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32results about How to "Reduce grain boundary defects" patented technology

Manufacturing method of polycrystalline silicon layer and polycrystalline silicon thin film transistor and manufacturing method thereof

The invention discloses a manufacturing method of a polycrystalline silicon layer and a polycrystalline silicon thin film transistor and a manufacturing method thereof, and relates to the field of displaying. According to the manufacturing methods, a crystallization rate of a formed polycrystalline silicon layer is high, crystalline grains are uniform, crystal boundary defects are little, thus electrics properties of the polycrystalline silicon thin film transistor can be improved, and reliability of the polycrystalline silicon thin film transistor is improved. The manufacturing method of the polycrystalline silicon layer includes the steps that a substrate is provided; a barrier layer and a buffer layer are sequentially formed on the substrate; multiple groves are arranged in the buffer layer through a picture composition process, and seed crystals are formed on the buffer layer; an amorphous silicon layer is formed on the buffer layer provided with the grooves and the seed crystals; and the amorphous silicon layer is converted into the polycrystalline silicon layer through adoption of a heating processing process. The manufacturing method of the polycrystalline silicon layer and the polycrystalline silicon thin film transistor and the manufacturing method of the polycrystalline silicon thin film transistor are used for improving quality of polycrystalline silicon films.
Owner:BOE TECH GRP CO LTD +1

Large grain organic and inorganic hybrid perovskite film preparation method

ActiveCN106159088AEasy to controlEasy preparation of controlled substrate temperatureSolid-state devicesSemiconductor/solid-state device manufacturingHysteresisSolar battery
The invention discloses a large grain organic and inorganic hybrid perovskite film preparation method, belonging to the perovskite type solar battery and correlated photoelectric semiconducting material field, and can prepare a uniform and compact large grain film through the steps of configuration of an organic and inorganic hybrid perovskite precursor solution, stirring and heating, spin coating, annealing, etc. The method requires no spin coating in a multistep approach, ca easily control the temperature of a room temperature substrate, has no strict requirements on an annealing and cooling rate, and can manufacture a film efficiently. The method realizes virtual grain film growth through adjusting the grain dimension of a perovskite light-absorption layer, thereby reducing grain inner defects, and increasing the carrier transport efficiency; in addition, the method controls grain boundary defects, greatly improves perovskite crystal film environment stability, and enhances perovskite thin-film device performances. A perovskite type virtual monocrystalline film prepared in the low temperature solution method can assemble hysteresis free, efficient and stable perovskite type solar batteries and correlated film transistor, electroluminescent and laser emission photoelectric semiconductor devices.
Owner:NANJING UNIV OF TECH

Manufacturing method for alloys with excellent durability performance under high temperature and high pressure conditions

The invention provides a manufacturing method for alloys with excellent durability performance under high temperature and high pressure conditions. The manufacturing method for the alloys with the excellent durability performance under the high temperature and high pressure conditions comprises the following steps of (1) raw material preparation, (2) vacuum smelting, (3) electroslag remelting, (4)forging, (5) heat treatment, and (6) durability performance testing, sampling, peeling, inspection, packaging and storage, wherein the step 2 comprises the steps of (2.1) charging, (2.2) melting, (2.3) refining, (2.4) pouring, and the manufacture of the alloys with the excellent durability performance under the high temperature and high pressure conditions is completed. On the one hand, the manufacturing method optimizes the design of alloy elements, moreover, the traditional vacuum degassing and desulphurization technology is combined, and the desulphurization and degassing effect of using Ni-Mg and rare earth is especially increased; and on the other hand, the heat treatment process of a Cr-Ni-Mo-W alloy is optimized, and high end Cr-Ni-Mo-W alloy steel with a lasting life of more than500 hours is successfully manufactured under the conditions of 815 DEG C high temperature and 110 MPa high pressure.
Owner:江苏汉青特种合金有限公司

