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37results about How to "Sensitive to discoloration" patented technology

Low-temperature reversible chromotropic pigment and preparation method thereof, temperature-sensitive pavement marking coating and preparation method and application thereof

The invention relates to low-temperature reversible chromotropic pigment and a preparation method of the low-temperature reversible chromotropic pigment, a temperature-sensitive pavement marking coating and a preparation method and application of the temperature-sensitive pavement marking coating. The preparation method of the low-temperature reversible chromotropic pigment comprises the followingsteps: firstly, uniformly mixing a hidden body, a chromogenic agent and a regulator, heating, carrying out heat preservation and then naturally cooling to obtain a low-temperature reversible chromotropic compound solution; adjusting the pH value to be 3 to 6 after emulsifying the low-temperature reversible chromotropic compound solution, rising the temperature after adding a resin prepolymer solution, cooling to the temperature of 30 to 40 DEG C after stopping the reaction, adding a dispersant I to be uniformly dispersed, carrying out suction filtration, washing and drying to obtain the low-temperature reversible chromotropic pigment; the temperature-sensitive pavement marking coating is prepared from the low-temperature reversible chromotropic pigment and a filler, a dispersant II, a wetting agent, acrylic emulsion, a film-forming additive and the like, and can be used for preparing temperature-sensitive pavement marks. The low-temperature reversible chromotropic pigment prepared bythe invention can produce color reversible changes when the temperature changes, and the temperature-sensitive pavement marks are prepared, thereby being capable of reminding a user of icy pavements timely to reduce traffic accidents.
Owner:CHANGAN UNIV

Detection test paper for content of micro-water in aviation fuel and preparation method of detection test paper

The invention relates to detection test paper for the content of micro-water in aviation fuel and a preparation method of the detection test paper. The detection test paper comprises filter paper and a detection composition, wherein the surface of the filter paper is uniformly coated with the detection composition; the detection composition comprises a first component and a second component; the first component is selected from cyanate and/or thiocyanate; and the second component comprises one or more metal ions of Fe<2+>, Fe<3+>, Cu<2+>, Cu<+> and Co<2+>. The preparation method comprises the following steps: uniformly mixing the first component and the second component, and coating the surface of the white filter paper with the mixture, thus obtaining the detection test paper. The detection test paper provided by the invention is changed in color in water; the obviousness of the color change has a corresponding relation with a water content range at 5 to 50 ppm; at a water content critical point of 30 ppm, the color changes obviously; at a low free water content, such as 10 ppm, developing can be realized sensitively, and the detection test paper is convenient to use; and moreover, the preparation method is simple, low in cost and long in storage period.
Owner:THE SECOND RES INST OF CIVIL AVIATION ADMINISTRATION OF CHINA

PH value sensitive micro capsule as well as preparation method and application thereof

The invention discloses a preparation method of a pH value sensitive micro capsule. The preparation method comprises the following steps: step 1, mixing pH value sensitive silica gel coated with an organic liquid layer and provided with a primary pore passage with an emulsifier aqueous solution; step 2, adding a high-molecular-weight water-soluble prepolymer containing urea and formaldehyde and alow-molecular-weight water-soluble prepolymer containing urea and formaldehyde into the mixed solution obtained in the step 1, and reacting at 45-55 DEG C for 2-3 hours to obtain micro capsules; step3, soaking the micro capsules prepared in the step 2 in ethanol, and dissolving low-molecular-weight urea-formaldehyde resin to form a secondary pore passage; and cleaning and drying the micro capsules with the composite holes to obtain a target product. The invention also discloses an application of the pH value sensitive micro capsule. The pH value sensitive micro capsule with a composite structure is prepared by matching the raw materials with the preparation process, and the pH value sensitive micro capsule is sensitive in pH color change and stable in structure; when being applied to textiles, the pH value sensitive micro capsule has an obvious indication effect on acidity, and meanwhile, the rubbing color fastness and the washing color fastness meet corresponding national standards.
Owner:JINHUA JIELING HOUSE WARES CO LTD

Aviation fuel free water detection test paper as well as preparation method and detection device thereof

The invention relates to the technical field of aerospace, and in particular, relates to aviation fuel free water detection test paper as well as a preparation method and a detection device thereof. The detection test paper comprises filter paper, potassium ferricyanide loaded on the surface of the filter paper, and a mixture of ferrous sulfate and a chelating agent. The preparation method of theaviation fuel free water detection test paper comprises the steps: infiltrating the filter paper into a K3[Fe(CN)6] solution, and then drying to obtain intermediate detection test paper; and coating the surface of the intermediate test paper with a powder mixture of FeSO4 and the chelating agent on. The aviation fuel free water detection test paper provided by the invention has the following advantages that the detection method is simple and convenient, easy to operate, free of specialization and instruments, convenient to use, capable of detecting by naked eyes, intuitive, concise, rapid andefficient; the detection sensitivity is high; the effective service life is long, whether failure occurs or not can be easily judged through visual color change, and the detection reliability is improved; the production cost is low.
Owner:THE SECOND RES INST OF CIVIL AVIATION ADMINISTRATION OF CHINA

