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42results about How to "Reduce the synthesis reaction temperature" patented technology

Method for producing nano-sized vanadium carbide powder

The invention relates to a method for producing nano-sized vanadium carbide powder, belonging to the technical field of preparing ceramic powder. The method comprises the following processes: (1) mixing a vanadium source, a carbon source and an auxiliary into a solution according to a certain proportion; (2) heating the solution, so that the solution is volatilized, concentrated and decomposed to obtain precursor powder containing the vanadium source and the carbon source; and (3) reacting the precursor powder for 1-5 hours at the temperature of 700-1300 DEG C under certain atmosphere. The method is simple in technology, low in cost, and easy to industrialize, and the obtained vanadium carbide powder has a particle size of less than 50nm, and good dispersity.
Owner:UNIV OF SCI & TECH BEIJING

Method for preparing SnIn4S photocatalyst through low-temperature coprecipitation method

The invention relates to a method for preparing a SnIn4S photocatalyst through a low-temperature coprecipitation method. The method is characterized by comprising the following steps: using soluble tin salt as a tin source, soluble indium salt as an indium source, thiourea or thioacetamide as a sulfur source, and methanol, ethanol, propanol and glycol as solvents, performing condensing refluxing at 60-90 DEG C, stirring at a constant speed, and reacting for 3-7 hours; cooling to room temperature, performing suction filtration on a sample, rinsing with deionized water and ethanol for three times, drying the obtained sample for 6-24 hours at 80-120 DEG C to obtain the SnIn4S photocatalyst with relatively higher activity. The SnIn4S photocatalyst can effectively degrade methyl orange, rhodamine B and other organic pollutants in visible light and reduce some heavy metal ions; the method has the significant advantages of simpleness, easiness, low reaction temperature, low energy consumption, short response time and high yield; the product of SnIn4S has very high photocatalytic performance.
Owner:NANCHANG HANGKONG UNIVERSITY

Production method of graphite/iron carbide/ iron nanocomposite

The invention relates to a production method of a graphite / iron carbide / iron nanocomposite and belongs to the technical field of magnetic nanopowder production. The production method includes the processes: (1) dissolving ferric nitrate, adjuvants and a water-soluble carbon source in distilled water according to a proper proportion; (2) heating and stirring, and reacting solution after volatilization and concentration so as to obtain precursor powder containing iron and carbon; (3) reacting the precursor powder at the temperature of 700-1100 DEG C under a certain atmosphere for 0.5-2 hours. Graphite / iron carbide, graphite / iron or graphite / iron carbide / iron can be obtained respectively by regulating process parameters. The production method is simple in process, low in cost and easy for industrial production, and the obtained graphite / iron carbide / iron nanocomposite with the size less than 50nm is good in dispersibility and high in saturation magnetization.
Owner:UNIV OF SCI & TECH BEIJING

Synthesis method for metal organic framework material MIL-53 (Al)

The present invention belongs to the technical field of preparation of metal organic framework materials, particularly relating to a synthesis method for a metal organic framework material MIL-53 (Al) coordinated with aromatic organic carboxylic acid and aluminum. The structural formula of the metal organic framework material MIL-53 (Al) is Al (OH) [O2C-C6H4-CO2]. The method comprises the following steps: taking aluminum hydroxide and terephthalic acid as raw materials and acid as an auxiliary; preparing MIL-53 (Al) by a hydrothermal method; and activating at high temperature to obtain the metal organic framework MIL-53 (Al) with open channels. According to the method provided by the present invention, a water-insoluble metallic aluminum source is used as a precursor, and an acid auxiliary is used cooperatively; and compared with the existing synthesis method, the method has the advantages of low raw material cost, relatively mild conditions, energy conservation and environment protection and the like, solves the existing problem in a current MIL-53 (Al) synthesis process, and has a potential industrial production prospect.
Owner:TONGJI UNIV

Method for low-temperature preparation of pure phase oxide material

The invention relates to a method for preparing pure phase oxide at low temperature, belonging to the material preparation technical field. The inventive method referrs the chemical formual of ABM<1-x>O3, (x=0.50-1.0), to dissolve the nitrates of cerium, zirconium, titanium or gallium into water, and slowly add the carbonate, oxalate, nitrate, acetate, basic hydroxide, hydroxide or oxide of calcium, barium, strontium, lead or lanthanide metal element into the solution to be dissolved completely, heats and mixes precursor solution in water bath or oil bath at 50-100DEG C, until the solution changes to gel, and reacts the gel at 1000DEG C for 2-10h, to obtain oxide materials of pure phase and high crystallinity. The method for preparing pure phase oxide at low temperature has simple process, easy operation, low cost, high product purity and easily accessible industrial production.
Owner:SHANGHAI INST OF CERAMIC CHEM & TECH CHINESE ACAD OF SCI