Preparation method of polysilicon thin film material

The invention relates to the field of preparation of a polysilicon thin film material, especially to a preparation method of a polysilicon thin film material. The method comprises the following steps: depositing an amorphous silicon film and a metal aluminum film successively on a glass substrate by using a magnetron sputtering technology so as to obtain a composite thin film; and carrying out laser irradiation on the composite thin film and carrying out crystallization on the amorphous silicon film, thereby obtaining a polysilicon thin film material. When the amorphous silicon film and the metal aluminum film are successively deposited by using the magnetron sputtering technology, the temperature is not higher than 150 DEG C. According to the provided preparation method, the amorphous silicon film and the metal aluminum film are obtained by using the magnetron sputtering technology and no dangerous gas like silane is required; the highest temperature does not exceed 150 DEG C during the process of successive deposition of the amorphous silicon film and the metal aluminum film with the magnetron sputtering technology, so that the cheap glass substrate can be used; and the temperature of the polysilicon thin film preparation process is low, thereby substantially reducing the energy consumption.
Owner:CHINA UNIV OF GEOSCIENCES (BEIJING)

Preparation method for directional growth of tellurium-zinc-cadmium film on graphene substrate

The invention discloses a preparation method for directional growth of a tellurium-zinc-cadmium film on a graphene substrate. The preparation method comprises: preparing a single layer of graphene ona copper foil by using a CVD method, and preparing a layer of a directional tellurium-zinc-cadmium film by using the graphene as a substrate through a close-space sublimation method. According to thepresent invention, through the scheme for close-space sublimation preparation of the film by setting the distance between the substrate and the sublimation source, the graphene material is used as thesubstrate structure, and has the high lattice matching degree with the target CdZnTe film so as to prepare the CdZnTe film with good orientation; a purpose of the invention is to prepare the directional CdZnTe film on the graphene substrate by using the close-space sublimation method, such that the loss of the carrier transmission between the upper pole and the lower pole during the device preparation is low, the carrier transmission speed is improved, and the device transmission speed is improved; and compared to the CdZnTe single crystal growth process, the method of the invention has advantages of simplenes, lower cost, large area preparation, batch growth and high feasibility.
Owner:SHANGHAI UNIV

A kind of low-temperature rapid sintering soft ferrite and its preparation method

The invention discloses low-temperature rapidly sintered soft magnetic ferrite and a preparation method thereof. The preparation method comprises the following steps: S1, weighing the following components in parts by mole: 60-80 parts of ferric oxide, 40-60 parts of zinc oxide, 30-50 parts of copper oxide and 15-20 parts of manganese carbonate, and performing mixing ball-milling till the average particle size is 5-30 [mu]m so as to obtain mixed powder; S2, pre-sintering the mixed powder at 900-1000 DEG C so as to obtain a pre-sintered material; S3, weighing yttrium oxide, aluminum oxide and lithium carbonate as doping materials; S4, adding the doping materials weighed in the step S3 into the pre-sintered material, performing secondary ball-milling for 6-8 hours, drying, adding polyvinyl alcohol, and performing pelletizing so as to obtain a granular material; S5, heating the granular material to sintering temperature in the presence of an air atmosphere, and performing warm-keeping sintering, thereby obtaining the low-temperature rapidly sintered soft magnetic ferrite, wherein the sintering temperature meets the equation that T=1454 / [1g(X+2Y+Z)+t]. Due to mutual cooperation of the main material and the doping materials, a preparation process is optimized, the sintering temperature is reduced, and meanwhile the electromagnetic properties of the ferrite are ensured.
Owner:ZHONGDE ELECTRONICS

