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312 results about "Nano-device" patented technology

Single nanowire electrochemical device and assembly and in-situ characterization method thereof

The invention relates to a single nanowire electrochemical device and an assembly and in-situ characterization method thereof. The method comprises the following steps of: dispersing nanowire anodes of vanadium oxide nanowires, and the like, nano film cathodes of HOPG (Highly Oriented Pyrolytic Graphite), and the like or nanowire cathodes of silicon nanowires, and the like and nano film anodes of LiCoO2, and the like on a substrate; respectively making metal electrodes at both ends of the nanowires and the nano films as current collectors by adopting technologies, such as PECVD (Plasma-Enhanced Chemical Vapor Deposition), and the like; then, depositing silicon nitride or spinning a photoresist on the metal current collectors as protection layers of the current collectors by adopting the PECVD technology, and the like; and finally, dispensing a polymer electrolyte on the surface of the substrate to finish the assembly of the single nanowire electrochemical device. In the invention, charging and discharging tests are carried out on the electrochemical device, then in-situ electrical transport performance tests, micro-domain Raman spectrum analysis, and the like are carried out on the single nanowire electrodes in different charging and discharging states, the direct relation among the electrical transport, the structure and the electrochemical performance of the nanowire electrode material is established, a platform is provided for battery diagnosis, and the like and a support power supply can be provided for the nano device.
Owner:武汉楚理佳纳新能源科技有限公司

Preparation method of graphite type carbon nitride nanotubes

The invention discloses a preparation method of graphite type carbon nitride nanotubes. The preparation method comprises the following steps: adding melamine powder into a high temperature-resistant container, and placing the high temperature-resistant container on a vibrator for vibration treatment; then adding a cover on the high temperature-resistant container, placing the high temperature-resistant container into a program heating control device, heating to a first preset temperature at a relatively high heating rate and keeping for a period of time; further heating the program heating control device to a second preset temperature at a relatively low heating rate and keeping for a period of time; and cooling an obtained product to room temperature, and then grinding to form powder so as to obtain the graphite type carbon nitride nanotubes disclosed by the invention. In the synthesis process of the preparation method, the addition of a template or additional organic matters is not required, the preparation method has the advantages of low price, high yield, good repeatability, no impurity interference of products and the like, is simple and easy to operate, and the prepared carbon nitride nanotubes have good fluorescence performance and photocatalytic performance, and have broad application prospects in the fields of nano devices, photocatalysis and the like.
Owner:TIANJIN UNIV

Method for preparing pH-responsive graft copolymer taking ethyl cellulose as main chain

The invention belongs to the fields of high polymer materials and biomedical engineering and particularly relates to a method for preparing pH-responsive graft copolymer taking ethyl cellulose as a main chain. The method comprises the following steps of: performing esterification reaction on residual hydroxyl in the ethyl cellulose main chain and a bromine-containing compound under the protection of inert gas nitrogen or argon to convert the hydroxyl into a bromine group; and performing atom transfer radical polymerization on a methacrylic acid-N,N-lignocaine ethyl ester monomer by using the bromine group as a macroinitiator to form pH-responsive polymer so as to finally obtain the pH-responsive graft copolymer taking the ethyl cellulose as the main chain. The pH-responsive graft copolymer taking the ethyl cellulose as the main chain has biodegradability, biocompatibility and pH value sensitivity and can be self-assembled into stable nano micelles in water, so the pH-responsive graft copolymer can be widely applied to the fields such as medicament release control carriers, biological intelligent switches, biological sensors, biological nano devices and the like. The method has the advantages of simpleness, practicability, industrialized production of raw materials and high popularization and application value.
Owner:TONGJI UNIV

Method for preparing sulfonated polyaniline grafted multi-wall carbon nanotube

The invention discloses a method for preparing a sulfonated polyaniline graft multi-walled carbon nano-tube composite material. The method comprises the following steps: after a multi-walled carbon nano-tube the surface of which is provided with a carboxyl group is subjected to acyl chlorination, the multi-walled carbon nano-tube reacts with para-phenylene diamine, so that anilino group is connected to the surface of the multi-walled carbon nano-tube through amido link; the anilino group connected to the surface of the carbon nano-tube initiates polymerization after the anilino group is oxidized, and the multi-walled carbon nano-tube and sulfonated polyaniline can be connected together through the amido link by further sulfonation and hydrolysis reactions, thereby forming the composite material using the multi-walled carbon nano-tube as a core and the sulfonated polyaniline as a shell. The method solves the problems that the polyaniline can be dissolved in water but has low electrical conductivity after the polyaniline is sulfonated, and the multi-walled carbon nano-tube can be easily agglomerated, but can not be dissolved in water, which has important significance in practical application for sulfonated polyaniline, the multi-walled carbon nano-tube and the polyaniline/multi-walled carbon nano-tube composite material. The method can be widely applied to microelectronic component printing, photoelectric nano-devices, sensors and the like.
Owner:TIANJIN UNIV
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