Borate matrix fluorescent powder for white-light LED and preparation method of borate matrix fluorescent powder

The invention discloses borate matrix fluorescent powder for white-light LED and a preparation method of the borate matrix fluorescent powder. The preparation method is characterized in that NaSr1-x-y-zCexSmyTbzBO3 single matrix fluorescent powder is prepared by a high temperature solid phase method, 0<=x<=0.10, 0<=y<=0.40, 0<=z<=0.40, and the raw materials used by the preparation method are high-purity Na2CO3, SrCO3, H3BO3, CeO2, Tb4O7 and Sm2O3. The fluorescent powder can emit white light under ultraviolet excitation, and the purity of white light can be regulated by regulating doping Ce<3+>, Sm<3+> and Tb<3+> ion concentration. The borate matrix fluorescent powder and the preparation method have the advantages that the preparation method is simple in process and low in synthesizing reaction temperature, the chromaticity coordinates of the prepared NaSrBO3:Ce,Sm,Tb fluorescent powder can be regulated by regulating the doping concentration of the Ce<3+>, the Tb<3+> and the Sm<3+>, and the fluorescent powder is high in light emitting efficiency, good in thermal stability and promising in application prospect in white-light LED under ultraviolet excitation.
Owner:FUJIAN INST OF RES ON THE STRUCTURE OF MATTER CHINESE ACAD OF SCI

Process for synthesizing silicane coupling agent KII 560 at low temp.

The present invention discloses low temperature process of synthesizing silane coupler KH-560. The process adopts anhydrous methanol as activating material, and low temperature synthesizing catalyst of alcohol solution of chloroplatinic acid compounded with chloroplatinic acid isopropyl alcohol and acetylacetone, so that it has low synthesis temperature, 65-80 deg.c, of allyl diglycidyl ether and trimethoxyl silane. The present invention has low power consumption, effective separation between high boiling point matter and low boiling point matter, low production cost and high product purity and yield.
Owner:樊福定

Low temperature synthesis method for graphite fluoride

The invention discloses a low temperature synthesis method for graphite fluoride. The method includes: reacting graphite with antimony pentachloride at 300-400DEG C for 7h to prepare an antimony pentachloride graphite intercalation compound; and introducing a fluorine-nitrogen mixed gas into the reactor to carry out reaction for 5-10h, with the fluorine accounting for 12%-15% of the total volume of the fluorine-nitrogen mixed gas. The graphite fluoride synthesis reaction temperature is far below its decomposition temperature, thus avoiding the potential danger of explosion. Graphite fluoride can form in ordinary fluorination equipment, the reaction temperature control range is large and is easy to control. The production cost is low, and the output rate is high.
Owner:QINGDAO TAIHAODA CARBON MATERIAL

Vitamin B12 group containing amphiphilic sodium alginate derivative and preparation method and application thereof

The invention discloses a vitamin B12 group containing amphiphilic sodium alginate derivative and a preparation method and application thereof. Particularly, the derivative is an amphiphilic sodium alginate derivative containing a vitamin B12 group and a cholesteryl group. The derivative has a compound structure formula represented by a formula (I) shown in the description. The vitamin B12 group containing amphiphilic sodium alginate derivative (VB12-CSAD) is prepared through subjecting a cholesteryl containing amphiphilic alginic acid derivative (CSAD) to a reaction with vitamin B12. The reaction conditions of synthesis of the VB12-CSAD are mild, and thus, the maintaining of bioactivity of the vitamin B12 is facilitated; the VB12-CSAD is high in stability in a digestive tract system; thesmall-intestine targeted absorption performance is high, so that the vitamin B12 group containing amphiphilic sodium alginate derivative is advantageously used as an oral-application nano-preparationfor small-intestine targeted absorption and has a relatively good application prospect in the aspect of improving safety and bioavailability of oral application drugs.
Owner:SUN YAT SEN UNIV +1

Preparation method of chromium carbide/carbon nano composite material with mesoporous structure

ActiveCN105752984AHigh reactivityAchieve mixed contactDispersityChromium carbide
The invention relates to a preparation method of a chromium carbide / carbon nano composite material with a mesoporous structure and belongs to the technical field of composite material preparation.The preparation method includes: (1), mixing chromium source, glycine and additives (carbon source, ammonium nitrate and the like) according to a certain proportion to form a solution; (2), heating while stirring, and decomposing after volatilizing and concentrating the solution to obtain precursor powder; (3), subjecting the precursor powder to reaction for 0.5-2 h within a temperature range of 700-1200 DEG C in certain protection atmosphere.The preparation method is simple in process, low in cost and easy for industrial production, and the chromium carbide / carbon nano composite material obtained by the method is uniform in particle distribution and high in dispersity.
Owner:UNIV OF SCI & TECH BEIJING