Polycrystalline silicon thin film manufacturing method

An embodiment of the invention discloses a polycrystalline silicon thin film manufacturing method. The polycrystalline silicon thin film manufacturing method comprises the steps: providing a first substrate, wherein the temperature resistance temperature of the first substrate is larger than or equal to 600 DEG C; forming a polycrystalline silicon thin film on the first substrate; and transferringthe formed polycrystalline silicon thin film to a glass substrate. According to the technical scheme provided by the invention, by forming the polycrystalline silicon thin film on the first substratewith higher temperature resistance, and then, transferring the formed polycrystalline silicon thin film onto the glass substrate, the problem that the manufacturing process of the polycrystalline silicon thin film is limited due to the temperature resistance of the glass substrate is avoided; and compared with a laser process adopted in the prior art, the method can allow crystal grains of the polycrystalline silicon thin film to reach a larger size, wherein crystal boundary defects of the polycrystalline silicon thin film with larger crystal grain size are fewer, so that the film forming quality of the formed polycrystalline silicon thin film and the electrical reliability of the polycrystalline silicon thin film are improved.
Owner:EVERDISPLAY OPTRONICS (SHANGHAI) CO LTD

Self-powered perovskite photoelectric detector and preparation method thereof

The invention belongs to the related technical field of micro-nano manufacturing. The invention discloses a self-powered perovskite photoelectric detector and a preparation method thereof. The photoelectric detector comprises a glass substrate, a CsPbIBr2 photosensitive film, a PMMA modification layer and an Ag electrode layer. The glass substrate comprises a substrate body and an ITO conductive layer arranged on the substrate body; the CsPbIBr2 photosensitive film is arranged on the ITO conductive layer; the PMMA modification layer is arranged on the surface, far away from the ITO conductivelayer, of the CsPbIBr2 photosensitive film; and the Ag electrode layer is arranged on the surface, far away from the CsPbIBr2 photosensitive film, of the PMMA modification layer. Compared with other perovskite photoelectric detectors, the perovskite photoelectric detector is lower in production cost and process complexity; and the introduction of the PMMA modification layer is beneficial to further passivating the defects of the CsPbIBr2 photosensitive film, improving the carrier transmission rate and reducing the adverse non-radiative recombination loss, thereby improving the sensitivity andresponse rate of the photoelectric detector.
Owner:HUAZHONG UNIV OF SCI & TECH

Jewel-like crystal based on animal skeletons and preparation method of jewel-like crystal

The invention relates to a jewel-like crystal based on animal skeletons and a preparation method of the jewel-like crystal. The preparation method comprises the following steps of burning animal skeletons into powder, then adding the powder into water, uniformly mixing, then adding an organic polymer monomer, a cross-linking agent, an initiator and a catalyst, and fully stirring to form slurry, injecting the slurry into a mold, enabling the organic polymer monomer to react, crosslink and polymerize to form polymer gel, and bonding and curing the particles in situ to form a green body, and carrying out high-temperature and high-pressure plasma-assisted sintering on the green body to obtain the jewel-like crystal. The technical means of material synthesis and crystal reconstruction are adopted, and the natural dead pet skeletons are subjected to atom recombination to form jewel-like crystals containing elements such as carbon, calcium, phosphorus, magnesium and oxygen; on the basis of the traditional hot pressing sintering technology, the plasma auxiliary sintering technology is combined, multi-field coupling of a thermal field, a force field and an electric field is achieved, energy needed by reaction is reduced, and the reaction rate and the production efficiency are improved.
Owner:福建省泉州市半岛建材有限公司

A preparation method of perovskite photovoltaic thin film based on double-effect seed growth method

The invention discloses a method for preparing a perovskite photovoltaic thin film based on a double-effect seed growth method, and belongs to the technical field of perovskite solar cells. The present invention adopts two-step deposition method to prepare perovskite photovoltaic film, by 2 Add CsPbX to the precursor solution 3 Seed crystals provide crystal nuclei for the growth process of perovskite photovoltaic thin films, and then the PbI 2 The FAI / MAI solution is deposited on the layer and heated and annealed to obtain a perovskite photovoltaic film. The invention effectively improves the crystallinity of the perovskite photovoltaic thin film, the crystal grains of the perovskite are significantly enlarged, and the short-circuit current, open-circuit voltage, filling factor and photoelectric conversion efficiency of the solar cell are significantly improved. Furthermore, since Cs + Ions were introduced into the perovskite photovoltaic film, and the light stability of the perovskite photovoltaic film was improved. The method is simple and practical, low in cost and easy to promote, and has great reference significance for improving the photovoltaic performance of perovskite photovoltaic thin films.
Owner:WUHAN UNIV

