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51results about How to "Process conditions are easy to achieve" patented technology

Method for preparing high stone powder mixing quantity porous baked brick

The invention belongs to the field of building material, and relates to a method for preparing a high stone powder mixing quantity porous baked brick which comprises the raw materials by weight percent: 80-95% of stone powder, 3-5% of sintering auxiliary agent and 0-17% of additive. The raw materials are simultaneously added pore for forming a medium with the weight accounting for 3-10% of the total weight of the powder, and the solvent is water solution containing 1-5% of binding agent. The preparation method comprises the steps such as weighing the raw materials, mixing, molding, drying, sintering, cooling and the like. As the organic binding agent and the sintering auxiliary are added, the bonding force among stone powder particles can be enhanced, and the formability and the sinteringperformance of adobe can be improved. By adding the pore for forming the medium, the density of the baked brick can be reduced. The invention has simple technique, low cost, high stone powder demand,energy conservation, environmental protection as well as high strength and low density of the baked brick. The invention can increase the stone powder mixing quantity in the baked brick and simultaneously reduce the density of the baked brick, thus being beneficial to expanding the application field of the baked brick and improving the using performance thereof.
Owner:周立忠 +1

Heat conduction composite material and preparation method thereof

The invention provides a heat conduction composite material, which comprises a polymer matrix and a heat conduction filler filled in the polymer matrix, and the heat conduction filler is a boron nitride nano sheet of which the edge is grafted with an amino functional group. The preparation method of the heat conduction composite material comprises the following steps: preparation of a heat conduction filler dispersion liquid: grafting amino functional groups to the edges of boron nitride nano sheets through surface modification to obtain the heat conduction filler; dispersing the heat conduction filler in a dispersing agent to form heat conduction filler dispersion liquid; preparation of a polymer matrix solution: carrying out polymerization reaction on monomers for forming a polymer matrix under the action of heating and a catalyst to obtain a polymer matrix solution; adding the heat conduction filler dispersion liquid into the polymer matrix solution according to a preset proportion,and stirring and mixing to obtain mixed slurry; and curing the mixed slurry to form a film to obtain the heat conduction composite material. The heat conduction composite material provided by the invention has a good heat conduction property and mechanical property.
Owner:SHENZHEN INST OF ADVANCED TECH CHINESE ACAD OF SCI

Method for separating lignin and cellulose from lignocellulose raw material

The invention discloses a method for separating lignin and cellulose from a lignocellulose raw material, and relates to the technical field of high-value utilization of agricultural waste resources. The method for separating the lignin and the cellulose from the lignocellulose raw material includes the following steps: mixing the lignocellulosic raw material and a mixed solvent, adding sulfuric acid, performing stirring and heating at 130-160 DEG C until reaction slurry is formed, performing filtering after cooling, washing the filter residues by using the mixed solvent, and performing dryingto obtain the cellulose; and collecting the filtrate and the washing solution, mixing the collected filtrate and washing solution, adding sulfuric acid, after the concentration of the sulfuric acid is0.5-3.0 wt%, performing a reaction at 170-190 DEG C to form a reaction solution, after cooling, adding water for precipitation, performing filtration, washing the filter residues by using water, andperforming drying to obtain the lignin, wherein the mixed solvent is a mixture of an organic solvent and water. The invention aims to provide the method for separating the cellulose and the lignin, and the method can obtain the cellulose and the lignin with high purity, and improve the yield of the lignin.
Owner:WUHAN POLYTECHNIC UNIVERSITY

Preparation method of inorganic-organic hybrid monolithic column

The invention relates to a preparation method of an inorganic-organic hybrid monolithic column. The preparation method comprises the following steps: A. adjusting the pH value of Fe<2+> compound containing aqueous solution, adding with nano-diamond, adding with H2O2 and reacting to obtain hydroxyl nano diamond; B. mixing the hydroxyl nano diamond with KH570, dissolving into ethyl alcohol, carrying out ultrasonic treatment, reacting, centrifuging, washing, and drying to obtain the coupled hydroxylized nano diamond; C. mixing the coupled hydroxylized nano diamond, dipentaerythritolhexaacrylate, a cross-linking agent, an initiator and a pore-foaming agent, injecting the mixture into a stainless steel column, and reacting for 1-1.5h; and D. connecting the stainless steel column with a high-pressure infusion pump, flushing, and drying to obtain the inorganic-organic hybrid monolithic column. The preparation method has simple process, the reaction condition can be realized easily, the operability is good, the prepared monolithic column has uniform framework and pore diameter, has good separation effect and can be used for separating complex samples under a wide-temperature-range condition, and the application field of the monolithic column can be expanded greatly.
Owner:HEBEI UNIVERSITY

