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33results about How to "With optical properties" patented technology

Ultra-high performance concrete slurry, ultra-high performance concrete and preparation method thereof

Belonging to the technical field of building materials, the invention in particular relates to an ultra-high performance concrete slurry, an ultra-high performance concrete and a preparation method thereof. The ultra-high performance concrete slurry comprises: cement, microsilica, nano silica, quartz powder, silica sand, steel fiber, a water reducing agent and water. According to the theory of theclosest packing, the adding proportion of each material is calculated, and trial mix experiments are carried out repeatedly, thus researching and developing the ultra-high performance concrete with the characteristics of minimum raw material variety, simple mixing process and maintenance technology, and the best mechanical properties.
Owner:GUANGDONG UNIV OF TECH

Method for treating aluminium section bar sarface by nano modified powder paint

The present invention relates to a metal surface treating technology, and is to utilize nano technology and nano material to modify traditional powder paint. Specifically, aluminum section bar surface is treated with nano modified powder paint to raise quality and increase special functions. The nano modified powder paint is prepared through the steps of mixing conventional paint material including resin, curing agent, pigment, assistant and stuffing with nano material, smelting, extruding, cooling, pressing, coarse crushing, grinding, sieving etc. The nano modified powder paint is used to treat aluminum shapes through electrostatic painting.
Owner:ZHONGKE JIEDA TECH INST BEIJING

Preparation method of NaV2O5 crystal material with right angle morphology

The invention relates to a preparation method of a NaV2O5 crystal material with right angle morphology. The method comprises the following steps: a), dissolving an aromatic acid organic matter in water, adding a sodium hydroxide solution under the condition of stirring at room temperature, adding a solvent, and stirring for 40-60 minutes at room temperature so as to obtain an evenly mixed solution; b), adding ammonium metavanadate in the mixture so as to obtain a yellow and transparent mixed liquid, transferring the mixture into a stainless steel reaction kettle with a polytetrafluoroethylenelining after stirring for 3 hours, and then placing the reaction kettle in a constant-temperature drying oven of 150-200 DEG C to age for 2-60 days; and c), taking out and filtering the mixture finally obtained in the step b), drying the mixture in the constant-temperature drying oven of 40-60 DEG C so as to finally obtain the NaV2O5 crystal material with a right angle L shape. In the preparationmethod provided by the invention, ammonium metavanadate is adopted as a reactant, an alkaline solvent system of the organic matter in water / absolute ethyl alcohol is used, thus the preparation methodis environment-friendly, has simple preparation process and utilizes simple equipment, and the obtained NaV2O5 crystal material with L shape can be used for research on nano optical devices.
Owner:HEBEI UNIV OF TECH

Preparation method and device of a nanofiber composite light-transmitting material

The invention relates to a method and device for preparing a nanofiber composite light-transmitting material, comprising: (1) preparing PA-6 spinning solution and PMMA spinning solution respectively, and spinning with a uniform blending device to obtain a composite nanofiber mat; ( 2) Lay the above-mentioned composite nanofiber felt in a mold, heat and pressurize, keep warm and pressurized for 20-60 minutes, take off the mold, and wait for complete cooling at room temperature to obtain the product. The device includes a receiving drum (1), a spinneret (2), a micro-injection pump (3) and a high-voltage power supply (4). The invention has the advantages of simple process, low cost and easy operation; the prepared composite light-transmitting material contains nanofiber reinforcement materials with a diameter less than 400nm, not only the original light transmission is not disturbed, but also the tensile mechanical properties can be significantly enhanced, thus It is very suitable for those occasions that have high requirements for light weight and mechanical properties.
Owner:DONGHUA UNIV

Insulation coating for surface of low-voltage electric appliance and preparation method thereof

