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32results about How to "Troubleshoot follow-up issues" patented technology

Method for producing industrial and agricultural monoammonium phosphate and magnesium ammonium phosphate with wet-process phosphoric acid

The invention provides a method for producing industrial and agricultural grade monoammonium phosphate and magnesium ammonium phosphate with wet-process phosphoric acid. The wet-process phosphoric acid is taken as a raw material. Sodium fluosilicate, monoammonium phosphate solution, monoammonium phosphate filter cakes and magnesium ammonium phosphate are respectively obtained through defluorination and a three-section substep neutralization process, wherein the monoammonium phosphate solution is concentrated and crystallized to obtain high-quality water soluble industrial monoammonium phosphate, and the monoammonium phosphate filter cakes and the monoammonium phosphate mother solution subjected to repeated crystallization are subjected to size mixed and dried to obtain qualified agricultural monoammonium phosphate. The magnesium ammonium phosphate is a good slow release nitrogenous fertilizer per se. The process has the advantages of little investment of equipment, good adaptability of raw material, low production cost and good product quality. The water soluble industrial monoammonium phosphate with low cost can provide a cheap and good water soluble phosphatic fertilizer for modern facility agriculture.
Owner:昆明隆祥化工有限公司

Processing device and processing method applicable to high-ammonia-nitrogen agricultural wastewater

The invention discloses a processing device and a processing method applicable to high-ammonia-nitrogen agricultural wastewater, and belongs to the field of processing of agricultural wastewater. According to the processing device and the processing method, a cylindrical electrolytic bath is arranged between an anaerobic sludge bed and a tower-type biological filter, and has a significant buffer effect on pollution load of the agricultural wastewater; at the same time through the arrangement of a return system and a two-phase denitrifying tank, the water quality of effluent water and the stable operation of the system can be ensured; biogas produced by the anaerobic sludge bed can be reused into the two-phase denitrifying tank, not only carbon emissions to the environment can be reduced, but also the denitrification rate of the two-phase denitrifying tank can be improved through utilization of anaerobic denitrification effect of methane, recycling utilization of waste matters can be realized, and the concept of green environmental protection can be embodied. The processing device is convenient to operate and easy to maintain, has relatively low construction costs and maintenance costs, and has good popularization and application value.
Owner:NANJING INST OF ENVIRONMENTAL SCI MINIST OF ECOLOGY & ENVIRONMENT OF THE PEOPLES REPUBLIC OF CHINA

Iron oxide doped iron metal organic framework and green macro preparation method and application thereof

The invention discloses an iron oxide doped iron metal organic framework material and a green macro preparation method and an application thereof. The preparation method comprises the following steps:(1) grinding and mixing ferrous sulfate heptahydrate and trimesic acid evenly, adding a sodium hydroxide solution, transferring to a micro wave reaction kettle, carrying out ultrasonic treatment, heating, and cooling to room temperature to obtain a mixed liquid; and (2) washing the mixed liquid obtained in the step (1), centrifuging to obtain a solid, washing the obtained solid, and drying in vacuum to obtain the iron oxide doped iron metal organic framework material. A heterogeneous catalyst is synthesized by a microwave solid-phase co-crystallization method, the synthesis cycle is greatly shortened, the synthesis process is green, environmentally friendly and efficient, and the synthesized iron oxide doped iron metal organic framework material can make full use of an unsaturated metal site to efficiently activate persulfate to degrade organic pollutants, avoid the generation of iron mud, reduce the cost of synthesis of the heterogeneous catalyst material and the cost of degradationof organic pollutants, and improve water environment quality.
Owner:SOUTH CHINA UNIV OF TECH

Method for producing industrial and agricultural monoammonium phosphate and magnesium ammonium phosphate with wet-process phosphoric acid

The invention provides a method for producing industrial and agricultural grade monoammonium phosphate and magnesium ammonium phosphate with wet-process phosphoric acid. The wet-process phosphoric acid is taken as a raw material. Sodium fluosilicate, monoammonium phosphate solution, monoammonium phosphate filter cakes and magnesium ammonium phosphate are respectively obtained through defluorination and a three-section substep neutralization process, wherein the monoammonium phosphate solution is concentrated and crystallized to obtain high-quality water soluble industrial monoammonium phosphate, and the monoammonium phosphate filter cakes and the monoammonium phosphate mother solution subjected to repeated crystallization are subjected to size mixed and dried to obtain qualified agricultural monoammonium phosphate. The magnesium ammonium phosphate is a good slow release nitrogenous fertilizer per se. The process has the advantages of little investment of equipment, good adaptability of raw material, low production cost and good product quality. The water soluble industrial monoammonium phosphate with low cost can provide a cheap and good water soluble phosphatic fertilizer for modern facility agriculture.
Owner:昆明隆祥化工有限公司

Technical method for preparing biodiesel using reactive separation process coupling technique

