement, practical application and production are facilitated, the obtained ceramic materialis low in dielectric constant, the temperature coefficient of resonance frequency approaches to zero, and the ultralow dielectric constant microwave dielectric ceramic material can be widely applied to manufacturing microwave devices such as a microwave substrate and a missile radome.
Owner:CHANGSHU INSTITUTE OF TECHNOLOGY

Zinc oxide resistor disc and preparation method thereof

The invention relates to the technical field of inorganic non-metallic materials, and particularly discloses a zinc oxide resistor disc with excellent comprehensive performance and a preparation method thereof. According to the method, on the basis of an existing solid phase method, the density of a green body is improved through raw material particle size grading, the influence of factors such as high porosity, low sintering density, poor particle size uniformity after sintering and uncontrollable grain boundary thickness which are likely to happen to a single raw material particle size on the performance of the zinc oxide resistor disc is overcome, and then the sintering compactness of the resistor disc is improved. According to the invention, crystallization of the resistor disc after sintering is further controlled, the uniformity of the particle size after sintering is improved, and the thickness of the grain boundary layer is regulated, so that the electrical performance of the zinc oxide resistor disc is improved; and the zinc oxide resistor disc prepared by the method has the advantages of high potential gradient, nonlinear coefficient and energy density, low leakage current and residual voltage ratio and the like, the preparation process is simple, the requirement on equipment is low, and batch production is easy.
Owner:STATE GRID HUNAN ELECTRIC POWER +2

A kind of high temperature X8R type ceramic capacitor dielectric material and preparation method thereof

The invention belongs to the technical field of multilayer ceramic capacitor materials, in particular to a high-temperature X8R type ceramic capacitor dielectric material and a preparation method thereof. This kind of high-temperature X8R ceramic capacitor dielectric material is based on the eutectic of barium titanate and bismuth sodium barium titanate, and the eutectic of oxides of niobium, manganese and A, silicon lithium eutectic, and boron barium are added. Fusion, Re 2 o 3 , wherein the element A is one or more of cobalt, nickel, zinc, bismuth, etc., and the element Re is one or more of rare earth elements such as praseodymium, samarium, gadolinium, neodymium, and dysprosium. The capacitor made by using the high-temperature X8R type ceramic capacitor dielectric material of the present invention has high dielectric constant, high compressive strength, high temperature stability, and can be combined with medium-low temperature sintered 30Pd-70Ag inner when preparing multilayer ceramic fixed capacitor The electrodes are matched to achieve medium-temperature sintering, and realize the application in high-temperature environment, which has high industrialization prospect and industrial application value.
Owner:FUJIAN TORCH ELECTRON TECH CO LTD
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