The invention discloses an insulation coating for the surface of a low-voltage electric appliance and a preparation method thereof, and relates to the technical field of the insulation coating. The insulation coating is prepared from the following raw materials in parts by weight: 20-30 parts of rubber powder, 15-25 parts of epoxy resin, 10-15 parts of organic silicon resin, 6-15 parts of nanosilicon dioxide, 3-8 parts of nano-zinc oxide, 3-8 parts of nano-magnesium oxide, 3-8 parts of nano-aluminium oxide, 8-16 parts of glass fiber, 6-15 parts of attapulgite, 3-8 parts of calcium stearate, 1.2-2.5 parts of dispersant, 0.8-1.5 parts of defoamer, 2-5 parts of anti-aging agent, 1.5-3.2 parts of adhesive force accelerant and 3.6-6.2 parts of curing agent. The insulation coating has the advantages of high insulation performance, high binding force, easiness in even coating, good anti-aging performance, small possibility of oxidative cracking, long service life, high practicality, simple and easily-learnt preparation process, high operability and easiness in mass production and popularization.
Owner:HEFEI OUSHIJIA ELECTRICAL & MECHANICAL EQUIP CO LTD

Device for magnetic nanoparticle self-assembly photonic crystal fiber

The invention discloses a device for a magnetic nanoparticle self-assembly photonic crystal fiber, which comprises a wide-spectrum laser, a single-mode fiber, a trace liquid injector, a liquid inlet, a quartz capillary, a left high-voltage electromagnetic coil, a right high-voltage electromagnetic coil, a high-power microscopic observer, an ultraviolet light curing device, a liquid outlet, a trace liquid collector and a detector. According to the invention, a UV glue liquid containing magnetic nanoparticles is injected into a the quartz capillary by using the trace biological injector, the magnetic nanoparticles are enabled to accomplish a periodically arranged photonic crystal structure with the aid of a high-frequency magnetic field, the self-assembly structure and morphology of the nanoparticles are monitored in real time by using the high-power microscopic observer, variations of a transmission spectrum are monitored in real time through the wide-spectrum laser and the detector, and the ultraviolet light curing device is started to acquire a self-assembly photonic crystal fiber. Compared with a traditional photonic crystal fiber manufacturing process, the method disclosed by the invention is low in cost, high in preparation speed, simple in required equipment, flexible and controllable in fiber parameter and capable of saving the manufacturing cost of the photonic crystal fiber.
Owner:NORTHEASTERN UNIV LIAONING

Optical device, light source device, and projector

An optical device, a light source device, and a projector are provided. The optical device capable of inhibiting optical element degradation and achieving long service lifetime is provided, and includes a reflecting plate (4A1) and a rotation member (6) that dissipates the heat of the reflecting plate (4A1). The rotation member (6) includes a base portion (61) placed on the reflecting plate (4A1) and a plurality of blade portions (62) that project to the side opposite to the base portion (61). The plurality of blade portions (62) each includes an inclined portion (62a) that is inclined with respect to the base portion (61).
Owner:SEIKO EPSON CORP

Prefabricated inorganic man-made luminous stone slab and preparation method thereof

The invention discloses a prefabricated inorganic man-made luminous stone slab and a preparation method thereof. The stone slab is prepared from, by weight, 14-25 parts of cement, 1-7 parts of calcined kaolin, 50-70 parts of mixed material of sand and luminous stone particles, 1-5 parts of stone powder, 6-15 parts of water, 2-6 parts of water reducing agent and 0.1-6 parts of magnesium oxide pigment. According to the prefabricated inorganic man-made luminous stone slab, by adding luminous stone, through irradiation and excitation of visible rays such as sunlight and lamp light, energy can be absorbed and stored, the light can be given out when the environment rays are dim, the certain luminance is provided accordingly, the chemical stability is good, and the stone slab has certain opticalperformance, wear reduction performance, wear-resistant performance and sound elimination and damping performance.
Owner:东莞环球经典新型材料有限公司

Environment-friendly ultraviolet color-changing color paste, and preparation method and application thereof

