The application discloses a preparation method of high-entropy MAX phase modified high-strength high-
conductivity copper, and belongs to the technical field of
metal matrix
composite material preparation. The preparation method comprises the following steps:
raw material pretreatment, ball milling mixing,
calcination reduction, SPS
sintering, cooling forming and aging treatment. In the ball milling process,
argon protection is adopted to avoid
powder oxidation. The
powder surface is purified through
calcination reduction, and the oxidation impurities of the
powder are removed. In the SPS
sintering, a two-stage heating process is adopted, that is, the
sintering stress is eliminated at 600 DEG C, and then the densification is realized by being heated to 900 DEG C, so that the sintering quality is guaranteed, and the grain coarsening and modified phase growth are inhibited. After the sintering, the bulk
composite material is placed in a heat treatment furnace, and is kept at 500 DEG C for 2 hours, and then is rapidly water quenched after the aging treatment is finished, so that the Cr2Nb strengthening phase in the matrix is uniformly dispersed and precipitated, the precipitated phase coarsening is inhibited, and a double strengthening
system is formed with the high-entropy MAX phase.