9results about How to "Reduce organic content" patented technology

The invention belongs to the technical field of organic synthesis, and particularly relates to a catalyst-free continuous production method of chlorotert-butane, which comprises the following steps: adding diluted hydrochloric acid as a starting solution into the tower kettle of a reactive distillation tower, and heating the tower kettle to boil until reflux exists at the tower top; the method comprises the following steps: adding tert-butyl alcohol and concentrated hydrochloric acid into a mixing preheater for preheating, then continuously feeding from a feed port of a reactive distillation tower until the tower top temperature is 45-48 DEG C, the side discharge port temperature is 50-52 DEG C and the tower kettle temperature is 96-105 DEG C, and carrying out reflux according to a reflux ratio of (1.5-3): 1; and continuously extracting crude chlorinated tert-butane from a side discharge port of the tower, cooling, neutralizing, drying and filtering to obtain the chlorinated tert-butane. According to the invention, through the integrated design of the mixing preheater and the reactive distillation column, especially by utilizing the reactive distillation technology to continuously remove the product, the chemical equilibrium limitation of the traditional intermittent process is successfully broken, the raw material conversion rate is obviously improved, and meanwhile, the green production targets of flow simplification, energy consumption reduction and three-waste emission reduction are realized.

The invention discloses a gel casting method of a solid sodium salt battery ceramic electrolyte for energy storage. The injection molding method comprises the following steps: calcining Na-beta ''-Al2O3 powder in an air atmosphere, mixing the calcined Na-beta''-Al2O3 powder with water and ammonium polyacrylate, carrying out primary ball milling, and carrying out spray drying and granulation to obtain spray granulation powder; adding the mixture into a premixed aqueous solution of a dispersing agent and an adhesive, and carrying out secondary ball milling to obtain slurry; injecting the obtained slurry into a mold, applying axial pressure to the slurry through a piston device of the mold, and maintaining the pressure; standing the whole mold in the pressurized state; taking a green body after pressure relief; carrying out coupling drying on the obtained green body in three stages, and then carrying out glue removal in an air atmosphere to obtain a prefabricated ceramic tube green body; and sintering to obtain the solid electrolyte. The solid electrolyte with high density, high ionic conductivity and high bending strength prepared by the method has a clean low-impedance grain boundary, and completely meets the high-performance requirement of a solid sodium battery on a core electrolyte.

This utility model provides an electrolytic generator and hot water equipment for supplementing minerals. The electrolytic generator includes a shell, a mineral filter element, and an electrode module. The shell is connected to an inlet pipe and an outlet pipe. The electrode module is connected to the shell. The mineral filter element is disposed in the shell and includes a cover plate and a filter element body. The cover plate and the filter element body are detachably connected. The filter element body contains minerals and is connected to the shell. The detachable connection between the cover plate and the filter element body allows for adjustment of the type and quantity of minerals and facilitates replacement of minerals. While supplementing the mineral element content of the water, it also increases the ion concentration of the water. Electrolysis of the incoming water increases the hydrogen and oxygen content of the water.

This invention relates to the field of secondary batteries, specifically, to providing an organic electrolyte for sodium-ion batteries, a preparation method thereof, and its application in sodium-ion batteries. The electrolyte for sodium-ion batteries comprises sodium salts, organic solvents, and additives, wherein the additives include nitrile compounds, sulfonates, and organic sodium salts; this electrolyte can generate a dense SEI layer rich in various inorganic elements, ensuring the sodium... + The rapid diffusion of ions, combined with a suitable reduction in the organic content of the SEI, improves the stability of the SEI during long-term cycling. Compared to sodium-ion batteries assembled using phosphate materials as the positive electrode active material, the capacity retention rate is greater than 80% after 1000 cycles at 1C rate.

The application discloses a kind of power plant water reuse RO system ultrasonic anti-fouling pretreatment device and control method, it is related to industrial water treatment technical field, including the following steps: to the water after coagulation sedimentation filtration treatment in the first ultrasonic treatment when entering ultrafiltration inlet mother pipe, first ultrasonic treatment uses built-in arrangement;Based on the water flow of entering ultrafiltration inlet mother pipe, the ultrasonic frequency of first ultrasonic treatment is adjusted, and the ultrasonic frequency is proportional to water flow.The application is processed by ultrasonic treatment before and after ultrafiltration and differential parameter control, reduces the pollution degree of organic matter and microorganism to membrane, slows down flux attenuation and prolongs membrane and filter element use cycle;While combining the frequency regulation of flow and pollution index and the synergistic effect of reagent, realize the adaptive adjustment of processing intensity, reduce energy consumption and improve operation stability under the premise of guaranteeing processing effect.