The invention discloses environment-friendly ultraviolet color-changing color paste, and a preparation method and application thereof. The color paste comprises the following raw materials in parts byweight: 55-68 parts of ultraviolet color-changing powder, 30-38 parts of polyvinyl chloride (PVC) paste resin, 8-16 parts of diatomaceous earth, 15-30 parts of an environment-friendly plasticizer, 16-23 parts of PVC resin powder, 15-22 parts of white oil, 26-43 parts of deionized water, 11-19 parts of light calcium carbonate, 2-3 parts of an ultraviolet absorbent and 7-12 parts of nano silicon dioxide. According to the invention, through double grinding, the particle size of the color-changing color paste is reduced, the specific surface area is increased, and the coloring force is higher. The color-changing color paste has small fineness, high glossiness, excellent dispersing effect and excellent storage stability. The environment-friendly plasticizer is adopted to synthesize plant ester, so that when being dissolved in an injection molding medium of plastic sandals and foam sandals, the color-changing color paste has excellent bonding performance with the plastic sandals. In addition, the color-changing color paste is free of aromatic compounds, has good safety, is capable of achieving automatic color changing function under ultraviolet irradiation through ultraviolet color-changing powder, and thus has a wide application prospect.
Owner:陈巩固

Sputtering target, optical information recording medium and process for producing the same

A sputtering target characterized in that it is comprised of an In2O3-ZnO-SnO2 composite oxide whose main component is SnO2 compounded with an oxide of any one or both of Ta and Y elements. There is provided a thin film for optical information recording medium (especially used a protective film) that is stable in film amorphous properties, realizes high film forming speed, excels in adherence with recording layer and mechanical properties and is high in transmittance and that by effecting nonsulfide constitution, can suppress deterioration of adjacent reflective layer and recording layer. Further, there are provided a process for producing the same and a sputtering target for use therein. Accordingly, not only can the performance of optical information recording medium be enhanced but also a striking productivity increase can be attained.
Owner:JX NIPPON MINING & METALS CO LTD

Scratching-resistant, wear-resistant and aging-resistant composite spraying film non-woven fabric material

The invention discloses a scratching-resistant, wear-resistant and aging-resistant composite spraying film non-woven fabric material. The scratching-resistant, wear-resistant and aging-resistant composite spraying film non-woven fabric material comprises a protecting layer, a weather resistant layer and a medium layer. The weather resistant layer is prepared from, by weight, 100 parts of polypropylene, 3-10 parts of color master batch, 0.4-1 part of antioxidant, 0.1-0.2 part of stabilizer and 0.3-0.5 part of ultraviolet light absorber. The spraying film non-woven fabric protecting layer is prepared from PET, and a PET film has the advantages of being good in optical performance, flat and smooth in surface, good in heat stability, small in shrinkage percentage, resistant to light aging and the like; as the surface hardness is high, the surface of the product can be protected and is not prone to scratching; as a single silicon film is adopted, it can be guaranteed that the single silicon film can be easily disassembled after being damaged or aged, and the attractiveness of the product cannot be influenced. The spraying film non-woven fabric weather resistant layer is prepared from PP modified resin; as the modified resin is added into the product, the weather resistance can be improved, and the surface quality of the product is improved by adding the color master batch.
Owner:集威新材料科技有限公司

Building material with air purification function and preparation method thereof

The invention provides a building material with an air purification function and a preparation method thereof, which relates to the technical field of building materials. The building material with the air purification function is prepared from the following raw materials in parts by weight: 60 to 70 parts of polyurethane high polymer material, 9 to 17 parts of pulverized fuel ash, 10 to 14 parts of ethyl petrol stearate, 5 to 15 parts of palmitic acid, 2 to 4 parts of nanosilicon dioxide, 2 to 4 parts of nano calcium carbonate, 10 to 16 parts of nanometer titania, 9 to 15 parts of nano-zinc oxide, 6 to 10 parts of activated carbon, 5 to 9 parts of bentonite, 4 to 8 parts of boron fiber, 6 to 8 parts of polypropylene fiber, 3 to 5 parts of kieselguhr, 0.3 to 0.9 part of heat stabilizer, 0.5 to 0.9 part of light stabilizer, 0.5 to 0.9 part of coupling agent, 0.3 to 0.7 part of antioxidant, and 0.4 to 0.6 part of foaming agent. The preparation method comprises the following steps of (1) weighing the raw materials; (2) preparing a mixture a; (3) preparing a mixture b; (4) preparing a mixture c; (5) entering a mould for forming. The building material with the air purification function and the preparation method thereof provided by the invention solve the problem that the functions of air purification, compression resistance, tensile strength and heat insulation of an existing building material need to be improved.
Owner:合肥聪亨新型建材科技有限公司

