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31results about How to "Determine content" patented technology

Intelligent cup capable of detecting liquid substance based on near infrared spectrum

The invention discloses an intelligent cup capable of detecting liquid substance based on near infrared spectrum, comprising a cup body, a cup lid, an liner, an MCU, a near infrared spectrum transmitter, a near infrared spectrum receiver, a display screen and a peripheral circuit, wherein the MCU and the peripheral circuit are both arranged at the bottom of the cup body, two transparent windows which are symmetrical along the axis are arranged at the lower end of the liner, the near infrared spectrum transmitter and the near infrared spectrum receiver are both arranged between the liner and the outer wall of the cup body and respectively positioned at the two transparent windows, the display screen is arranged on the outer wall of the cup body, and the signal ends of the near infrared spectrum transmitter, the near infrared spectrum receiver, the display screen and the peripheral circuit are all connected with the signal end of the MCU. The intelligent cup samples and detects drinking water in the cup by the near infrared spectrum detection unit, and determines the liquid substance or content, particularly the content of heavy metal and other harmful substances by analyzing sampled data of the substance spectrum diagram and being compared with the known substance spectrum characteristics.
Owner:成都小爱未来智慧科技有限公司

Preparation and use method of ratio fluorescent probe for visual distinguishing detection

The invention discloses a preparation and use method of a ratio fluorescent probe for visual distinguishing detection. The preparation method specifically comprises the following steps: step 1, preparation of silicon-based carbon quantum dots; step 2, preparation of the nano mesoporous molecularly imprinted material coated with the silicon-based carbon quantum dots; step 3, performing surface modification on the nano mesoporous molecularly imprinted material; and step 4, preparing the ratio fluorescent probe based on the nano mesoporous molecularly imprinted material. The use method comprises the following steps: (1) diluting tetracycline or oxytetracycline into solutions with different gradient concentrations; (2) dispersing the prepared ratiometric fluorescent probe based on the nano mesoporous molecularly imprinted material in ultrapure water; (3) adding a Tris-HCl buffer solution with the pH value of 8 into a quartz cuvette, uniformly mixing the Tris-HCl buffer solution and the solution, and respectively dropwise adding the tetracycline solution or the oxytetracycline solution in the step (1) for fluorescence determination; the main substrate is the silicon dioxide molecular imprinting layer with the mesoporous structure, the method is reliable, mass production can be carried out, and the probe is widely applied to the society.
Owner:HENAN POLYTECHNIC UNIV

Method for detecting EDTA (ethylene diamine tetraacetic acid) in laundry detergent

The invention relates to a method for detecting EDTA (ethylene diamine tetraacetic acid) in a laundry detergent. The method comprises steps as follows: (1) preparing a potassium bicarbonate aqueous solution; (2) adding the to-be-detected laundry detergent to the potassium bicarbonate aqueous solution, stirring the solution at the temperature of 45-50 DEG C for 10-20 min, filtering the solution while the solution is hot, and naturally cooling the solution to the room temperature to obtain a pretreated solution; (3) adding an iron liquid to the pretreated solution, performing oscillating extraction and then centrifugation, and removing an aqueous phase to obtain an ion liquid phase; (4) adding trivalent iron salt to the ion liquid phase, after full and even mixing, performing chromatography separation with a gel column chromatography Superose 12 column, performing washing with n-hexane firstly, then performing gradient elution with a petroleum ether-normal propyl alcohol mixed solvent serving as an eluent, and collecting the eluent; (5) evaporation the solvent of the eluent until the solvent is almost dry, and performing dissolution, volume determination and filtration with an organic membrane to obtain a detection sample; (6) performing liquid chromatography separation on the to-be-detected sample to determine the content. The method is excellent in EDTA quantitation accuracy, and a new detection means is provided for control on the content of the EDTA in the laundry detergent.
Owner:CHINA CERTIFICATION & INSPECTION GRP NINGBO

Standard colorimetric method for measuring content of carbonyl compound in industrial methanol