A thin film preparation method of a quasi-one-dimensional structure material with controllable orientation

The invention discloses a method for preparing a thin film of a quasi-one-dimensional structural material with controllable orientation. The method is based on a vertical evaporation tube furnace, and specifically includes the following steps: (1) placing the evaporation source material and the substrate to be deposited on the In the vertical evaporation tube furnace; (2) vacuum treatment, so that the vacuum degree of the vertical evaporation tube furnace remains at the preset vacuum degree and the fluctuation does not exceed ± 1Pa; (3) heat treatment in the heating zone, so that The evaporation source material is evaporated and deposited on the substrate to form a thin film; during the preparation process, the orientation of the formed quasi-one-dimensional material film can be controlled by controlling the parameters of the evaporation process. The present invention improves the key process parameters of the preparation method, adopts a vertical evaporation tube furnace with a specific structure for deposition, realizes the deposition and orientation control of a quasi-one-dimensional material film, and obtains a semiconductor film with a controllable orientation independent of the substrate , compared with the prior art, it can effectively solve the problem that the orientation of quasi-one-dimensional materials cannot be controlled.
Owner:HUAZHONG UNIV OF SCI & TECH +1

Preparation method of CZTS thin-film solar cell back electrode with modification layer

The invention provides a preparation method of a CZTS thin-film solar cell back electrode with a modification layer, and the method comprises the following steps: firstly, placing a Mo substrate under a vacuum condition, and carrying out the radio-frequency sputtering of ZnS, so as to form a first sputtering layer; secondly, under the vacuum condition, Cu is subjected to direct current sputtering, and a second sputtering layer is formed on the surface of the first sputtering layer; thirdly, spin-coating CZTS precursor sol on the surface of the second sputtering layer; and finally, carrying out annealing treatment under S steam. Wherein the first sputtering layer of the modification layer can be used as an S vapor barrier layer to inhibit vulcanization of the Mo layer and reduce the thickness of MoS2; and the second sputtering layer of the modification layer takes Cu as a raw material for direct current sputtering, so that the crystallization of an upper-layer CZTS precursor is facilitated, and the grain boundary defect of the CZTS is reduced. Besides, the modification layer can form a heavy p + type layer between the CZTS thin film on the upper layer and the Mo electrode on the lower layer, the carrier transmission performance of the contact side of the CZTS layer and the Mo back electrode is improved, and the photoelectric conversion efficiency of the solar cell device is further improved.
Owner:HUBEI UNIV OF TECH

A method for manufacturing an alloy with excellent durability under high temperature and high pressure conditions

The invention provides a method for manufacturing an alloy with excellent durability under high temperature and high pressure conditions, comprising the following steps: 1) raw material preparation; 2) vacuum smelting, including: 2.1) charging; 2.2) melting; 2.3) refining; 2.4) pouring ; 3) electroslag remelting; 4) forging; 5) heat treatment; 6) durability performance testing, sampling, peeling, inspection, packaging, storage, and completing the manufacture of alloys with excellent durability under high temperature and high pressure conditions. On the one hand, the manufacturing method optimizes the design of alloying elements; moreover, in combination with the above-mentioned traditional vacuum degassing and desulfurization technologies, the desulfurization and degassing effects of Ni-Mg and rare earth are especially increased; on the other hand, Cr-Ni-Mo is optimized. The heat treatment process of ‑W alloy successfully produced a high-end Cr‑Ni‑Mo‑W alloy steel with a durable life of more than 500 hours under the conditions of high temperature 815 °C and high pressure 110 MPa.
Owner:江苏汉青特种合金有限公司
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