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40results about How to "Good emulsifying performance" patented technology

Self-microemulsion nanometer composition of ganodenic acid extract and preparation method thereof

The invention relates to a preparation method of a self-microemulsion nanometer composition of ganodenic acid extract; the self-microemulsion nanometer composition takes ganodenic acid extract as crude drug, and the mixture of surface active agent, cosurfactant, and oil phase is adopted as drug carrier; the preparation method is characterized in that: the components are as follows by weight part: 10 parts of ganodenic acid extracts, 50-400 parts of surface active agents, 100-800 parts of cosurfactants, and 15 to 600 parts of oil phase; the ganodenic acid extract is total triterpenoids in ganoderma lucidum which is obtained by extracting lucid ganoderma fruiting body with a supercritical CO2 extracting method. In the method, the total triterpenoids in ganoderma lucidum, which is an insolubility drug, is prepared into self-microemulsion formulation, so as to improve the dissolution rate of the drug, promote the drug adsorption and be beneficial to improving the bio-availability; in addition, the drug can keep a dissolution state in intestine so as to better to permeate through cell membranes dispersedly, thereby improving the drug effect of the drug and enhancing the in-vivo anti-tumor effect.
Owner:JIANGSU PROVINCE INST OF TRADITIONAL CHINESE MEDICINE

Traditional Chinese medicine composition capable of removing miliaria and relieving itch and preparation method thereof

The invention belongs to field of daily necessities and particularly relates to a traditional Chinese medicine composition capable of removing miliaria and relieving itch and a preparation method thereof. The traditional Chinese medicine composition comprises stemona root, artemisia leaves, flavescent sophora root, phellodendron bark, mint, borneol powder and chlorhexidine acetate. The invention also provides a lotion which comprises the traditional Chinese medicine composition, a solubilizer and water. The traditional Chinese medicine composition provided by the invention is capable of completely removing miliaria and relieving itch after being used for seven days; the effective mosquito-repelling time of the traditional Chinese medicine composition is as long as 7.5 hours, and the traditional Chinese medicine composition has obvious effects of removing miliaria and relieving itch, and repelling mosquitos. The invention also provides a preparation method. According to the method, normal-pressure forward and reverse currents are combined with high-frequency high-voltage current to extract medicinal herbs; by virtue of combining pretreatment based on normal-pressure forward and reverse currents with high-frequency current oscillation, effective ingredients are dissolved out, so that the extraction temperature is low, effective ingredient damage caused by high temperature can be reduced, furthermore, the extraction yield is high, the extraction time is short, the cost is low and the preparation method has favorable application prospect.
Owner:湖南知达医药科技有限公司

Amphoteric reaction-type surfactant and preparation method thereof

The invention relates to an amphoteric reaction-type surfactant and a preparation method thereof. Specifically, the amphoteric reaction-type surfactant is a polymerizable surfactant having a good emulsification capability and belongs to the technical field of fine chemical engineering. The preparation method of the amphoteric reaction-type surfactant comprises the following steps that maleic anhydride and N,N-dimethyl-1,3-propanediamine undergo a reaction to produce an intermediate of N-(3-dimethylaminopropyl)maleamic acid; the intermediate of N-(3-dimethylaminopropyl)maleamic acid sequentially reacts with long-chain alkyl bromide; and the reaction products obtained by the previous step are subjected to post-treatment to form the amphoteric reaction-type surfactant. The preparation method provided by the invention adopts a neutralization reaction-quaternization reaction one-step synthesis method, wherein the neutralization reaction-quaternization reaction one-step synthesis method is characterized in that neutralization conditions are controlled in appropriate ranges; and after a neutralization reaction, a quaternization reaction is directly caused without separation and purification processes. Therefore, the preparation method provided by the invention can reduce a material loss produced in neutralization, time spent in neutralized product purification and reagents used in the neutralized product purification.
Owner:长兴三伟热熔胶有限公司