The utility model discloses a domestic sewage treatment and ecological utilization device which comprises a sewage treatment tank, a filter net basket structure is inserted into the inner wall of the sewage treatment tank, a plurality of feeding devices are assembled on the inner wall of the filter net basket structure in a penetrating manner, a sewage discharge pipe is fixedly assembled on the upper edge of one side of the sewage treatment tank, and a water outlet pipe is fixedly assembled on the lower edge of the other side of the sewage treatment tank. A sewage discharge pipe is fixedly connected to one side of the inner wall of the sewage treatment tank in a penetrating manner, a plurality of water quality detectors are assembled on the inner wall of the filter net basket structure in a penetrating manner, the water quality detectors are fixedly connected to the inner wall of the sewage treatment tank in a penetrating manner, and red nematodes are put into different inner cavities of the filter net basket structure for dispersion treatment, so that the water treatment efficiency is ensured; the sewage treatment tank is simple in structure and convenient to use, prevents red nematodes from being accumulated at the bottom of the sewage treatment tank and affecting the water treatment effect, can detect the water quality conditions of different areas by cooperating with the water quality detector, periodically adjusts to put the red nematodes into a certain cavity in the filter net basket structure, and is convenient to use and high in practicability.

The utility model provides an in-vitro scaling type electrocatalytic oxidation device, which relates to the technical field of sewage electrolysis treatment and comprises a cathode plate, an anode plate, an anion exchange partition plate, a cathode electrolysis chamber plate and an anode electrolysis chamber plate. Wherein the cathode electrolysis chamber is located between the anion exchange partition plate and the cathode plate, and the anode electrolysis chamber plate is located between the anion exchange partition plate and the anode plate. The utility model has the beneficial effects that the anode plate can generate hydroxyl radicals with high oxidability in the anode electrolysis chamber, so that the sewage in the anode electrolysis chamber is oxidized, and the treatment of organic wastewater is realized; and the anion exchange partition plate can prevent cations in the anode electrolysis chamber from moving towards the cathode electrolysis chamber and reduce the concentration of the cations in the cathode electrolysis chamber, so that the problem that the surface of a cathode plate is scaled due to the fact that the concentration of the cations in the cathode electrolysis chamber is too high is solved, the electrocatalytic oxidation device can continuously work for a long time, and the sewage treatment efficiency is improved.

The present invention provides a method for continuously preparing titanium and titanium alloy wire materials with a short process, which relates to the technical field of preparing titanium and titanium alloy wire materials. The preparation method includes powder preparation, slurry preparation, wire blank forming, wire blank drying, wire blank coating, degreasing sintering, cold drawing and post-treatment carried out in sequence. Among them, the titanium and titanium alloy extrusion slurry is poured into the slurry tank of a screw extruder, and an ultraviolet light source or a heat source is equipped at the die opening of the screw extruder. The slurry is extruded through the die opening and in-situ solidified into a wire blank under the action of the light source or the heat source. By matching continuous production equipment with the technological processes of screw extrusion molding, degreasing sintering and cold drawing, the present invention avoids the high-temperature melting process of the traditional casting-drawing process and the complex processes of multi-pass hot rolling-drawing, realizes the short-process continuous and controllable preparation of titanium and titanium alloy wire materials, has high flexibility in the design of its composition and diameter, strong stability, wide applicability, low cost and excellent performance, and is very suitable for large-scale industrial production.

This disclosure relates to a method for stabilizing concentrated oil refinery sludge. The method includes: heating a mixture of concentrated oil refinery sludge and a treatment agent under acidic conditions to obtain a treated material; wherein the concentrated oil refinery sludge has a moisture content of 98-98.5% by weight, a total suspended solids content of 15-20 g / L, and a volatile suspended solids content of 10-15 g / L; the treatment agent is obtained by pretreating ammonia oxime wastewater. This disclosure uses a treatment agent obtained after pretreating ammonia oxime wastewater to treat concentrated oil refinery sludge, which can significantly reduce the organic matter content and moisture content of the sludge cake, achieving substantial stabilization of the concentrated oil refinery sludge, while simultaneously realizing the resource utilization of the ammonia oxime wastewater.