The invention discloses a
transition metal sulfur-group compound thin-layer material as well as a preparation method thereof and application thereof. The preparation method comprises the following steps: uniformly spreading a
transition metal source between two linings to prepare a sandwich structure; performing
thermal treatment on the sandwich structure, fusing and bonding two substrates together, performing
chemical vapor deposition reaction on a
sulfur-
group element source and the fused bonded sandwich structure under protection of protective gas, heating the
transition metal source to dissolve and diffuse at a
reaction temperature, separating out the transition
metal source on the surfaces of the substrates, and enabling the transition
metal source to react with the
sulfur-
group element source, wherein the sulfur-
group element source comprises one or more of a sulfur source, a
selenium source and a
tellurium source. In this way, a dissolving-separating out principle is combined with the
chemical vapor deposition reaction to prepare the transition
metal sulfur-group compound thin-layer material, and a preparation process of the transition metal sulfur-group compound thin-layer material is simple and easy, and is controllable in process; and the obtained transition metal sulfur-group compound thin-layer material is uniformly distributed in a
centimeter-level range, is good in morphology, is excellent in performances such as optical performances and electrical performances, and has a wide application prospect.