1results about How to "Increase electrophilicity" patented technology

This invention belongs to the field of acyclic compound technology, specifically relating to a method for preparing tert-amyl peroxide. A tert-amyl hydrogen peroxide aqueous solution is added to a solvent and stirred to obtain a mixed solution. Under stirring conditions, p-toluenesulfonic acid and ferric phosphide are added sequentially to the mixed solution. After the addition is complete, stirring continues to produce reaction solution I. Under stirring conditions, acetic anhydride is added to reaction solution I. After the addition is complete, stirring continues to produce reaction solution II. A washing solution is added to reaction solution II, and the mixture is stirred and washed, then separated to obtain crude tert-amyl peroxide. The crude tert-amyl peroxide is washed, dried, and the solvent is removed to obtain tert-amyl peroxide. This invention avoids the problems of large amounts of hydrochloric acid produced by traditional acyl chloride methods and the corrosiveness caused by using sulfuric acid as a catalyst. Furthermore, ferric phosphide is magnetic, allowing for recycling through magnetic separation after the reaction. p-Toluenesulfonic acid can be regenerated through ion exchange resin, significantly reducing production costs.