Patents
Literature
Hiro is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Hiro

30results about How to "Raise the sodium content" patented technology

Method for preparing prussian blue material through composite reduction of graphene oxide, and application

The invention relates to a method for preparing a prussian blue material through reduction of graphene oxide, and application. The preparation method comprises the steps of ultrasonically dispersing the graphene oxide into a sodium ferrocyanide water solution, adding ascorbic acid for resisting oxidation, adding sodium citrate for reducing a reaction rate, dropwise adding hydrochloric acid for adjusting the solution to be acidic, heating and stirring for reacting under the inert gas protection to obtain a material, washing, vacuum drying, and carrying out microwave irradiation for reducing thegraphene oxide to obtain the product. When the prussian blue material prepared through composite reduction of the graphene oxide provided by the invention is used as a sodium-ion battery anode, the specific capacity, the cycle performance and the rate capability of a battery are greatly improved, the charge and discharge specific capacity of the battery in an organic system reaches up to not lessthan 153mAh.g<-1>, and the specific capacity of the battery in a water system single platform reaches up to not less than 81mAh.g<-1>; the preparation method is low in cost, fast, simple, and favorable in application prospect.
Owner:HARBIN INST OF TECH SHENZHEN GRADUATE SCHOOL

Method for preferentially extracting lithium and recycling valuable metals from waste ternary lithium ion battery positive electrode materials

The invention discloses a method for preferentially extracting lithium and recycling valuable metals from waste ternary lithium ion battery positive electrode materials. The method comprises the following steps that the positive electrode material obtained by disassembling, crushing and separating the waste lithium ion battery is uniformly mixed with concentrated sulfuric acid, roasting is carried out at the temperature of between 400 and 600 DEG C, leaching is carried out a roasted product by using pure water and a dilute alkali solution, lithium-containing aqueous solution is obtained, and a Li<2>CO<3> or a lithium hydroxide product is prepared after impurity removal; and the valuable elements such as cobalt, nickel and manganese in water leaching residues are leached out through a reduction acid leaching method, and corresponding compound products are prepared after impurity removal, extraction and purification. The method is simple in process, short in flow, low in reagent cost and capable of efficiently recycling valuable metal elements such as lithium, cobalt, nickel and manganese in the waste ternary lithium ion battery material.
Owner:JINCHUAN GROUP LIMITED +1

Combustion method and device for preventing combustion coking and contamination of high-sodium coal

The invention relates to a combustion method and device for preventing combustion coking and contamination of high-sodium coal. An outlet of a fluidized bed is connected with an inlet of a cyclone separator, one outlet of the cyclone separator is connected with one inlet of a coal mill through a heat exchanger and a dust remover, the other outlet of the cyclone separator is connected with one inlet of a coke preprocessing device, an outlet of the coal mill is connected with the other inlet of the coke preprocessing device through a three-grade pyrolysis bed, an outlet of the coke preprocessing device is connected with an inlet of a turbulent burner on the fluidized bed, and a forced draught fan is respectively connected with a primary air inlet in the bottom of the fluidized bed and a secondary air inlet in the middle of the fluidized bed. According to the combustion method and device, a common pyrolysis device is replaced by the three-stage fluidized bed, pyrolysis gas sodium-removal purification devices are connected behind the three stages of the three-grade pyrolysis bed respectively, the problem that alkali metal sodium elements are transformed between forms in the pyrolysis process and can not be effectively removed can be effectively solved, the problem that coke can not be easily and effectively combusted in a common pulverized coal furnace can be well solved, and energy can be effectively used.
Owner:UNIV OF SHANGHAI FOR SCI & TECH

Positive electrode material for sodium phase rich sodium-ion batteries and preparation method and application thereof

The invention belongs to the technical field of sodium-ion battery materials, and specifically discloses a positive electrode material for sodium phase rich sodium-ion batteries which is a composite material of sodium phase rich titanium-manganese-sodium phosphate and carbon; and the chemical formula of the sodium phase rich titanium-manganese-sodium phosphate is Na3+4xMnTi1-x(PO4)3, wherein x isgreater than 0 and smaller than or equal to 0.3. The invention also discloses preparation of the composite material and application thereof in the sodium-ion batteries. According to the composite material, the sodium phase rich titanium-manganese-sodium phosphate is creatively adopted, and the content of sodium in the material is improved through an appropriate proportion of titanium defect. Redundant sodium content in the character is beneficial for maintaining the stability of the structure in the process that sodium ions are taken out, and then the long cycling stability of the material ispromoted. Moreover, the sodium phase rich titanium-manganese-sodium phosphate is cooperative with carbon, so that the electrical properties, such as capacity and cycle performance, of the obtained composite material can be promoted obviously. Moreover, the system of Na-Mn-Ti-P-O is rich in resources and low in cost, and the preparation method is simple in operation and wide in commercial application prospects.
Owner:湖南钠邦新能源有限公司

Method for preparing mesoporous molecular sieve with high aluminum content under neutral condition