Nano-material with air purifying function and preparation method thereof

The invention provides a nano-material with an air purifying function and a preparation method thereof, belonging to the technical field of nano-materials. The nano-material with the air purifying function comprises the following raw materials by weight: 60 to 80 parts of a polyurethane high-polymer material, 9 to 15 parts of quartz stone flour, 10 to 14 parts of ethyl stearate, 5 to 15 parts of palmitic acid, 2 to 4 parts of nanometer silica, 2 to 4 parts of nanometer calcium carbonate, 10 to 16 parts of nanometer titanium dioxide, 3 to 5 parts of a stabilizing agent additive, 0.5 to 0.9 part of a coupling agent, 0.3 to 0.7 part of an anti-oxidant and 0.4 to 0.8 part of a foaming agent. The preparation method comprises the following steps: (1) weighing of the raw materials; (2) preparation of a mixture a; (3) preparation of a mixture b; (4) preparation of a mixture c; and (5) charging of a mold and molding. The nano-material prepared in the invention has the advantages of high strength, good heat insulation performance and air purifying performance.
Owner:HEBEI JIASHICHENG ENERGY TECH CO LTD

Preparation method of hyperbranched modified azobenzene and acrylate copolymer emulsion

ActiveCN104140504AImprove photochromic performanceWith optical propertiesTenebresent compositionsEmulsionMagnetic stirrer
The invention relates to a preparation method of a hyperbranched modified azobenzene and acrylate copolymer emulsion. An emulsion polymerization reaction is carried out in a four-hole bottle provided with a condenser tube, a mechanical stirrer and a constant voltage funnel by adopting a pre-emulsification technology under the protection of nitrogen. The method comprises the following steps: pre-emulsifying methyl methacrylate, butyl acrylate monomer, sodium dodecyl sulfat, deionized water and hyperbranched modified azobenzene in a constant temperature magnetic stirrer; and adding the above obtained pre-emulsion and an ammonium persulfate solution to the four-hole bottle, and reacting under stirring to obtain the hyperbranched modified azobenzene and acrylate copolymer emulsion. The hyperbranched modified azobenzene and acrylate emulsion copolymerization reaction method has the advantages of simple operation process, abundant sources of raw materials, extensive applicability and easy industrial production.
Owner:JIANGSU YINBAO AGRI SCI RES INST CO LTD

Nanometer material having formaldehyde absorbing function, and preparation method thereof

InactiveCN107189404AHas the function of absorbing formaldehydeHigh strengthAntioxidantThermal insulation
The present invention provides a nanometer material having a formaldehyde absorbing function, and a preparation method thereof, and relates to the technical field of nanometer materials, wherein the raw materials comprise, by weight, 60-70 parts of a polyurethane polymer material, 9-13 parts of fly ash, 10-14 parts of isopropyl stearate, 5-13 parts of palmitic acid, 2-4 parts of nano-silica, 2-4 parts of nanometer calcium phosphate, 11-17 parts of diatomaceous earth, 10-16 parts of active carbon powder, 3-7 parts of a stabilizer additive, 0.5-0.7 part of a coupling agent, 0.2-0.4 part of an antioxidant, and 0.2-0.8 part of a foaming agent. The preparation method comprises: (1) weighing raw materials, (2) preparing a mixture a, (3) preparing a mixture b, (4) preparing a mixture c, and (5) feeding into a mold, and molding. The prepared nanometer material of the present invention has advantages of high strength, good thermal insulation performance, and formaldehyde absorption.
Owner:HEBEI JIASHICHENG ENERGY TECH CO LTD