Solvent-free method for preparing 1,3-propane sultone

The invention discloses a solvent-free method for preparing 11,3-propane sultone. According to the method, propenol and ammonium sulfite are used as reaction raw materials; and deionized water is adopted as medium. The preparation method comprises the following steps: stirring ammonium sulfate and deionized water; at 20-50 DEG C, preparing a mixed solution from acrolein, an initiator and deionizedwater, dropwise adding the mixed solution into a beaker, and carrying out catalytic reaction to generate an aqueous solution of 3-hydroxypropylammonium sulfonate; adding calcium hydroxide to carry out alkalization reaction, after alkalization is completed, adding concentrated sulfuric acid for acidification treatment to obtain 3-hydroxypropanesulfonic acid and solid calcium sulfate, and performing filtration to obtain an aqueous solution of the 3-hydroxypropanesulfonic acid; carrying out concentration and reduced pressure rectification to obtain a target product; adding a certain amount of calcium hydroxide and water into kettle residues, performing hydrolysis to obtain an aqueous solution of calcium 3-hydroxypropanesulfonate, adding concentrated sulfuric acid for acidification treatment,performing filtration to obtain an aqueous solution of 3-hydroxypropanesulfonic acid, and carrying out concentration and reduced pressure rectification to obtain the target product. The method has the advantages of simple process, simple raw materials, no solvent and no waste, and the yield can reach 95%.
Owner:江苏瀚康新材料有限公司

Preparation method of nano chromium carbide powder

The invention relates to a preparation method of nano chromium carbide powder, which belongs to the technical field of nano powder preparation. The process is as follows: (1) make a solution of chromium nitrate, glycine and carbon source according to a certain ratio; (2) heat and stir, the solution is volatilized, concentrated and then decomposed to obtain the precursor powder; (3) the precursor powder is heated at 600 Within the temperature range of ~1000°C, react in a certain protective atmosphere for 0.5-3 hours. The invention has the advantages of simple process, low cost and easy industrial production, and the particle size of the obtained chromium carbide powder is less than 100nm, and the dispersibility is good.
Owner:UNIV OF SCI & TECH BEIJING

Branched polymer-urea-glyoxal copolycondensation resin as well as preparation method and application thereof

The invention provides a branched polymer-urea-glyoxal copolycondensation resin and a preparation method thereof, and the preparation method comprises the following steps: 1, carrying out grafting reaction on branched polyethyleneimine and urea to obtain a grafted modified branched polyethyleneimine polymerization product marked as HPEIU-1800; 2, mixing a glyoxal aqueous solution with urea, adjusting the pH value to 7.5-8.0, carrying out a heating and thermal insulation reaction, adding the HPEIU-1800 synthesized in the step 1, and continuing the heating and thermal insulation reaction to obtain a target product. Due to the introduction of the branched polymer, the obtained resin has excellent bonding strength and water resistance. And no formaldehyde or organic solvent is used as synthetic raw materials, so the resin does not release formaldehyde and has excellent environmental protection property. The invention also provides an application of the resin in a wood adhesive.
Owner:SOUTHWEST FORESTRY UNIVERSITY

Production method of nanometer iron carbide powder

The invention relates to a preparation method of nanometer iron carbide powder and belongs to the technical field of preparation of nanometer powder. The preparation method comprises the following technological steps: (1) mixing ferric nitrate, glycine and a carbon source at a certain ratio to form a solution; (2) heating, stirring, volatilizing, concentrating and decomposing the solution to obtain precursor powder; and (3) allowing the precursor powder to react for 0.5-3 hours in a certain atmosphere at the temperature of 500 to 800 DEG C. The preparation method disclosed by the invention is simple in process, low in cost and easy for industrial production, and the obtained iron carbide powder particles are smaller than 30nm in particle size and good in dispersity.
Owner:UNIV OF SCI & TECH BEIJING