Preparation method of medical carbon dioxide adsorbent calcium lime

The invention discloses a preparation method of medical carbon dioxide adsorbent calcium lime. The medical carbon dioxide adsorbent calcium lime comprises the following components in percentage by weight: 50 to 55 percent of a main absorbent, 3 to 5 percent of a wetting agent, 3 to 5 percent of lithium hydroxide, 3 to 5 percent of triethanolamine, 3 to 5 percent of an enhancer, 3 to 5 percent of polyvinyl alcohol, 3 to 5 percent of a PH indicating coloring agent, 3 to 5 percent of a disintegrating agent and the balance of water. The preparation method specifically comprises the following preparation steps: 1, preparing the main absorbent, pulverizing and passing through a 800-mesh sieve to obtain main absorbent powder for future use; 2, mixing the main absorbent, the wetting agent and theenhancer according to the mass percentage ratio of 77:4:3 to perform preparation, stirring for 1 hour until the materials are basically uniform, preparing a PVA solution with the mass percentage of 8percent by weight according to a water bath method, and preparing a pH indicating coloring agent solution of 15 g/L. Calcium hydroxide serves as a main component, the calcium hydroxide can react withacidic gas CO2, has certain hardness and is not liable to absorb moisture, and lots of heat is not generated during preparation, so that the cost is low, and the whole process is simple, safe, controllable and suitable for being widely popularized.
Owner:江苏立峰生物科技有限公司

Method for preparing forward-switched reversible thermochromic composite film

The invention discloses a method for preparing a forward-switched reversible thermochromic composite film and relates to preparation methods for reversible thermochromic composite films. The object of the invention is to solve the problems that the existing thermochromic films are reversely switched, are chromogenic at room temperature and are achromatic during heating-up, and the apparent integrity of a product can be destroyed and the attractiveness of the product is affected when the existing thermochromic films are applied to the surface of the product. The method comprises the steps: (1) pretreating a glass plate; (2) preparing a mixed solution; (3) preparing a coating solution; and (4) carrying out spraying and drying, thereby obtaining the forward-switched reversible thermochromic composite film. The reversible thermochromic composite film prepared by the method is forwardly switched, are achromatic at room temperature and are chromogenic during heating, so that the aim of keeping integrity of the product can be achieved when the reversible thermochromic composite film is applied to the surface of the product; and the forward-switched reversible thermochromic composite film prepared by the method has relatively good elastoplasticity and is environmentally friendly, environment-friendly, non-toxic and harmless. The invention can achieve the method for preparing the forward-switched reversible thermochromic composite film.
Owner:NORTHEAST FORESTRY UNIVERSITY

Synthesis method of POS-based membrane material with reversible color change and ultraviolet shielding functions

The invention relates to a synthesis method of a POSS-based membrane material with reversible color change and ultraviolet shielding functions, belonging to the technical field of synthesis of POSS-based materials. The method solves the problems that at present, materials with both thermochromism and ultraviolet shielding performance are few, and the application range of POSS is fixed. The method comprises the steps: dissolving POSS in water; adding a copper salt and a chromium salt into the POSS aqueous solution, and stirring at room temperature for 3 hours; and stirring at 20-40 DEG C for 1-24 hours, and volatilizing the solvent at 20-80 DEG C to obtain the POSS-based membrane material with reversible color change and ultraviolet shielding functions. The POSS-based membrane material with reversible color changing and ultraviolet shielding functions is synthesized for the first time, the POSS-based membrane material is changed from green to luminous yellow at 80 DEG C and is obvious in color changing, the membrane material almost has no ultraviolet transmittance at 200-400 nm, the ultraviolet transmittance is almost 0%, and the POSS-based membrane material can be used as an ultraviolet shielding material. According to the room-temperature synthesis and environment-friendly method disclosed by the invention, POSS is simultaneously applied to the fields of color change and ultraviolet shielding.
Owner:HARBIN INST OF TECH

Preparation method and detection device of aviation fuel free water detection test paper

The invention relates to the field of aerospace technology, in particular to a test paper for detecting free water in aviation fuel, a preparation method and a detection device thereof. The detection test paper comprises: filter paper, and a mixture of potassium ferricyanide, ferrous sulfate and a chelating agent loaded on the surface of the filter paper. The preparation method of aviation fuel free water detection test paper includes: soaking the filter paper in K 3 [Fe(CN) 6 ] solution, and then dried to obtain the intermediate detection test paper; the surface of the intermediate detection test paper is coated with FeSO 4 Powder mix with chelating agent. The aviation fuel free water detection test paper provided by the present invention has the following advantages: the detection method is simple, easy to operate, no specialization is required, no instrument is needed, it is convenient to use, it can be detected with the naked eye, intuitive and simple, fast and efficient; high detection sensitivity; effective service life Long, it is easy to judge whether it is invalid through the intuitive color change, and the reliability of detection is improved; the production cost is low.
Owner:THE SECOND RES INST OF CIVIL AVIATION ADMINISTRATION OF CHINA

Humidity-sensitive color-changing microcapsule and preparation method and application thereof

The invention discloses a humidity-sensitive color-changing microcapsule and a preparation method. The preparation method comprises the following steps: step 1, weighing 20-40 parts by mass of anthocyanidin, 10-12 parts by mass of an emulsifier, 6-8 parts by mass of a color developing agent and 6-8 parts by mass of an accelerant, dissolving the weighed materials in an organic solvent, and stirring the materials at 70-75 DEG C and 150-300 r / min for 1-2 h to obtain an organic solvent / anthocyanidin mixed solution; step 2, dropwise adding a certain amount of tetraethyl orthosilicate and a silane coupling agent into the mixed solution in the step 1, adding a reagent for adjusting the pH value to enable the pH value to be 9, and stirring and reacting at 70-75 DEG C and 150-300r / min for 1.5-2.5 hours so as to obtain a uniformly dispersed microcapsule suspension; and step 3, removing the solvent from the microcapsule suspension prepared in the step 2 through reduced pressure distillation, and drying at 50 DEG C for 12 hours to obtain the anthocyanin / SiO2 microcapsule. The humidity-sensitive color-changing microcapsule wall material has a porous structure and a hydrophilic material, and is printed on a fabric in a screen printing manner, and the fabric is sensitive in color change when meeting humidity, high in reversible resilience and reusable.
Owner:JIANGNAN UNIV
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