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40results about How to "Improve flash point" patented technology

Biodiesel with low temperature liquidity and preparation method of biodiesel

The invention discloses a biodiesel with low temperature liquidity and a preparation method of the biodiesel. The biodiesel with low temperature liquidity comprises 2.5-30 percent by volume of direct coal liquefaction hydro-upgraded modified full-fraction oil and 70-97.5 percent by volume of illegal cooling oil biodiesel. The preparation method of the biodiesel comprises the step: after mixing the illegal cooking oil biodiesel and the direct coal liquefaction hydro-upgraded modified full-fraction oil, and standing for 8-12 hours to obtain the biodiesel with low-temperature liquidity. According to the biodiesel with low temperature liquidity, the pour point, the cloud point, the flash point, the kinematic viscosity, the oxidation stability, the heat value, the density and the acid value of mixed oil are detected according to the GB_T20828-2007, and accord with relevant requirements of EN14214 and ASTMD6751 for the technical performance of the biodiesel through detection. Compared with the illegal cooking oil biodiesel, the biodiesel has the advantages that the cloud point is reduced by 1-8 DEG C, the pour point is reduced by 2-10 DEG C, namely, the low temperature liquidity is remarkably improved, and the preparation method is simple and effective.
Owner:SHANGHAI APPLIED TECHNOLOGIES COLLEGE

Method for preparing silicon-based biolubricant base oil from organosilicon modified fatty acid ester

The invention provides a method for preparing silicon-based biolubricant base oil from organosilicon modified fatty acid ester. The method comprises the following specific steps: mixing fatty acid ester with organic acid and a catalyst and adding the mixture into an epoxidation reaction kettle, dropwise slowly adding an oxidizing agent, reacting, standing for layering, fetching a supernatant liquid and distilling to obtain epoxidized aliphatic ester; carrying out a ring-opening reaction between epoxidized aliphatic ester and organic acid, washing to neutral level after the reaction and carrying out reduced pressure distillation to obtain a ring-opening product; stirring the ring-opening product and heating to reaction temperature, dropwise adding organosilicon and an acid binding agent according to requirements and carrying out a silylation reaction, directly carrying out reduced pressure distillation after the reaction, and separating a solid to obtain the silicon-based biolubricant base oil. By the above method, the disadvantage that biolubricant base oil produced by existing technologies has poor oxidation stability and poor viscosity-temperature characteristic is overcome. The production process is environment-friendly, and energy consumption is low. The industrial acid binding agent used in the method is low-cost such that cost of the product is reduced.
Owner:NANJING UNIV OF TECH

Mixed type polybasicester plasticizer and preparation method thereof

The invention discloses a method for comprehensively utilizing by-products generated in a trimellitic anhydride refining process. The method comprises the following steps: taking polyester waste as a raw material, taking 1,3-diethyl imidazole boron fluoborate as a catalyst, selecting the content and the process temperature of the catalyst, and regulating and controlling molecular size and distribution of a polyethylene terephthalate compound which is obtained by alcoholysis; and when the molecular size and the distribution are in a suitable range, adding refined residues of trimellitic anhydride and carrying out esterification/ester interchange reaction on the refined residues of the trimellitic anhydride and isooctanol to obtain a mixed type polybasicester plasticizer of which performance indexes such as acidity, heating loss and flashing point are good. Compared with the prior art, the mixed type polybasicester plasticizer has better performance indexes such as the acidity, the heating loss and the flashing point, has excellent heat resistance and processing convenience, and can meet requirements of plasticizers in the conventional field. Meanwhile, the preparation method is simple, easy to operate, low in cost of equipment and pollution-free; social benefit and economic benefit are huge; and the method is suitable for being generally popularized and used.
Owner:安徽泰达新材料股份有限公司

A kind of preparation method of aqueous phase suspension method cpvc resin

ActiveCN107459595BSuspension fastEvenly suspendedPolymer sciencePolyol
The invention discloses a CPVC resin preparation method by using a water phase suspension method, and belongs to the technical field of chemical raw materials. The preparation method is characterized in that the preparation steps comprise uniformly spraying a polyhydric alcohol aqueous solution on the surface of PVC resin by using a spraying device; then uniformly suspending the PVC resin which is sprayed with the polyhydric alcohol into a deionized water polymerizing kettle; adding an initiating agent and introducing chlorine gas for chlorination reaction; after the finish of introducing the chlorine gas, adding a chain terminating agent to stop the reaction; and performing washing and drying to obtain a product. The preparation method provided by the invention aims at the characteristics of CPVC resin production process by using the water phase suspension method, gives up the use of dispersing agents, first performs surface activating treatment on the PVC resin by using the polyhydric alcohol, and then performs the chlorination reaction. The prepared CPVC resin has high chlorine content and aging whiteness, has a good stability property, is easy to plasticize uniformly, and has good processability. As a chemical raw material, the CPVC resin can be widely used in preparing various products such as tubular materials, board materials, sectional materials, sheet materials, injection molded parts, foam materials and the like.
Owner:CHINA PETROLEUM & CHEM CORP
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