Low-refractive index film, method for forming the low-refractive index film, and antireflection film

This invention provides a method for low-refractive index film formation, which can form a thin film having a uniform composition distribution within the film and a low-refractive index, a low-refractive index film formed by the method for low-refractive index film formation, and an antireflection film using the low-refractive index film. The method for low-refractive index film formation comprises forming a low-refractive index film formed of MgF2-SiO2 on a substrate (11) by reactive sputtering. Targets (4A, 4B) as a sinter of MgF2-SiO2 are provided. An alternating voltage having a frequencyof 20 to 90 kHz is applied across the substrate (11) and the targets (4A, 4B) under a mixed gas atmosphere composed of inert gas and O2 for sputtering deposition.
Owner:SONY CORP

Crystal glass mosaic patch

The invention discloses a crystal glass mosaic patch, and belongs to the technical field of building materials. The mosaic patch comprises a medium layer, and a plurality of mosaic blocks adhered on the medium layer; combined plastic layers are arranged in the mosaic blocks; a cover bag is connected to the bottom surface of the medium layer; adhesive is stored in a space surrounded with the bottom surface and the cover bag; a belt strip for opening is arranged at the outer part of the cover bag. With the adoption of the crystal glass mosaic patch, the problems of simple pattern and color and easy falling down from the adhered wall of the existing crystal glass mosaic patch can be solved.
Owner:岑溪市新建球陶瓷有限公司

Flame-retardant anticorrosive coating material for outdoor power equipment, and preparation method thereof

The invention discloses a flame-retardant anticorrosive coating material for outdoor power equipment, and a preparation method thereof, wherein the flame-retardant anticorrosive coating material is prepared from the following raw materials by weight: 20-30 parts of a phosphorus-containing phenol formaldehyde resin, 1-5 parts of a fluorine-silicon polymer three-proofing aid, 15-25 parts of an epoxyresin, 8-12 parts of a polyamide resin, 5-8 parts of polymethyl acrylate, 6-9 parts of nanometer silicon dioxide, 1-4 parts of nanometer titanium dioxide, 8-12 parts of nanometer zinc oxide, 2-6 parts of a silane coupling agent and 15-25 parts of a solvent. According to the invention, the flame-retardant anticorrosive coating material has advantages of good flame retardancy, good water resistance, good oil resistance, good antifouling property, good weather resistance, good aging resistance, good corrosion resistance, good rust resistance, high bonding strength with equipment, simple preparation method and good application prospects.
Owner:广西凯威铁塔有限公司

High-strength pervious concrete suitable for sponge city construction and preparation method of high-strength pervious concrete

The invention discloses high-strength pervious concrete suitable for sponge city construction and a preparation method, and particularly relates to the technical field of concrete materials, and the high-strength pervious concrete comprises cement, composite fibers, a composite reinforcing agent, water, a water reducing agent, a quick-setting early strength agent and aggregate. The composite fiber and the composite reinforcing agent in the formula are matched for use, so that the strength and the water permeability of the concrete can be effectively enhanced; the glass fibers, the basalt fibers and the polypropylene fibers are matched for use, so that the internal structural strength of the concrete can be further enhanced, and meanwhile, the composite fibers form a fiber network in the concrete, so that the high water permeability of the concrete can be effectively enhanced; and the nano silicon dioxide, the nano zirconium diboride powder and the nano silicon nitride in the composite reinforcing agent are matched to modify the composite fibers, so that the structural strength and the self performance of the composite fibers can be effectively enhanced, and the structural strength and the water permeability of the concrete are further improved.
Owner:扬州通惠系统集成科技有限公司

Special material for flame-retardant plastic sheets for steel coil packaging, and preparation method thereof