Method and device for recovering waste silicon powder from trichlorosilane synthetic furnace

A method for recovering waste silicon powder from the trichlorosilane synthetic furnace comprises the synthetic furnace and a silicon powder collection tank, and includes steps: A, replacing the synthetic furnace after the synthetic furnace stops normally; B, after replacement is qualified, connecting a silicon powder discharging valve at the bottom of the synthetic furnace with the silicon powder collection tank through a metal hose, and feeding nitrogen into the synthetic furnace through a nitrogen inlet pipeline; and C, turning on the silicon powder discharging valve to enable the silicon powder along with the nitrogen to be brought into the silicon powder collection tank, and emptying the nitrogen through a cloth bag filter at the top of the silicon powder collection tank to enable the silicon powder to be collected into the silicon powder collection tank, so that the silicon powder is fully recycled. The method for recovering waste silicon powder from the trichlorosilane synthetic furnace has the advantages that the method is simple in process, easy in implementation of process conditions and convenient to operate; and waste silicon powder in the synthetic furnace can be fully recycled in reproduction, and dust hazards to personnel bodies during recovery can be avoided. The invention further discloses a device for recovering waste silicon powder from the trichlorosilane synthetic furnace.
Owner:XINTE ENERGY

Soldering paste and application thereof

The invention relates to the technical field of device welding, and particularly discloses soldering paste. The soldering paste comprises flaky nano-silver, a metal organic source and an organic solvent carrier. The invention further discloses application of the soldering paste in an electronic device packaging interconnection structure, the electronic device packaging interconnection structure comprises a first master slice, a second master slice and a connecting layer which is used for connecting the first master slice and the second master slice, the connecting layer is formed by sintering the soldering paste through a sintering process of heating and applying pressure, and in the sintering process, the heating temperature ranges from 130 DE C to 300 DE C, and the pressure applying pressure ranges from 1 MPa to 20 MPa. The soldering paste can be well applied to the field of electronic packaging of low-temperature welding and high-temperature service, the bonding degree of a connecting interface of the connecting layer formed by sintering the solder paste is good, uniform and compact, the shear strength at 150 DE C can reach 51 MPa or above, and the soldering paste has very high shear strength and can be well applied to packaging and interconnection of electronic devices.
Owner:SHENZHEN INST OF ADVANCED ELECTRONICS MATERIALS

Nano-silver soldering paste, preparation method thereof and application of nano-silver soldering paste in chip packaging interconnection structure

The invention provides nano-silver soldering paste and a preparation method thereof. The nano-silver soldering paste comprises flaky nano-silver and an organic solvent carrier which are mixed with each other, wherein the organic solvent carrier is a mixture of any two or more of ethylene glycol, glycerol, diethylene glycol, triethylene glycol, beta terpineol, gamma terpineol and delta terpineol; and the volume percentage of any organic solvent is not less than 20%. The preparation method of the nano-silver soldering paste comprises the following steps of: providing the flaky nano-silver and the organic solvent carrier, and stirring and mixing the flaky nano-silver and the organic solvent carrier to prepare the nano-silver soldering paste. The invention further provides an application of the nano-silver soldering paste in a chip packaging interconnection structure. The nano-silver soldering paste has a low-temperature sintering performance and can be well applied to the field of electronic packaging of low-temperature welding and high-temperature service. A connecting layer formed by sintering the soldering paste is high in shear strength, good in bonding degree of a connecting interface and uniform and compact.
Owner:SHENZHEN INST OF ADVANCED TECH CHINESE ACAD OF SCI

