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481results about How to "Raise the crystallization temperature" patented technology

Method for synthesizing acyl naphthalene by using micro-channel reactor

The invention discloses a method for synthesizing acyl naphthalene by using a micro-channel reactor. The method comprises the following steps: (1) preparing acylation liquid, namely adding nitrobenzene and anhydrous aluminum chloride into a reactor in a low-temperature tank, finally adding acyl chloride, and controlling the temperature in the reactor to be 0-3 DEG C; (2) preparing a feed solution,namely adding nitrobenzene and 2-methyl naphthalene into a reactor provided with a stirrer; (3) reacting, namely injecting the feed solution and the acylation liquid into a micro mixer to be mixed, and feeding into the micro-channel reactor to be reacted; (4) washing, namely enabling the product discharged from the micro-channel reactor to enter the micro mixer again so as to be washed, enablingthe mixture into the micro-channel reactor, controlling the reactor temperature to 40-50 DEG C, and performing ultrasonic oscillation outside the reactor; (5) performing reduced pressure distillation,namely separating the products obtained in the step (4), and performing vacuum decompression to 500-1000Pa so as to obtain a crude product 2-methyl-6-acyl naphthalene; and (6) recrystallizing, namelyadding the crude product obtained in the step (5) into a solvent of 50-60 DEG C, stirring and dissolving, naturally cooling and crystallizing, continuously cooling and crystallizing in an ice-water bath, and finally filtering to obtain the purified product 2-methyl-6-acyl naphthalene.
Owner:BEIJING INSTITUTE OF PETROCHEMICAL TECHNOLOGY +1

Nucleating additive formulations of bicyclo[2.2.1]heptane dicarboxylate salts

Milled, small particle size, solid bicyclo[2.2.1]heptane dicarboxylate salt-containing thermoplastic nucleating additive formulations further comprising at least one anticaking agent for improved haze reduction, improved nucleation performance, and prevention of potential cementation (via agglomeration) of the salt component present therein are provided. Such small particle size dicarboxylate salts provide desirable properties within thermoplastic articles, particularly as nucleating agents, but apparently suffer from certain clarity issues and agglomeration problems (due to the flat and thin plate structures of such compounds and the propensity they exhibit to cohere to each other during storage), making utilization thereof less desirable for certain applications. Thus, an improvement has been provided to permit full benefit of the excellent crystallization temperatures, stiffness, and calcium stearate compatibility such dicarboxylate salts accord within target low haze thermoplastics. Furthermore, unexpected improvements in dusting reduction have been found upon the utilization of such anticaking additives in combination with the aforementioned nucleating salts. Thermoplastic additive compositions and methods of producing thermoplastics with such nucleator / anticaking additive combinations are also contemplated within this invention.
Owner:MILLIKEN & CO

Tank furnace for producing basalt continuous fiber

The invention relates to a tank furnace for producing basalt continuous filament and pertains to the technical field of novel inorganic non-metallic material processing equipment, the main characteristics are that the furnace body consists of a melting tank and material channels, the melting tank and the material channels are connected by non-submerged dog-holes, the melting tank is divided into a melting area and a homogenization area, a burner is arranged at the top of the furnace vertically, the burner guns of melting area and the feeding pipes are arranged in intervals, and the strong melting area of even feeding and even heating is formed. The material channels are arranged in three directions in the homogenization area of the melting tank, burner guns are arranged in the material channel in sections, the temperature of the fused mass in the material channels is guaranteed, more than 12 wiredrawing shaping areas are evenly arranged in each material channel so as to supply basalt melt mass for the wiredrawing bushing well, emptying devices are arranged at the tail part of the melting tank and the tail parts of all material channels, during the operation, the operation of discharging the meltwater can be carried out when impurities are stored in the meltwater for a long time or the varieties of raw materials are changed. The invention is in favor of improving the quality and industrialized production of the basalt continuous filament.
Owner:江苏天龙玄武岩连续纤维股份有限公司

Novel casting powder and application thereof

The invention relates to novel casting powder and application thereof, and belongs to the technical field of steel continuous casting powder. The casting powder comprises the following components according to mass percentage, 30-33% of CaO, 28-34% of SiO2, 2-5% of Al2O3, 1-3% of MgO, 12-16% of (Na2O+Li2O), 1-6% of B2O3, and 11-14% of F-. The casting powder has the characteristics of low melting point (950 to 1,050 DEG C), low viscosity (the viscosity is 0.06 to 0.10Pa.s at the temperature of 1,300 DEG C), high crystallization temperature (1,215 to 1,302 DEG C) and the like. The casting power designed by the invention is suitable for the continuous casting of high-carbon chromium-containing steel of which the mass percentage of C is 1.3-1.8% and the mass percentage of Cr is 10-15%. When the casting powder is applied to the continuous casting production of a high-carbon chromium-containing steel slab, Cr2O3 and other impurities with a high melting point in a crystallizer can be effectively absorbed, the infiltration capability of the casting powder is improved, and the slow cooling of a meniscus is implemented, so that the objectives of increasing the lubricating of a casting blank, controlling the heat transferring at the meniscus, reducing the cracking and inclusion of the casting blank and improving the quality of the casting blank are achieved.
Owner:CENT SOUTH UNIV

Sb-Te-Ti phase-change storage material and Ti-Sb2Te phase-change storage material

The invention relates to a Sb-Te-Ti phase-change thin-film material capable of being used for a phase-change memory, and preparation and application of the Sb-Te-Ti phase-change thin-film material. The novel Sb-Te-Ti phase-change storage material is prepared by doping Ti into a Sb-Te phase-change material, the doped Ti forms bonds with both Sb and Te, and the chemical general formula of the Sb-Te-Ti phase-change storage material is SbxTeyTi100-x-y, wherein x is more than 0 and less than 80, and y is more than 0 and less than 100-x. When the phase-change storage material is a Ti-Sb2Te phase-change storage material, a Ti atom replaces a Sb atom without phase separation. The grain growth is dominant in the crystallization process of the conventional Sb-Te phase-change material, so that the phase change rate is high, but the retention cannot meet industrial requirements. The crystallization temperature of the novel Sb-Te-Ti phase-change storage material is greatly raised, the retention is promoted, and the thermal stability is enhanced; simultaneously, the non-crystalline state resistance is reduced and the crystalline state resistance is increased; and the novel Sb-Te-Ti phase-change storage material can be widely applied to the phase-change memory.
Owner:SHANGHAI INST OF MICROSYSTEM & INFORMATION TECH CHINESE ACAD OF SCI
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