The invention discloses a special material for flame-retardant plastic sheets for steel coil packaging. The raw materials of the special material comprise, by weight, 80 parts of PC / ABS, 1-2 parts ofa silane coupling agent, 2-4 parts of muscovite powder, 4-8 parts of a toughening agent, 15-20 parts of a plasticizer, 8-15 parts of a flame retardant, 0.3-0.5 part of an antioxidant, 0.2-0.5 part ofa lubricant, 0.1-0.3 part of nano-silica and 0.1-0.3 part of wollastonite powder. The invention also discloses a preparation method of the special material for flame-retardant plastic sheets for steelcoil packaging. The preparation method comprises the following steps: (1) uniformly mixing the PC / ABS, the silane coupling agent, the muscovite powder, the toughening agent, the plasticizer, the flame retardant, the antioxidant, the lubricant, nano-silica and the wollastonite powder; and (2) transferring the obtained mixture into a twin-screw extruder, and carrying out melt extrusion granulationmolding under a vacuum condition by the twin-screw extruder. The special material for the flame-retardant plastic steel sheets for steel coil packaging has good mechanical properties, and meets the using requirements of steel coil packaging materials.
Owner:武汉市太行冶金材料有限公司

Optical device, light source device and projector

An optical device, a light source device, and a projector are provided. The optical device capable of inhibiting optical element degradation and achieving long service lifetime is provided, and includes a reflecting plate (4A1) and a rotation member (6) that dissipates the heat of the reflecting plate (4A1). The rotation member (6) includes a base portion (61) placed on the reflecting plate (4A1) and a plurality of blade portions (62) that project to the side opposite to the base portion (61). The plurality of blade portions (62) each includes an inclined portion (62a) that is inclined with respect to the base portion (61).
Owner:SEIKO EPSON CORP

Poly(alpha-carbonyl diazo alkane) as well as preparation method and application thereof

The invention discloses a polymer, namely poly(alpha-carbonyl diazo alkane), of which a main chain contains diazo groups as well as a preparation method and an application thereof. The preparation method comprises the following steps: by adopting polyheterocyclic radical-copper (II) as a catalyst, catalyzing an alpha-carbonyl diazo compound, preparing highly-functionalized poly(alpha-carbonyl diazo alkane) by virtue of polymerization, and ensuring that nitrogen is not easy to release by virtue of stabilization effects of polyheterocyclic radicals on reactive intermediate diazo free radicals, so that poly(alpha-carbonyl diazo alkane) of which a main chain contains the diazo groups and a side chain contains carbonyl functional groups can be prepared by participating in polymerization reaction by virtue of gradual transfer and insert steps. The preparation method disclosed by the invention is of a novel method for preparing the polymer with optical performance and high functionalization, and can be applied to the fields of optics, dyes, oil paint, printing, blending materials and the like.
Owner:WUHAN UNIV

Full-automatic acupuncture reinforcing and reducing therapeutic apparatus

The invention discloses a full-automatic acupuncture reinforcing and reducing therapeutic apparatus. The full-automatic acupuncture reinforcing and reducing therapeutic apparatus comprises a plurality of acupuncture structures, each acupuncture structure is electrically connected with a console, each acupuncture structure comprises a shell, when the full-automatic acupuncture reinforcing and reducing therapeutic apparatus is used, a bioelectricity signal is obtained through a microelectrode and sent to the console, and the console analyzes the bioelectricity signal; a first group of electromagnetic units are started and a second group of electromagnetic units are closed, so that a piston rod of an air cylinder is attracted and connected with a first magnet on a lifting and inserting rod, and the air cylinder drives needles on the lifting and inserting rod to move up and down to generate lifting and inserting reinforcing and reducing, or the first group of electromagnetic units are closed and the second group of electromagnetic units are started. A screw rod is attracted and connected with a second magnet at the top of a twisting rod, and the piston rod drives a nut to move up and down along the screw rod, so that the screw rod drives the twisting rod to rotate and drives a needle on the lifting and inserting rod to rotate to generate twisting reinforcing and reducing.
Owner:中国人民解放军陆军特色医学中心

