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163results about How to "Impurities increase" patented technology

Process for producing carboxylic acid

A process for producing a purified carboxylic acid having “n+1” carbon atoms comprises feeding a carboxylic acid stream containing a carboxylic acid having “n+1” carbon atoms, a hydrogen halide, a lower boiling point (bp) component, a higher bp component, and others to a first distillation column; separating a lower bp fraction containing part of the lower bp component and a higher bp fraction containing part of the higher bp component in the first column; withdrawing a side stream containing at least the carboxylic acid by side cut from the first column; feeding the side stream to a second distillation column; separating a lower bp fraction containing part of the lower bp component and a higher bp fraction containing part of the higher bp component in the second column; and withdrawing a side stream containing the carboxylic acid by side cut from the second column to recover a purified carboxylic acid; and the process further comprises feeding at least one first component (A) selected from the group consisting of an alcohol, corresponding to the carboxylic acid, having “n” carbon atom(s), and an ester of the alcohol with the carboxylic acid to the first column, and if necessary water. Such a process ensures reduction of the concentration of the hydrogen halide in the purified carboxylic acid.
Owner:DAICEL CHEM IND LTD

Production process for directly-spun terylene industrial filament of liquid-phase tackifying fusant

The invention discloses a production process for a directly-spun terylene industrial filament of a liquid-phase tackifying fusant, belonging to the technical field of spinning. The production process includes the following steps: esterification, polycondensation, liquid-phase tackification and spinning. The production process is characterized in that: in a vertical reaction kettle, liquid-phase tackfication is carried out on the fusant obtained through esterification and polycondensation of glycol and phthalic acid; the vertical reaction kettle adopts a tower type film forming structure; the fusant enters the vertical reaction kettle from the top part for distribution, and the film forming is naturally finished under the action of gravity; a backflow pipeline is provided for the discharging of the reaction kettle, the viscosity and flow rate of the fusant are controlled by the backflow adjusting, the intrinsic viscosity of the polyester fusant after being tackified in a liquid-phase manner is within 0.85 to 1.0dl/g, and the fusant is conveyed to a spinning box body by a gear pump for spinning. By reasonably designing the reaction kettle and allocating the process, the invention effectively solves the consistency between the fusant reacting condition and the staying time; meanwhile, the consumption of a public medium is reduced, and the cost is lowered; by optimizing the process, the invention increases the production efficiency of a system and improves the product quality.
Owner:ZHEJIANG GUXIANDAO POLYESTER DOPE DYED YARN CO LTD

Method of Manufacturing Anti-Bacteria Polyamide Fiber via High Speed Spinning

A method of manufacturing anti-bacteria polyamide fiber via high speed spinning disclosed a kind of method, which can make manufacturing anti-bacteria polyamide fiber via high-speed spinning realized, including the preparation of anti-bacteria particles and process of high-speed spinning. The preparation of anti-bacteria particles includes surface treatment of anti-bacteria agent and its process of preparation. Choose nano zeolite carrying silver ion as anti-bacteria agent, mix the anti-bacteria particles and polymer chips, after melting, produce anti-bacteria yarns via high speed spinning. The surface treatment to the anti-bacteria agent the invention can improve the spinnability of raw material and place foundation for realizing high speed spinning. Further more, for the spinning pack, adopt good quality mental powder as filtering and pressuring material and increase length diameter rate of hole of spinneret to lengthen the friction distance that the melt passing the spinneret holes in order to eliminate the inner energy of polymer, which prevent the melt from breaking cause by released inner energy while polymer bursting from the spinneret holes. The method described in the invention is simple and easy to implemented. High speed spinning realized by adopting this method, solve the problems of long process rout, low output and lower grade products caused by existing low-speed spinning and greatly increase the beneficial result of enterprise.
Owner:LIAONING YINZHU CHEMTEX GROUP
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