This is the craft method of preparing biological diesel oil by using the coupling technology in reaction separating course. It relates to the new craft of preparing biology diesel oil (fatty diethylene glycol dinitrate) through the ester exchange reaction of vegetable oil and higher alcohols, and belongs to chemical industry craft technology field. It includes: the ester exchange reaction of vegetable oil and higher alcohols; the separation of product fatty diethylene glycol dinitrate, glycerol and reaction mixed liquid; the separation of product fatty diethylene glycol dinitrate, glycerol and higher alcohols; the separation of fat diethylene glycol dinitrate and glycerol; the condensation backflow of fatty alcohol; and the separation of glycerol. It makes the circumvolving higher alcohols carry out the product fatty diethylene glycol dinitrate and glycerol through higher reaction temperature, and realizes the separation of outcome and reactant; the non-homogeneous phase catalyst stays in the actor, and don't need to have following process to the catalyst. The invention realizes the coupling of reaction and separation courses, speeds up the speed of non-homogeneous phase reaction, and avoids the problem of the following process to catalyst in the homogeneous phase process. Besides it can save production cost, and improves the producing performance of biology diesel oil.
Owner:TSINGHUA UNIV

System and method for safe filling after liquid ethane pipeline overhauling

PendingCN111536420AGuarantee safe operationGuarantee the safety of operationPipeline systemsEngineeringEnvironmental geology
The invention discloses a system and method for safe filling after liquid ethane pipeline overhauling. The system comprises a trunk system, a trunk valve chamber system, an ethane filling system and apipeline temperature and pressure detection system, the trunk valve chamber system is responsible for emptying and reopening of upstream and downstream pipelines of a valve chamber and also providesa channel for replacing of a trunk pipeline, and the ethane filling system is used for introducing ethane from an upstream trunk line, heating the ethane for temperature adjustment and then feeding the ethane into a to-be-opened downstream trunk line before the downstream trunk line is reopened. According to the functional demand of reopening of a liquid ethane pipeline after overhauling and releasing, on the basis of the characteristic that the liquid ethane is vaporized under the low pressure to cause the low temperature, by adopting the measures that an upstream pipe section provides a medium filling channel through a valve chamber bypass, an initial-stage filled medium is externally connected with equipment for vaporization heating, and middle-and-later-stage filling, boosting and liquidation are conducted, the problem of low temperature of the medium in the filling process of an isolated and overhauled section of the liquid ethane pipeline is effectively controlled, safe operationof the liquid ethane pipeline is guaranteed, and the effective guarantee is provided for safe operation of the liquid ethane pipeline.
Owner:CHINA PETROLEUM ENG & CONSTR +1

Method for preparing high-purity calcium nitrate by desulfurization and denitrification by-products

The invention discloses a method for preparing high-purity calcium nitrate by desulfurization and denitrification byproducts. The method comprises the following steps: S1, mixing the desulfurization and denitrification byproducts, water and an antioxidant according to a certain ratio, and performing solid-liquid separation on a mixed solution; S2, mixing a second filtrate and a third filtrate in S1, evaporating, concentrating, cooling, crystallizing and drying; S3, mixing and stirring an obtained crystallizing solid in S2 and an organic solvent, and performing solid-liquid separation to produce a second solid component and an organic solvent filtrate; performing reduced pressure distillation on the organic solvent filtrate, wherein the organic solvent is recycled, and a crystallizing product is the high-purity calcium nitrate solid. The method for preparing the high-purity calcium nitrate by the desulfurization and denitrification byproducts has the advantages that by using the desulfurization and denitrification byproducts as the raw materials, the high-purity calcium nitrate is prepared by stepped extracting and oxidizing; the raw materials are easy to obtain, the corresponding technological process is safe and reliable, and the problem of subsequent treatment difficulty of the desulfurization and denitrification byproducts is solved.
Owner:BEIJING BUILDING MATERIALS ACADEMY OF SCI RES

Device for disposing solid blockages in natural gas hydrate slurry pipeline

The invention relates to a device for disposing solid blockages in a natural gas hydrate slurry pipeline. The device comprises a first decomposition bin for heating and decomposing the blockages intonatural gas, second decomposition bins for receiving the natural gas decomposed by the first decomposition bin, a heating bin for heating the first decomposition bin, a first sensor and a second sensor, wherein the first sensor and the second sensor are used for sensing the position of a pipe cleaner moving in a natural gas pipeline; the first decomposition bin is connected with a blockage feedingpipeline which communicates with or does not communicate with a natural gas pipeline, and pipeline blocking plates capable of moving in the radial direction to close or open the natural gas pipelineare further arranged; the upper ends of the second decomposition bins are connected with a natural gas discharging pipeline which communicates with or does not communicate with the natural gas pipeline; and a cutting device for crushing the blockages is mounted on the wall of the natural gas pipeline. According to the device, after being crushed, the blockages in the natural gas pipeline are decomposed into the natural gas in a heating manner and then is discharged into the natural gas pipeline again, so that the function of converting the blockages into the natural gas underground in the natural gas transportation process can be realized.
Owner:CHANGZHOU UNIV

Underground nuclear power plant having low-and-intermediate-level radioactive waste disposal site