A kind of synthetic method of cinnoline salt compound

The invention belongs to the technical field of organic synthesis, and in particular relates to a synthetic method of cinnoline salt compound, which is to compound the compound shown in formula (I) and formula (II) under the action of a composite catalytic system composed of metal catalyst-auxiliary ) compound shown in catalyzed cyclization reaction to obtain the cinnoline salt compound shown in formula (III). The invention provides a method for synthesizing a nitrogen-containing internal salt structure. The synthesis method can obtain the target product with good yield through a unique composite catalytic system and mutual synergy and promotion between components and conditions. It provides a new method for the synthesis of nitrogen-containing inner salt compounds, and the corresponding products have certain optical properties, and have good research value and application potential.
Owner:WENZHOU UNIVERSITY

A device for magnetic nanoparticle self-assembled photonic crystal fiber

The invention discloses a device for a magnetic nanoparticle self-assembly photonic crystal fiber, which comprises a wide-spectrum laser, a single-mode fiber, a trace liquid injector, a liquid inlet, a quartz capillary, a left high-voltage electromagnetic coil, a right high-voltage electromagnetic coil, a high-power microscopic observer, an ultraviolet light curing device, a liquid outlet, a trace liquid collector and a detector. According to the invention, a UV glue liquid containing magnetic nanoparticles is injected into a the quartz capillary by using the trace biological injector, the magnetic nanoparticles are enabled to accomplish a periodically arranged photonic crystal structure with the aid of a high-frequency magnetic field, the self-assembly structure and morphology of the nanoparticles are monitored in real time by using the high-power microscopic observer, variations of a transmission spectrum are monitored in real time through the wide-spectrum laser and the detector, and the ultraviolet light curing device is started to acquire a self-assembly photonic crystal fiber. Compared with a traditional photonic crystal fiber manufacturing process, the method disclosed by the invention is low in cost, high in preparation speed, simple in required equipment, flexible and controllable in fiber parameter and capable of saving the manufacturing cost of the photonic crystal fiber.
Owner:NORTHEASTERN UNIV LIAONING

Synthesis method for cinnoline salt compound

The invention belongs to the technical field of organic synthesis, and particularly relates to a synthesis method for a cinnoline salt compound. The synthesis method comprises the following step: carrying out a catalytic cyclization reaction on a compound as shown in a formula (I) and a compound as shown in a formula (II) under the action of a composite catalysis system comprising a metal catalystand assistants so as to obtain the cinnoline salt compound as shown in a formula (III). The invention provides a synthesis method of a nitrogen-containing inner salt structure. According to the synthesis method, target products with good yield can be obtained through a unique composite catalytic system and the mutual cooperation and promotion effect of components and conditions; a brand new method is provided for the synthesis of nitrogen-containing inner salt compounds; and the corresponding products have certain optical properties, and present good research value and application potential.
Owner:WENZHOU UNIVERSITY

Preparation method of NaV2O5 crystal material with right angle morphology

The invention relates to a preparation method of a NaV2O5 crystal material with right angle morphology. The method comprises the following steps: a), dissolving an aromatic acid organic matter in water, adding a sodium hydroxide solution under the condition of stirring at room temperature, adding a solvent, and stirring for 40-60 minutes at room temperature so as to obtain an evenly mixed solution; b), adding ammonium metavanadate in the mixture so as to obtain a yellow and transparent mixed liquid, transferring the mixture into a stainless steel reaction kettle with a polytetrafluoroethylenelining after stirring for 3 hours, and then placing the reaction kettle in a constant-temperature drying oven of 150-200 DEG C to age for 2-60 days; and c), taking out and filtering the mixture finally obtained in the step b), drying the mixture in the constant-temperature drying oven of 40-60 DEG C so as to finally obtain the NaV2O5 crystal material with a right angle L shape. In the preparationmethod provided by the invention, ammonium metavanadate is adopted as a reactant, an alkaline solvent system of the organic matter in water / absolute ethyl alcohol is used, thus the preparation methodis environment-friendly, has simple preparation process and utilizes simple equipment, and the obtained NaV2O5 crystal material with L shape can be used for research on nano optical devices.
Owner:HEBEI UNIV OF TECH
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