Method and device for recovering waste silicon powder from trichlorosilane synthetic furnace

A method for recovering waste silicon powder from the trichlorosilane synthetic furnace comprises the synthetic furnace and a silicon powder collection tank, and includes steps: A, replacing the synthetic furnace after the synthetic furnace stops normally; B, after replacement is qualified, connecting a silicon powder discharging valve at the bottom of the synthetic furnace with the silicon powder collection tank through a metal hose, and feeding nitrogen into the synthetic furnace through a nitrogen inlet pipeline; and C, turning on the silicon powder discharging valve to enable the silicon powder along with the nitrogen to be brought into the silicon powder collection tank, and emptying the nitrogen through a cloth bag filter at the top of the silicon powder collection tank to enable the silicon powder to be collected into the silicon powder collection tank, so that the silicon powder is fully recycled. The method for recovering waste silicon powder from the trichlorosilane synthetic furnace has the advantages that the method is simple in process, easy in implementation of process conditions and convenient to operate; and waste silicon powder in the synthetic furnace can be fully recycled in reproduction, and dust hazards to personnel bodies during recovery can be avoided. The invention further discloses a device for recovering waste silicon powder from the trichlorosilane synthetic furnace.
Owner:XINTE ENERGY

Hydrogel microneedle patch for noninvasive blood glucose detection as well as preparation method and application of hydrogel microneedle patch

PendingCN114847938ADetection visualizationDetecting Visualized In Vivo Blood Glucose RapidlyCatheterSensorsUltraviolet lightsGlucose detection
The invention discloses a hydrogel microneedle patch for noninvasive blood glucose detection as well as a preparation method and application of the hydrogel microneedle patch. According to the invention, the microneedle patch is prepared by a turnover technology and is noninvasively applied to the skin surface, so that simple and rapid extraction of interstitial fluid in vivo and a new method for real-time, rapid and quantitative detection of blood glucose in vivo are realized. The hydrogel microneedle patch contains two hydrogel components: one hydrogel component is hydrogel which can be cured and formed by ultraviolet light, and the other hydrogel component is hydrogel which can be cured and formed by ultraviolet light; and the other hydrogel is functional hydrogel with pH responsiveness, and glucose oxidase is added, so that the hydrogel can sensitively react to in-vivo glucose. The double-response hydrogel is jointly mixed and prepared into a microneedle patch form, the microneedle patch is endowed with noninvasive/minimally invasive property when applied to the skin surface, the microneedle patch is very suitable for extraction of interstitial fluid in vivo, and then real-time, rapid and accurate detection of the blood glucose level in vivo is achieved.
Owner:WUHAN UNIV

Method and equipment for intermittently recycling waste liquid of chlorosilane during polycrystalline silicon production

ActiveCN102910633BImprove handling of difficult problemsReduce wasteHalogenated silanesProcess engineeringEnvironmental engineering
The invention discloses a method for intermittently recycling chlorosilane in discharged waste liquid in a washing tower during polycrystalline silicon production, and the method the following steps of: intermittently charging a chlorosilane waste liquid produced in polycrystalline silicon production into an evaporation device at different places, evaporating trichlorosilane and silicon tetrachloride with lower boiling point into a gas state when the temperature of the evaporation device is controlled at 120-180DEG C and the pressure of the evaporation device is controlled at 0.1-0.6MPa, and charging the gaseous trichlorosilane and silicon tetrachloride into a rectifying tower so as to be purified and recycled. The invention further provides the evaporation device used in the method. The invention has the beneficial effects that the method is simple in process, the process condition is easy to realize, and the method is convenient to operate; and the treatment difficulty of the chlorosilane waste liquid during polycrystalline silicon production in the process of production can be improved, the discharge quantity of exhaust liquor can be mainly reduced, the waste of the chlorosilane can be reduced, the treatment load of an alkali liquor pond can be reduced, the environment pollution problem can be remitted, the labor quantity can be reduced, the production cost can be reduced, the complete recycle of the chlorosilane can be realized, and the phenomenon of equipment blockage can be avoided.
Owner:XINTE ENERGY
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