The invention discloses a standard colorimetric method for measuring the content of a carbonyl compound in industrial methanol, belonging to the field of industrial methanol. The standard colorimetric method comprises the following steps of: firstly, preparing a series of standard solutions with different contents of the carbonyl compound, reacting with 2,4-dinitrophenylhydrazine and potassium hydroxide under a certain condition, and observing that the color gradually changes from faint yellow to deep red brown with the gradual increase of the content of the carbonyl compound. According to information such as the colors of the standard solutions, volume part mass number of the content of the carbonyl compound, and methanol grade, a standard colorimetric card. A sample completely reacts under the same condition, compared with the standard colorimetric card, a closest color is found, and the information such as content of the carbonyl compound and the methanol sample grade is directly read. The quantitative calculation of the content of the carbonyl compound can be realized. The standard colorimetric method has the characteristics of intuition, rapidness, convenience, low requirements for detection devices, apparatuses and occasions, and the like.
Owner:宋继增

Method for determining content of Ti in TiO2 photocatalyst

The invention discloses a method for determining the content of Ti in a TiO2 photocatalyst and belongs to the field of chemical testing. The method comprises the following steps: adding 10-100mg of carrier catalyst into a polytetrafluoroethylene microwave digestion tube, adding 1-10ml of 98% concentrated sulfuric acid and 1-10ml of 30% hydrogen peroxide, and performing heating digestion reaction in a microwave digester, wherein the reaction temperature is controlled within 140-200 DEG C, and the reaction time is controlled within 25-55min; after the reaction is finished, a digestion solution is obtained, filtering the digestion solution, making up to the volume to 50ml, and determining the content of the Ti in a liquid supernatant by virtue of ICP-OES. The carrier TiO2 catalyst is acidized and subjected to microwave digestion pretreatment, TiO2 is converted into the Ti in a soluble ionic state, and the quick, simple and convenient method is provided for the determination of the content of the Ti in the TiO2 photocatalyst. The method is suitable for determining the content of the Ti in a TiO2 nano-sheet colloid, a TiO2 nano-tube, a thin TiO2 film and catalysts in other forms, is suitable for being used for determining the content of the Ti in the TiO2 photocatalyst after repeated reaction, and is wide in application range.
Owner:INST OF URBAN ENVIRONMENT CHINESE ACAD OF SCI

Method for detecting content of aluminium and aluminium alloy oxide inclusions

The invention discloses a method for detecting the content of aluminium and aluminium alloy oxide inclusions, comprising the following steps: (1) first, cutting a sample material of aluminum sheets, washing the sample material with absolute ethyl alcohol and absolute methanol, and drying; (2) weighing 1+/- 0.0001 g sample material, putting the sample material in a beaker containing 60-100 ml of methanol, adding 2-5 ml bromine in the beaker to react for 30-60 min at a temperature of 20-50 DEG C; (3) then adding 1-3 ml of bromine to react for 15-50 min at a temperature of 20-50 DEG C, and then adding 1-3 ml of bromine again to react for 15-50 min at a temperature of 20-50 DEG C, then reacting at a temperature of 30-60 DEG C until the sample material dissolves completely; (4) filtering the solution with filter paper, removing the filtrate, cleaning the filter paper with methanol until no bromine remains; (5) putting the filter paper having precipitations in a crucible, ashing from a low temperature, heating up to 600-900 DEG C and keeping warm for 20-60 min and then taking out, cooling, adding 1-3 g of alkali, and fusing at a temperature of 550-800 DEG C, taking out and adding hot water in the beaker, adding hydrochloric acid while shaking the beaker, pouring the liquid of the beaker in a 100 ml volumetric flask, and bringing to volume by water; and (6) respectively taking 10 ml of the solution out from the 100 ml volumetric flask, bringing to volume by water, then comparing by using a standard curve obtained by atomic absorption, and then determining the content of the aluminium and aluminium alloy oxide inclusions.
Owner:SNTO TECH GRP

Method for detecting pesticide residues in vegetables

The present invention relates to the technical field of vegetable pesticide detection, and discloses a method for detecting pesticide residues in vegetables, including the following steps: S1: extracting samples; S2: detecting the samples, wherein the processed and classified samples are sent into different chromatographic analysis instruments respectively for detection, so as to more comprehensively detect the residual components and content of pesticides in the vegetables; S3: going through a gas chromatograph, so as to analyze the content of some gasified pesticide residues of the pesticideresidues in the vegetables, thus enabling the content of the pesticide residues in the vegetables to be detected quickly, effectively and sensitively; S8: going through a high performance liquid chromatograph that is used to analyze high boiling point and non-volatile, heat-labile and large molecular weight organic compounds, so as to perform chromatographic analysis in a manner of high pressuresolvent delivery; S3: introducing the data into an analyzer, comparing each of detected chromatograms, determining the chromatograms of the pesticide residues in the vegetables by using a mathematicalinduction method in combination with previous data references and determining the content of the pesticide residues of leaves and stems of the vegetables.
Owner:中农康正技术服务有限公司

