The invention relates to the technical field of material preparation, and discloses a method for preparing
tungsten-
molybdenum alloy powder through
coprecipitation of
tungsten molybdate, which comprises the following steps: mixing
sodium tungstate,
sodium molybdate and water to prepare a
tungsten-
molybdenum mixed solution; mixing the tungsten-
molybdenum mixed solution with a
lead salt precipitator; under the stirring state, tungsten and molybdenum are subjected to a co-
precipitation reaction; after the reaction, carrying out
solid-liquid separation and washing on the
slurry to obtain
solid which is
lead tungstate and
molybdate coprecipitation wet
slag and liquid which is
precipitation mother liquor;
drying and
grinding the wet
slag to obtain
lead tungstate and molybdate
coprecipitation powder; the
lead tungstate and molybdate coprecipitation
powder is placed in
hydrogen flow, reduction reaction is conducted, and the lead
tungstate and molybdate coprecipitation powder is converted into a mixture of tungsten molybdenum
alloy powder and elementary substance lead; and then stopping introducing the
hydrogen, starting a
vacuum pump, and carrying out vacuum treatment, so that the elemental lead is volatilized and condensed into liquid lead in a condensation area to be recovered, and meanwhile, obtaining the unleaded tungsten-molybdenum
alloy powder. The high temperature link of the whole process does not exceed 1100 DEG C, so that the
energy consumption is obviously reduced, and high-purity tungsten-molybdenum alloy powder and
metal lead can be obtained.