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84results about How to "Low flash point" patented technology

Oxidation resistant dimethyl silicon oil based magnetic fluid and preparation method thereof

The invention provides oxidation resistant dimethyl silicon oil based magnetic fluid and a preparation method thereof; the dimethyl silicon oil based magnetic fluid is prepared by nano-magnetic particles, a surface modifier and carrier fluid, and the carrier fluid is the dimethyl silicon oil. The preparation method of the dimethyl silicon oil based magnetic fluid comprises the following steps: preparing the nano-magnetic particles; treating the nano-magnetic particles in an activated way; preparing the nano-magnetic particles which are modified by the surface modifier; adding the modified nano-magnetic particles which are purified into methylene dichloride, dispersing and filtering the mixture to obtain the methylene dichloride based magnetic fluid; adding the magnetic fluid into the dimethyl silicon oil to be stirred and dispersed, heating the mixture and maintaining the temperature between 50 and 90 DEG C, separating and precipitating the mixture to obtain the dimethyl silicon oil based magnetic fluid. The dimethyl silicon oil based magnetic fluid in the invention has the advantages of high stability, low temperature resistance and high temperature resistance. The preparation method is simple, high in efficiency and low in requirement on equipments, thus being easy to be applied in various fields and having wide application prospect.
Owner:SUN YAT SEN UNIV

Preparation technique of beta-hydroxyalkylamide

The invention relates to a preparation technique of beta-hydroxyalkylamide, which comprises the following steps: (a) proportionally adding diethanolamine and an alkaline catalyst into a reaction kettle, evacuating until the pressure in the kettle reaches 0.005-0.01MPa, and controlling the temperature at 50-80 DEG C; (b) dropwisely adding dimethyl adipate within 3 hours to carry out ammonolysis reaction, and evaporating to remove alcohol emitted in the reaction process; (c) after finishing dropwisely adding the dimethyl adipate, heating the reaction kettle to the high temperature of 105-120 DEG C to react for 2-4 hours, cooling to 75-95 DEG C to react for 0.5-2 hours, and keeping the viscosity of the product at 800-1000CPS; and (d) after the reaction finishes, carrying out after-treatment (crystallizing, centrifugalizing and drying) on the crude product. The mol ratio of dimethyl adipate to diethanolamine is 1:(1.8-4); the alkaline catalyst is selected from NaOH, KOH, CH3ONa and CH3ONa/NaOH; the alkaline catalyst accounts for 2-6 wt% of the dimethyl adipate; the crystallizing solvent is a mixed solvent in which the ratio of methanol to ethyl acetate is 1:(2-9); and the consumption of the crystallizing solvent is 1.5-4 times of HAA by weight. The invention can effectively enhance the purity of the product and inhibit the generation of side reactions.
Owner:HUANGSHAN HUAHUI TECH

Power grid transformer oil safety detection equipment

The invention discloses power grid transformer oil safety detection equipment, which comprises a compensation oil storage tank, an oil change mechanism, a distribution mechanism, a heat treatment mechanism, a carrier gas circulation mechanism, a temperature control mechanism, a waste oil recovery mechanism and a gas detection mechanism. An interlayer is arranged in the middle of a cylinder to forman independent driving chamber located on the lower portion and an independent sampling and supplementing oil chamber located on the upper portion. An electric driving mechanism is installed in the driving chamber, a push rod of the electric driving mechanism extends into the sampling and supplementing oil chamber and is provided with a piston, and the piston divides the sampling and supplementing oil chamber into a lower sampling oil chamber and an upper supplementing oil chamber. After sampled oil of the same batch is divided into a plurality of equal parts, emphasized detection is carriedout on different equal parts. Temperature control mechanisms located in different flat grooves can be arranged differently. The purpose of achieving the maximum detection degree is achieved accordingto the separation performance of different gases. Unimpeded butt joint of sampled oil treatment and a carrier gas channel can be achieved. The operability of fault gas detection is improved, and the detection precision is improved.
Owner:河南展丰工程技术咨询有限公司

Anti-glare film with high wear resistance and low flash point

ActiveCN112327394AGood compatibilityWill not cause differences in strength or weaknessDiffusing elementsPolyurea/polyurethane coatingsRefractive indexHigh wear resistance
The invention discloses an anti-glare film with high wear resistance and a low flash point. The anti-glare film comprises a base material, and a first anti-glare coating, a second anti-glare coating and a third anti-glare coating which are sequentially coated on the base material; the first anti-glare coating, the second anti-glare coating and the third anti-glare coating respectively contain first anti-glare particles, second anti-glare particles and third anti-glare particles, the particle sizes of the first anti-glare particles, the second anti-glare particles and the third anti-glare particles are sequentially increased, the particle size difference of the first anti-glare particles and the second anti-glare particles is 0.5-5 [mu]m, the particle size difference between the second anti-glare particles and the third anti-glare particles is 1-7 [mu]m; and the first anti-glare particles, the second anti-glare particles and the third anti-glare particles are all organic particles, andthe refractive index difference between the first anti-glare particles, the second anti-glare particles and the resin in the corresponding coatings is less than 0.1. The anti-glare film provided by the invention has excellent properties of low flash point and high definition, and also has excellent wear resistance.
Owner:NUOVO FILM SUZHOU CHINA INC

Magnetic liquid based on oxidation-resistant alpha olefin synthetic oil and preparation method thereof

The invention relates to the field of nanoscale science and technology, and discloses magnetic liquid based on oxidation-resistant alpha olefin synthetic oil and a preparation method of the magnetic liquid based on the oxidation-resistant alpha olefin synthetic oil. The magnetic liquid comprises magnetic nano-particles, surfactants and carrier liquid, and is characterized in that the magnetic nano-particles are ferrite-class magnetic particles DxM1-xFe2O4, wherein the D and the M are Co, Mn, Ni, Mg or Zn, and x=0-1, and the carrier liquid is the alpha olefin synthetic oil or mixed oil with the alpha olefin synthetic oil and other basic oil. According to the magnetic liquid based on the oxidation-resistant alpha olefin synthetic oil and the preparation method of the magnetic liquid based on the oxidation-resistant alpha olefin synthetic oil, the DxM1-xFe2O4 magenetic particles are small in particle diameter, overcome the defects that existing magnetic liquid is poor in oxidation resistance and stability, and the like, are good in oxidation resistance, good in modification effect, and are capable of being dispersed in the carrier liquid, and good magnetic performance can be kept for a long time under a high-temperature environment. The preparation method of the magnetic liquid based on the oxidation-resistant alpha olefin synthetic oil is simple in operation, high in production efficiency, and low in requirement on equipment, and has good application prospects.
Owner:SUN YAT SEN UNIV
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