Reagent for rapidly detecting paraquat, and preparation method and application thereof

The invention relates to a reagent for rapidly detecting paraquat, and a preparation method and application thereof. The reagent for rapidly detecting the paraquat is prepared by mixing two raw materials of sodium hydrosulfite and soluble carbonate. Compared with an existing detection reagent, the reagent is more convenient to use and higher in use safety. According to the method for rapidly detecting the paraquat, the color can be observed at the sample usage amount of 100-300 mg per 0.3 mL, the effect can be more obvious at the sample usage amount of 100-300 mg per 1 mL, and compared with aconventional test method, the sample usage amount is greatly reduced, the practical application value is wider; through the adoption of the detection method, the test can be completed within several seconds, and the test efficiency is higher under a condition of multiple test samples; and the test proves that 100-300 mg per 1 mL of distilled water is added into the reagent, slight vibration is carried out, a cotton swab is used for dipping a small amount of liquid, and then suspicious spots are wiped, so that the paraquat with the content of more than 0.1 microgram can be detected through thecolor change of the cotton swab, and thus the reagent provided by the invention has a wider test range.
Owner:孙剑聪

Standard colorimetric method for measuring content of carbonyl compounds in industrial methanol

The invention discloses a standard colorimetric method for carbonyl compound content in industrial methanol, and belongs to the field of industrial methanol. The method comprises the following steps:preparing a series of standard solutions with different carbonyl compound contents, reacting the standard solutions with 2, 4dinitrophenylhydrazine and potassium hydroxide in sequence under certain conditions, and observing to find that the color is gradually changed from faint yellow to dark red brown along with the gradual increase of the carbonyl compound contents; preparing a standard colorimetric card according to the color of the standard solution, the volume part mass number of the carbonyl compound content, the methanol grade and other information; after the sample is completely reacted under the same condition, comparing the sample with a standard colorimetric card, finding out the closest color, and directly reading out information such as the content of the carbonyl compound andthe grade of a methanol sample. Quantitative calculation of the content of the carbonyl compound can be achieved. The determination method has the characteristics of intuition, rapidness, simplicity,convenience, low requirements on detection equipment, instruments, places and the like.
Owner:邯郸市峰峰矿区煤化工产品研发中心

Method for improving the control of water-conducting household appliances and household appliances suitable therefor

The invention relates to a method for operating a water-conducting household appliance having a drum (3), a control device (18) and a spectrometer (21), the drum receiving objects (22, 34) to be treated, The drum has at least one circumference with at least one radiation channel (30, 35), the spectrometer comprises at least one radiation source (5, 27), at least one radiation detector (7, 28) and a microcomputer (6), wherein , the microcomputer (6) and the control device (18) are configured to exchange information with each other, so that data can be exchanged between the spectrometer (21) and the control device (18), it is characterized in that the method comprises the following steps: (a) The drum (3) is rotated at a predetermined rotational speed Dz, wherein the frequency f based on the number of revolution cycles of the radiation channels (30, 35) per unit time is defined as the ratio of the rotational speed Dz to the radiation channels (30, 35) The product of the quantities; (b) continuously emitted by at least one radiation source (5, 27) of the spectrometer (21) in the wavelength range λ 1 ‑λ 2 the radiation (31) in passes through at least one radiation channel (30, 35) of the rotating drum (3), so that a periodically interrupted radiation (31) with frequency f is produced in the drum (3), and the objects (22, 34) in the rotating drum (3) are loaded with radiation (31) periodically interrupted at a frequency f, and at least one radiation detector (7, 28) is arranged such that the objects (22, 28) 34) The reflected radiation (32) is recorded directly as a measurement signal without passing through the radiation channel (30, 35) and thus not being interrupted by the radiation channel (30, 35) at frequency f, and is generated by the control device (18) only in relation to A periodic function with a period length 1 / f - in particular a sinusoidal or rectangular function - associated with the household appliance (1) as a reference signal; (c) the measurement signal and the reference signal are transmitted to the microcomputer (6), with the aid of the stored in The analysis routine in the microcomputer (6) analyzes the measurement signal and compares it with the reference signal, and transmits the analyzed measurement signal to the control device (18); (d) via the control device (18) An operating program is selected and / or adapted with respect to the evaluated measurement signals, wherein steps (b) to (d) are carried out one or more times. Furthermore, the invention relates to a domestic appliance which is suitable for carrying out the method.
Owner:BOSCH SIEMENS HAUSGERATE GMBH