ActiveCN106128534ASave design and construction costsAvoid radioactive releaseNuclear energy generationFacility decommissioningNuclear plantCyclic process
The invention discloses an underground nuclear power plant having a low-and-intermediate-level radioactive waste disposal site. The underground nuclear power plant comprises a nuclear island arranged in an underground cavern group of a nuclear island of a mountain and a conventional island arranged on a ground platform at the outer side of the mountain. The nuclear island consists of a reactor workshop arranged at the center, a nuclear fuel workshop, a safety workshop, an electrical workshop, and a nuclear auxiliary workshop, wherein the nuclear fuel workshop, the safety workshop, the electrical workshop, and the nuclear auxiliary workshop encircle the reactor workshop. And the nuclear island also includes a low-and-intermediate-level radioactive waste disposal site arranged in the underground cavern group of the nuclear island of the mountain; and the low-and-intermediate-level radioactive waste disposal site is communicated with the nuclear auxiliary workshop of the nuclear island by a waste transport tunnel. According to the invention, on the basis of combination of characteristics of the underground nuclear power plant, the processing requirement of the low-and-intermediate-level radioactive waste can be met, the closed circulation of fuels can be realized, and the radioactive contamination possibly occurring during the fuel cycle process can be reduced; and the unified planning and building of the nuclear power plant and the disposal site can be realized and costs are saved.
Owner:CHANGJIANG SURVEY PLANNING DESIGN & RES

A treatment device for solid blockages in natural gas hydrate slurry pipelines

The invention relates to a treatment device for solid blockages in natural gas hydrate slurry pipelines, comprising a first decomposition chamber for heating and decomposing the blockages into natural gas, a second decomposition chamber for receiving the natural gas decomposed by the first decomposition chamber, and a device for heating the first decomposition chamber The heating chamber, the first sensor and the second sensor that sense the position of the pig moving in the natural gas pipeline, the first decomposing chamber is connected with a blockage feed pipe that communicates with or closes the natural gas pipeline, and is also equipped with a radial Move the pipeline blocking plate that closes or opens the natural gas pipeline, and the upper end of the second decomposition bin is connected with a natural gas discharge pipeline that is connected or closed with the natural gas pipeline; a cutting device for breaking blockages is installed on the wall of the natural gas pipeline. The invention breaks the blockage in the natural gas pipeline, decomposes it into natural gas by heating and discharges it into the natural gas pipeline, thereby realizing the function of converting the blockage into natural gas underground during the transportation of natural gas.
Owner:CHANGZHOU UNIV

Petroleum coke fine powder coke forming process

PendingCN114506840AHigh resistivity of powderMeet the requirements of prebaked anode productionCarbon preparation/purificationWaste oilThermal treatment
The invention discloses a forming process of petroleum coke fine powder coke. The forming process comprises the following steps: taking fine powder coke which is screened from raw materials and has the moisture content of less than 10wt% as a forming raw material; biomass waste oil obtained by simply refining kitchen waste oil is adopted as a forming agent; mixing the fine coke powder with the biomass waste oil; after uniformly mixing, carrying out normal-temperature extrusion forming on the mixture through an extrusion forming machine to obtain columnar granules with the diameter of 2-15mm and the length of 5-15mm; the formed granules are placed in a sintering furnace to be dried and sintered, the sintering finishing temperature is 200-300 DEG C, the heating rate is 20-30 DEG C/min, and high-temperature heat preservation is conducted for 0.5-1 h; mixing the molded granules subjected to heating treatment into the screened petroleum coke granules, and carrying out a petroleum coke calcining process; and finally calcining to obtain finished product particles. The casting yield of the petroleum coke is increased, the production quality of the anode is guaranteed, and the problem that the anode raw material formula is limited by the fine coke powder amount is solved.
Owner:GUIYANG AL-MG DESIGN & RES INST

Method for preparing high-purity calcium nitrate by desulfurization and denitrification byproducts

The invention discloses a method for preparing high-purity calcium nitrate by desulfurization and denitrification byproducts. The method comprises the following steps: S1, mixing the desulfurization and denitrification byproducts, water and an antioxidant according to a certain ratio, and performing solid-liquid separation on a mixed solution; S2, mixing a second filtrate and a third filtrate in S1, evaporating, concentrating, cooling, crystallizing and drying; S3, mixing and stirring an obtained crystallizing solid in S2 and an organic solvent, and performing solid-liquid separation to produce a second solid component and an organic solvent filtrate; performing reduced pressure distillation on the organic solvent filtrate, wherein the organic solvent is recycled, and a crystallizing product is the high-purity calcium nitrate solid. The method for preparing the high-purity calcium nitrate by the desulfurization and denitrification byproducts has the advantages that by using the desulfurization and denitrification byproducts as the raw materials, the high-purity calcium nitrate is prepared by stepped extracting and oxidizing; the raw materials are easy to obtain, the corresponding technological process is safe and reliable, and the problem of subsequent treatment difficulty of the desulfurization and denitrification byproducts is solved.
Owner:BEIJING BUILDING MATERIALS ACADEMY OF SCI RES
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