The invention discloses a method for preparing a mesoporous molecular sieve with high aluminum content under a neutral condition. The method comprises the following steps: (1) dissolving a template agent; (2) mixing a silicon source, potassium persulfate, sodium chloride and water to prepare a silicate solution; (3) dropwise adding the silicate solution into the template solution to generate a gel system; and (4) performing crystallization, suction filtration, drying and calcination on the initial mesoporous molecular sieve gel to obtain the mesoporous molecular sieve. The preparation method comprises the following steps: adding potassium persulfate and sodium chloride into an aqueous solution containing a silicon source for hydrolysis, then uniformly mixing with a nonionic surfactant solution, adding an aluminum source, and initiating a free radical reaction by using hydroxyl free radicals generated by the potassium persulfate, so as to obtain the silicon-based surfactant. According to the invention, the sodium salt is added into the template agent, so that the charge matching effect between the template agent and the inorganic silicon source and the self-assembly process under the neutral condition are facilitated, and the sodium content and acidity of the molecular sieve product are greatly improved due to the existence of the sodium salt, so that the preparation of the mesoporous molecular sieve with high aluminum content and strong acidity is realized.
Owner:BEIJING UNIV OF CHEM TECH +3

Hemihydrate gypsum base material imitation stone floor and preparation method thereof

The invention relates to the technical field of chemical building materials, in particular to a hemihydrate gypsum base material imitation stone floor and a preparation method thereof. By properly proportioning hemihydrate gypsum, bamboo carbon fibers, cement, calcite powder, polyvinyl alcohol, methylcellulose, ethylcellulose and imitation stone paint, the hemihydrate gypsum is further activated in an environment with the cement, and the activity of the hemihydrate gypsum is improved; moreover, through the addition of polyvinyl alcohol, methylcellulose, ethylcellulose, the bamboo carbon fibers and the calcite powder, the strength and toughness of a base material of a product made from the hemihydrate gypsum are enhanced, characteristics of heat retaining property and light weight of the hemihydrate gypsum also can be reserved, the radioactivity of the hemihydrate gypsum product is also reduced, and the product quality is improved.
Owner:GUIZHOU KAILIN GRP CO LTD

Preparation method of sodium manganese oxide and application of sodium manganese oxide in super capacitor

The invention relates to a preparation method of a sodium manganese oxide and an application of the sodium manganese oxide in a super capacitor. The preparation method comprises the steps of firstly, employing a coprecipitation method to mix a divalent manganese salt and a sodium hydroxide solution to form a Mn (OH) 2 suspension, and then carrying out washing-solid-liquid separation for several times to obtain Mn (OH) 2 precipitate powder; and grinding the precipitate and sodium hydroxide, sintering in an argon atmosphere at 300-900 DEG C to obtain a product, cooling to room temperature, taking out the product, washing with water for several times, and drying in a vacuum drying oven to obtain the manganese oxide doped with high sodium content. The prepared sodium manganese oxide is prepared into an electrode to form an asymmetric water system supercapacitor together with an activated carbon electrode, so that the electrochemical performance of the device is favorably improved. The sodium manganese oxide prepared by the method is low in cost, has the advantages of high specific capacitance, wide charge-discharge voltage window, long cycle service life and the like in an aqueous electrolyte, is simple in preparation process, and can realize macro-scale preparation.
Owner:NANCHANG UNIV

Combustion method and device for preventing high-sodium coal from coking and contamination

The invention relates to a combustion method and device for preventing coking and contamination of high-sodium coal. The outlet of the fluidized bed is connected to the inlet of the cyclone separator, and one outlet of the cyclone separator is connected to pulverized coal through a heat exchanger and a dust collector. One inlet of the mill, and the other outlet is connected to an inlet of the coke pretreatment device; the outlet of the coal mill is connected to the other inlet of the coke pretreatment device through a three-stage pyrolysis bed, and the outlet of the coke pretreatment device is connected to all the coke pretreatment devices on the fluidized bed The inlet of the above-mentioned swirl burner is connected; the blower is respectively connected with the primary air inlet at the bottom of the fluidized bed and the secondary air inlet in the middle. The present invention uses three-stage pyrolysis beds to replace common pyrolysis devices, and a pyrolysis gas desodium purification device is connected behind each stage of pyrolysis beds, which can effectively solve the problem of alkali metal sodium in various forms during the pyrolysis process. The problem that coke cannot be effectively removed due to mutual conversion can not only solve the problem that coke is difficult to burn effectively in ordinary pulverized coal furnaces, but also realize the effective utilization of energy.
Owner:UNIV OF SHANGHAI FOR SCI & TECH

A kind of positive electrode material of sodium-rich phase sodium-ion battery and its preparation and application

The invention belongs to the technical field of sodium-ion battery materials, and specifically discloses a sodium-rich phase sodium-ion battery cathode composite material, which is a composite material of sodium-rich phase sodium titanomanganese phosphate and carbon, and the chemical formula of the sodium-rich phase sodium titanomanganese phosphate is Na 3+4x MnTi 1‑x (PO 4 ) 3 , where 0<x≤0.3. The invention also discloses the preparation of the composite material and its application in sodium ion batteries. The composite material of the present invention innovatively adopts the sodium-rich titanium manganese phosphate sodium, which increases the sodium content in the material through the appropriate proportion of titanium defects. The excess sodium content in the lattice is conducive to maintaining the stability of the structure during the extraction of sodium ions, thereby improving the long-term cycle stability of the material. In addition, the synergy between the sodium-rich phase sodium titanomanganese phosphate and carbon can significantly improve the electrical properties of the composite material, such as improving the capacity and cycle performance of the composite material. In addition, the "Na‑Mn‑Ti‑P‑O" system is rich in resources and low in cost, and the preparation method is simple to operate and has broad prospects for commercial application.
Owner:湖南钠邦新能源有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products