Grease emulsifying agent for coated feed and preparation process thereof

ActiveCN103181458AStable emulsifying effectSuitable for granulation processingAnimal feeding stuffSucrose monolaurateEmulsion
The invention relates to an animal feed additive, i.e. a composite grease emulsifying agent for a coated feed, and a preparation method thereof. The composite grease emulsifying agent for the coated feed comprises the following components in raw material ratio in percentage by weight: 10 percent to 30 percent of glyceryl monostearate, 10 percent to 30 percent of sucrose monolaurate, 5 percent to 20 percent of sorbitol anhydride monolaurate, 5 percent to 10 percent of glycerol monolaurate, 20 percent to 50 percent of polyethylene glycol and 20 percent to 50 percent of silicon dioxide. The preparation process of the grease emulsifying agent comprises the following steps of: firstly, carrying out heat preservation after heating and melting high HLB (Hydrophile-Lipophile Balance) value raw materials; adding silicon dioxide to adsorb to form fine particles; and then dissolving low HLB value raw materials and polyethylene glycol by an organic solvent, uniformly spraying the solution on the fine particles to obtain a finished product. Four food emulsifying agents with different HLB values, which are selected by the invention, are processed by scientific compatibility, are suitable for emulsifying various greases in the feed, have stable emulsifying effects and can keep the state of not breaking emulsion for a long time; after being subjected to coating processing, all of four emulsifying agent ingredients can tolerate high temperature treatment and are suitable for pelletizing processing of the feed.
Owner:HANGZHOU KINGTECHINA FEED CO LTD

Preparation method of automobile filter paper emulsion

The invention relates to a preparation method of an automobile filter paper emulsion. The method includes the steps that firstly, a polymeric emulsifier is prepared, wherein a mixture of soft monomers, water-soluble dispersing monomers and water-soluble crosslinking monomers is added into an isopropanol solvent at the stirring speed of 200-1000 r/min, the temperature is adjusted to be 50-90 DEG C,an oil-soluble initiator accounting for 0.1%-0.5% of the total monomer mass is added, a heat-preserved reaction is carried out for 120-300 min, preparation is completed, the solvent is distilled offunder high-temperature and vacuum conditions, and a 10% aqueous solution is prepared; secondly, the polymeric emulsifier aqueous solution prepared in the first step is heated to 70-90 DEG C, and two types of blending monomers and an aqueous initiator are dropwise added; thirdly, after the reaction is finished, the temperature is decreased to 60-70 DEG C, a redox system is added into the system tocarry out monomer removal, then the pH value is adjusted, and finally filtration is carried out for discharging. The emulsion has the advantages of being small in particle size, good in chemical and mechanical property, excellent in emulsifying property and film-forming property, high in crosslinking degree and the like, and the waterproof property and mechanical strength after film formation of the filter paper emulsion are greatly improved.
Owner:ZHEJIANG JIUBEN BIOCHEM

Water-in-oil type emulsified gasoline

InactiveCN101781591AEasy to purchase and prepare materialsSmall and uniform particle sizeLiquid carbonaceous fuelsHydrophileGasoline
The invention discloses water-in-oil type emulsified gasoline and a preparation method thereof. Span 80 and OP10 or Tween 80 are used as a compound emulsifier the hydrophile-lipophile balance (HLB) value of which is 9, and a long-chain alpha-olefin amphiphilic graft copolymer is used as a dispersant, wherein the preparation method of the long-chain alpha-olefin amphiphilic graft copolymer refers to 101157759A. The water-in-oil type emulsified gasoline comprises the following components in percentage by weight: 0.5-1 percent of long-chain alpha-olefin amphiphilic graft copolymer, 5-15 percent of compound emulsifier, 5-20 percent of water and the balance of gasoline. The preparation method comprises the steps of sequentially adding water, the compound emulsifier and the long-chain alpha-olefin amphiphilic graft copolymer in gasoline, and stirring the mixture for 5-10 minutes with a high-speed shearing and dispersing emulsifying machine under the rotate speed of 10,000 rpm. The emulsified gasoline provided in the invention is very stable, oil-water separation can not occur within 60 days when the emulsified gasoline is stored under 25 DEG C, oil-water separation can not occur within 5 days when the emulsified gasoline is stored under 40 DEG C, and oil-water separation can not occur within at least 130 minutes when the emulsified gasoline is centrifuged under the rotate speed of 15,000 rpm. The water-in-oil type emulsified gasoline has very good practical value.
Owner:ZHEJIANG UNIV