Method for the improved control of a water-conducting domestic appliance, and domestic appliance which is suitable for carrying out the method

ActiveCN109983170AIncreased sensitivity of measurementGood noise suppressionOther washing machinesControl devices for washing apparatusPhysicsOptical spectrometer
The invention relates to a method for operating a water-conducting domestic appliance comprising a drum 3 for receiving objects 22, 34 to be treated, said drum having at least one perimeter with at least one radiation passage 30, 35; a controller 18; and a spectrometer 21, which comprises at least one radiation source 5, 27, at least one radiation detector 7, 28, and a microcomputer 6. The microcomputer 6 and the controller 18 are designed to exchange information between each other such that data can be exchanged between the spectrometer 21 and the controller 18. The invention is characterizedby the following steps: (a) rotating the drum 3 at a specified rotational speed Dz, wherein a frequency f, which is based on the number of rotation cycles of radiation passages 30, 35 per unit of time, is defined as the product of the rotational speed Dz multiplied by the number of radiation passages 30, 35; (b) continuously ascertaining radiation 31 from the at least one radiation source 5, 27 of the spectrometer 21 in a wavelength range lambda1 to lambda2 through the at least one radiation passage 30, 35 of the rotating drum 3 such that a radiation 3 which is periodically interrupted at thefrequency f is produced in the drum interior and the objects 22, 34 in the rotating drum 3 are supplied with the radiation 31 periodically interrupted at the frequency f, wherein the at least one radiation detector 7, 28 is arranged such that the radiation 32 reflected by the objects 22, 34 is registered directly as a measurement signal without passing through the radiation passage 30, 35, and thus without being interrupted by the radiation passage 30, 35 at the frequency f, and a periodic function, which depends solely on the domestic appliance 1, with the period length 1/f, in particular asine or rectangular function, is generated as a reference signal by the controller 18; (c) transmitting the measurement signal and the reference signal to the microcomputer 6, analyzing the measurement signal and the comparison thereof with the reference signal using an analysis routine stored in the microcomputer 6, and transmitting the analyzed measurement signal to the controller 18; and (d) selecting and/or adapting an operating program by means of the controller 18 with respect to the analyzed measurement signal, wherein steps (b) to (d) are carried out once or multiple times. The invention further relates to a domestic appliance which is suitable for carrying out the method.
Owner:BSH BOSCH & SIEMENS HAUSGERAETE GMBH

A kind of detection method of EDTA in laundry detergent

InactiveCN104267124BMaximum Limit and Maximum Efficiency ExtractionHigh recovery rateComponent separationIron saltsFiltration
The invention relates to a method for detecting EDTA (ethylene diamine tetraacetic acid) in a laundry detergent. The method comprises steps as follows: (1) preparing a potassium bicarbonate aqueous solution; (2) adding the to-be-detected laundry detergent to the potassium bicarbonate aqueous solution, stirring the solution at the temperature of 45-50 DEG C for 10-20 min, filtering the solution while the solution is hot, and naturally cooling the solution to the room temperature to obtain a pretreated solution; (3) adding an iron liquid to the pretreated solution, performing oscillating extraction and then centrifugation, and removing an aqueous phase to obtain an ion liquid phase; (4) adding trivalent iron salt to the ion liquid phase, after full and even mixing, performing chromatography separation with a gel column chromatography Superose 12 column, performing washing with n-hexane firstly, then performing gradient elution with a petroleum ether-normal propyl alcohol mixed solvent serving as an eluent, and collecting the eluent; (5) evaporation the solvent of the eluent until the solvent is almost dry, and performing dissolution, volume determination and filtration with an organic membrane to obtain a detection sample; (6) performing liquid chromatography separation on the to-be-detected sample to determine the content. The method is excellent in EDTA quantitation accuracy, and a new detection means is provided for control on the content of the EDTA in the laundry detergent.
Owner:CHINA CERTIFICATION & INSPECTION GRP NINGBO
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