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76 results about "Phosphorus pentasulphide" patented technology

Phosphorus pentasulfide is the inorganic compound with the formula P2S5 or dimer P4S10. This yellow solid is the one of two phosphorus sulfides of commercial value. Samples often appear greenish-gray due to impurities.

Preparation method of sulfide solid electrolyte

The invention provides a preparation method of sulfide solid electrolyte and belongs to the field of solid electrolyte. The preparation method comprises the following steps: (1) putting raw materialsincluding sulfur powder, lithium hydride, phosphorus pentasulfide and lithium phosphate into a vacuum drying box and drying; (2) under the protection of an inert atmosphere and weighing the dried rawmaterials in percentage by mass respectively: 15 percent to 40 percent of the sulfur powder, 5 percent to 20 percent of the lithium hydride, 50 percent to 70 percent of the phosphorus pentasulfide and0 to 10 percent of the lithium phosphate; pre-grinding in a mortar for 5 to 20min; adding the raw materials into a sealed ball milling pot; carrying out ball milling at room temperature and at a rotary speed of 200 to 600r/min for 24 to 60h; (3) after ball milling reaction is finished, taking the powder out from the ball milling pot under the inert atmosphere; adding the powder into a crucible and sintering in a high-temperature tubular furnace under a nitrogen atmosphere, wherein the sintering temperature is 200 to 400 DEG C and the sintering time is 2 to 6h; taking the powder out from the crucible to obtain the sulfide solid electrolyte. The preparation method of the sulfide solid electrolyte, provided by the invention, has the characteristics of simple technology, low raw material costand easiness for industrialized production.
Owner:UNIV OF SCI & TECH BEIJING

Novel process for producing thiabendazole

The invention discloses a process for producing thiabendazole. The process includes carrying out condensation reaction on lactic acid and o-phenylenediamine in acidic aqueous solution(with, but not limited to, hydrochloric acid); regulating pH (potential of hydrogen) values to obtain 2-alpha-hydroxyl ethyl benzimidazole; placing the 2-alpha-hydroxyl ethyl benzimidazole in a container with acetone and sulfuric acid (but not limited to sulfuric acid, or hydrochloric acid and other inorganic acid and strong acid and weak alkali salt) and carrying out oxidation reaction on the 2-alpha-hydroxyl ethyl benzimidazole and potassium permanganate (but not limited to potassium permanganate, or hydrogen peroxide and organic peroxide); carrying out extraction, desolvation and drying to obtain 2-acetyl benzimidazole; placing the 2-acetyl benzimidazole in a container with glacial acetic acid and carrying out halogenations reaction on the 2-acetyl benzimidazole and bromine (but not limited to, or chlorine and other halogens); drying filter cake to obtain 2-dibromomethane acetyl benzimidazole hydrobromide; carrying out reaction on formamide and phosphorus pentasulfide in a container with ethyl acetate to obtain thioformamide; removing phosphorus pentoxide by means of filter-press by the aid of nitrogen to obtain thioformamide/ethyl acetate solution and carrying out cyclization reaction on the thioformamide/ethyl acetate solution and 2-dibromomethane acetyl benzimidazole; purifying reaction products and regulating pH (potential of hydrogen) values to obtain the thiabendazole with the content higher than or equal to 99%. The acetone and the sulfuric acid in the corresponding container are used as solvents. The glacial acetic acid in the corresponding container is used as a solvent. The ethyl acetate in the corresponding container is used as a solvent. The process has the advantages that the cost can be lowered, risks in the aspects of safety and environmental protection can be reduced, environmental pollution can be abated, and the production efficiency can be improved; integral reaction procedures are carried out at the normal temperatures under the normal pressures, accordingly, reaction conditions are mild, the yield of the reaction at each step is quite stable, and the overall yield measured by the aid of the o-phenylenediamine can reach 75% at least.
Owner:孟宪锋

Production technology for synthesizing high-purity phosphorus pentasulfide by liquid-phase continuous process

The invention relates to production technology for synthesizing high-purity phosphorus pentasulfide by liquid-phase continuous process, which belongs to the field of preparation of fine phosphorus chemical products in chemical industry. The production technology for synthesizing high-purity phosphorus pentasulfide by liquid-phase continuous process comprises the following steps: after melting and precipitating solid yellow phosphorus and solid sulphur, continuously conveying the melted and precipitated solid yellow phosphorus and solid sulphur into a reaction kettle with a pump in the ratio of 1 to 2.6, stirring under the condition of 400 DEG C and 0.15 MPa to perform liquid phase reaction, continuously pumping reacted raw materials into a distillation still, performing negative pressure distillation in the distillation still by using reaction heat, condensing formed phosphorus pentasulfide steam by reduced pressure distillation into liquid phosphorus pentasulfide by using a condenser, concentrating the liquid phosphorus pentasulfide into a phosphorus pentasulfide product storage tank, conveying the product into a pelleter with the pump, processing the product into sheet, crushing, grinding and finally packaging into finished products. The production technology for synthesizing high-purity phosphorus pentasulfide by liquid-phase continuous process has the advantages of simple operation, stability and safety, low energy consumption, high degree of automation and excellent product quality.
Owner:LIAONING PROVINCE PETROLEUM CHEM IND PLANNING&DESIGNING INST

All-solid sodium secondary battery electrolyte and preparation method and application thereof

The invention provides an all-solid sodium secondary battery electrolyte and a method and application thereof. The all-solid sodium secondary battery electrolyte is prepared from a first component anda second component, wherein the first component is selected from Na2S (sodium sulfide) and/or Na2Se (disodium selenide); the second component is selected from one or multiple of Sb2S3 (antimony trisulfide), Sb2Se3 (antimony triselenide), Sb2S5 (antimony pentasulfide), Sb2Se5 (antimony pentaselenide), P2S5 (phosphorus pentasulfide), P2S3 (phosphorus trisulfide), As2S3 (arsenic trisulfide), As2S5 (arsenic pentasulfide), S (sulfur), Se (selenide), SnS2 (selenide disulfide), SiS2 (silicon disulfide), SnS (selenide sulfur), GeS2 (germanium disulfide) and GeS (germanium sulfide); the granularity ofthe all-solid sodium secondary battery electrolyte is 10nm to 10mum; the raw materials also comprise doping matters, and the doping matters are selected from one or multiple of a third component, oxide and halide; the third component and the second component are different. The all-solid sodium secondary battery electrolyte has the advantages that the sodium ion conductivity is higher in an all-solid sodium secondary battery; the electrochemical window is broader; the all-solid sodium secondary battery prepared by the electrolyte has good rate and cycle properties.
Owner:NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI
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