Phenolated lignin, amphoteric lignin emulsifier, emulsified asphalt and preparation method

The invention discloses phenolated lignin, an amphoteric lignin emulsifier, emulsified asphalt and a preparation method of the phenolated lignin. The preparation method of the phenolated lignin comprises the following steps: adding deionized water into lignin, heating to 40-60 DEG C, adding alkali to adjust the pH value to 9-12, adding a catalyst, adding phenol, and reacting at 60-100 DEG C for 0.5-4 hours to generate the phenolated lignin; the preparation method of the amphoteric lignin emulsifier comprises the following steps: mixing a sodium hydrogen sulfite solution with epoxy chloropropane, and reacting to generate a first intermediate; adding the phenolated lignin prepared by the method into deionized water, heating to 60-80 DEG C, adding a sodium hydroxide solution to adjust and stabilize the pH value of the phenolated lignin solution, cooling to 40-60 DEG C, adding dimethylamine, stirring for 10-30 minutes, adding a formaldehyde solution, heating to 70-80 DEG C, and reacting for 3-8 hours to generate a second intermediate; and mixing the two intermediates to generate the amphoteric lignin emulsifier. The phenolated lignin with high reaction activity is adopted and has hydrophilic groups such as amido, sulfo and hydroxyl, and the prepared emulsifier has excellent emulsifying performance.
Owner:JINAN SHENGQUAN GROUP SHARE HLDG

Long-acting rice pre-emergence special herbicide and preparation method thereof

The invention provides a long-acting rice pre-emergence special herbicide and a preparation method thereof. The preparation method comprises the following steps: (1) preparing a urea formaldehyde prepolymer solution; (2) ultrasonically stirring and mixing bensulfuron methyl, bispyribac-sodium, isoxaflutole and acetone to obtain a herbicide A primary mixed solution; performing ultrasonic stirring and mixing on cyhalofop-butyl, metolachlor and acetone, and obtaining a herbicide B primary mixed solution; (3) performing secondary ultrasonic stirring and mixing on the herbicide A primary mixed solution, chitosan, a compound emulsifier and water to obtain a herbicide A emulsion; performing secondary ultrasonic stirring and mixing on the herbicide B primary mixed solution, mushroom proteoglycan,Arabic gum, a compound emulsifier and water to obtain a herbicide B emulsion; (4) respectively mixing with the urea formaldehyde prepolymer solution; (5) spray drying; (6) mixing the micro-capsule particles A and the micro-capsule particles B according to a mass ratio of 3: (0.5-1); the herbicide has a good prevention effect on broadleaf weeds and gramineous weeds, has a good continuous weed sealing effect, and can maintain good and stable seedling emergence number and growth quality.
Owner:HAINAN SHENNONG DAFENG SEED TECH

Walnut oil low-fat emulsion gel and preparation method thereof

The invention discloses walnut oil low-fat emulsion gel and a preparation method thereof. The emulsion gel is prepared from walnut oil, konjac glucomannan, xanthan gum and Tween 80, wherein the konjacglucomannan and the xanthan gum are synergized to form gel as a continuous phase; the Tween 80 is used as an emulsifier; oil drops formed after the walnut oil is emulsified are used as a dispersion phase; the emulsion gel is commonly formed. A preparation process comprises the following steps: adding the Tween 80 into a konjac glucomannan water solution with the concentration of 1.0 percent; after uniformly mixing, adding the walnut oil and homogenizing to obtain emulsion; uniformly stirring and mixing the emulsion and a xanthan gum water solution with the concentration of 1.0 percent; stirring at a constant temperature of 70 to 90 DEG C for 15 to 45min to sufficiently mix a system; and after canning, sterilizing at 121 DEG C for 30 min; cooling to 40 +/-5 DEG C to obtain the walnut oil low-fat emulsion gel with good viscoelasticity. The emulsion gel disclosed by the invention has simple components and good sensory quality, can tolerate high-temperature treatment at 121 DEG C and is not separated; the emulsion gel can be used as a carrier of functional grease and meets the requirements of special crowds; the emulsion gel has soft texture and high resilience and is suitable for thespecial crowds with dysphagia to eat.
Owner:新疆塔格拉克生态农业有限公司
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