The invention discloses a preparation method of a
TiN tension
coating on the surface of oriented
silicon steel, which belongs to the field of
silicon steel tension coatings and comprises the following steps: brushing a precursor solution containing a
titanium ion complex on the surface of
silicon steel, and carrying out heat treatment on the silicon steel at a temperature higher than a first temperature. In the heating process of heat treatment, when the temperature is lower than a first temperature, the silicon steel is protected by
inert atmosphere, when the temperature is higher than the first temperature, the ligand of the introduced
ammonia gas and
titanium ion complex is an organic ligand, and the first temperature is higher than the degradation temperature of the organic ligand. The compact
titanium nitride tension
coating can be prepared on the silicon steel, the area and the shape of the silicon steel are not limited, large-area
brush coating can be achieved,
brush coating and heat treatment can be matched with the silicon steel preparation process, the cost of improvement on original silicon steel production equipment is low, and the
atmosphere is controlled in stages according to the temperature, so that the prepared coating is compact and good in film forming quality; and the
binding force between the coating and the silicon steel is strong.