Preparation method of resorcinol formaldehyde resin for modified rubber adhesive

The invention discloses a preparation method of a resorcinol formaldehyde resin for a modified rubber adhesive, which comprises the following steps: a) adding p-alkylphenol and polyformaldehyde into an organic solvent, and stirring uniformly at 40-70 DEG C; b) dropwisely adding an alkali solution, and keeping the temperature for 1-4 hours; c) heating the product obtained in the step b) to 80-100 DEG C, keeping the temperature for 2-4 hours, and cooling to 90 DEG C below; d) adding an acidity regulator into the product obtained in the step c), stirring, adding resorcinol, heating to 100-150 DEG C, and reacting under reflux for 2-5 hours; and e) removing the organic solvent from the product obtained in the step b), and starting granulation when the softening point of the product is 99-109 DEG C to obtain the granular resorcinol formaldehyde resin. The method uses polyformaldehyde instead of the formalin, and has the advantages of simple material feeding and lower risk.
Owner:SHANGHAI LUCKY BIOLOGICAL & CHEM TECH +1

Preparation method of 4-octylphenethyl alcohol

The invention relates to the technical field of preparation of 4-octylphenethyl alcohol, in particular to a preparation method of 4-octylphenethyl alcohol. The method comprises the following operationsteps of 1, synthesizing a Grignard reagent R1-Mg-X1, wherein R1 is octyl, X1 is halogen (Cl, Br or I), and R1-X1 and magnesium powder react in anhydrous ether or tetrahydrofuran (THF) to prepare theGrignard reagent R1-Mg-X1; and 2, carrying out an alkylation reaction on R2-CH2-X2 and the R1-Mg-X1 to obtain R2-CH2-R1 and X1-Mg-X2, wherein R2 is phenethyl alcohol, X2 is halogen (Cl, Br or I), andR2-CH2-R1 is the product 4-octylphenethyl alcohol. The specific technological process is as follows: R2-CH2-X2 + R1-Mg-X1-R2-CH2-R1 + X1-Mg-X2, wherein R1 is octyl, X1 is halogen (Cl, Br or I), R2 isphenethyl alcohol, and X2 is halogen (Cl, Br or I). The method has the advantages of few byproducts, high yield, low cost and relatively low synthesis reaction temperature, is beneficial to industrial production, has low environmental pollution, and implements green production.
Owner:南京康德祥医药科技有限公司

Low-temperature synthesis method of polyfluorocarbon

InactiveCN109721052AReduce the synthesis reaction temperatureWide range of reaction temperature controlGraphiteDecompositionAntimony pentachloride
The invention discloses a low-temperature synthesis method of polyfluorocarbon. The low-temperature synthesis method comprises the steps: reacting graphite with antimony pentachloride to prepare an antimony pentachloride graphite intercalation compound, wherein the reaction temperature is 300-400 DEG C, and the reaction time is 7 h; and introducing a fluorine-helium mixed gas to a reactor, and carrying out a reaction for 5-10 h, wherein fluorine in the fluorine-helium mixed gas accounts for 12%-15% of the total volume of the mixed gas. The synthesis reaction temperature of polyfluorocarbon isfar lower than the decomposition temperature of polyfluorocarbon, so that potential explosion hazards are avoided; polyfluorocarbon can be formed in common fluorination equipment, the control range ofthe reaction temperature is relatively wide, and the reaction temperature is easy to control; and the production cost is relatively low, and the yield is relatively high.
Owner:李倩

Preparing process of propane diamide compound

The present invention provides the preparation process of propane diamide compound. The propane diamide compound is prepared through adding malonic acid, amine and solvent, heating to 60-65 deg.c dropping phosphor trichloride and reaction at the said temperature for 1.5-2 hr. The general reaction expression is 2RNH2+HOOCCH2COOH+PCl3-R-NHCOCH2COLNH-R+H3PO3+HCl. The preparation process of present invention has short reaction period, low reaction temperature and high yield. The propane diamide compound product can be used to release compound parent substance for development inhibitor and development promoter.
Owner:CHINA LUCKY FILM CORP

A kind of preparation method of aluminum nitride/boron nitride composite ceramic powder

The invention discloses a preparation method of aluminum nitride / boron nitride composite ceramic powder, and belongs to the technical field of preparation of ceramic powder. The preparation method comprises the following specific steps of with aluminum source, boron source, amine organism, waters soluble carbon source and assistant agent as raw materials, preparing a solution according to a certain ratio, heating and stirring, volatilizing and concentrating the solution, and reacting to obtain precursor powders; reacting the precursor powders for 2-4h in a flowing nitrogen atmosphere at 1300-1700 DEG C, heating the reacted powders for 1-3h in air at 500-650 DEG C so as to obtain the aluminum nitride / boron nitride composite ceramic powder. The preparation method is applicable for synthesizing high-purity high-dispersion and high fine granularity under a lower reaction temperature condition, the operation is simple, the cost is low, and the industrial production is prompted.
Owner:UNIV OF SCI & TECH BEIJING
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