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336results about How to "Avoid overgrowth" patented technology

Multi-layer graphene/lithium iron phosphate intercalated composite material, preparation method thereof, and lithium ion battery adopting multi-layer grapheme/lithium iron phosphate intercalated composite material as anode material

The invention relates to a lithium iron phosphate intercalated composite material, a preparation method thereof and a lithium ion battery adopting the multi-layer graphene / lithium iron phosphate intercalated composite material as an anode material. In the prior art, the electronic conductivity of the lithium iron phosphate material is poor, high-rate charging / discharging capacity of the lithium ion battery adopting the lithium iron phosphate material as the anode material is poor. The purpose of the present invention is to solve the problems in the prior art, and improve the rapid charging capacity of the power lithium ion battery so as to meet the requirements of the pure electrocar. The composite material is prepared through the following steps that: a rheological phase reaction method is adopted for multi-layer graphene, a trivalent iron salt, a phosphorus compound, a lithium compound and carbon source of small organic molecule to obtain a composite precursor, then the precursor is sintered to obtain the multi-layer graphene / lithium iron phosphate intercalated composite material. The anode slurry of the lithium ion battery anode plate comprises the composite material, a conductive agent and polyvinylidene difluoride. The composite material is an intercalated structure, wherein the lithium iron phosphate particles are intercalated between the multi-layer graphene to form the intercalated structure. The trivalent iron salt is adopted as the raw material, such that the cost is reduced. The lithium ion battery has good charging / discharging cycle performance, wherein the specific capacity is more than 60 mA.h.g<-1> at the rate of 20C.
Owner:HARBIN INST OF TECH

Method for preparing ternary complex anode material (LiNixCoyMn1-x-yO2)

The invention discloses a method for preparing a ternary complex anode material (LiNixCoyMn1-x-yO2), which is characterized in that the lithium ion battery anode material (LiNixCoyMn1-x-yO2) is prepared by adopting a coprecipitation-silicon cladding-high temperature sintering-desilicication integrated method, and specifically comprises the following steps: mixing a nickel source and a cobalt source with a manganese source according to molar ratio of nickel-cobalt-manganese: x:y:(1-x-y), adding with water, stirring to form a solution, adding with a certain amount of ammonia water and a sodium hydroxide solution to generate a uniform NixCoyMn1-x-y(OH)2 ocyhydrate precursor, washing and filtering the precursor, adding with a certain amount of polyvinylpyrrolidone, stirring for a certain period, adding with a certain quantity of organosilicon reagents, stirring continuously to obtain an ocyhydrate precursor wrapped by organosilicon reagent-polyvinylpyrrolidone, washing, filtering, drying and then mixing the ocyhydrate precursor with a lithium source, calcining the mixture under air or an oxygen atmosphere under the temperature of 450-950 DEG C for 2-48 hours, and removing a silicon wrapping layer on a product by the utilizing a sodium hydroxide solution, thus obtaining the nanoscale or standard nanoscale lithium ion battery ternary complex anode material (LiNixCoyMn1-x-yO2). The particle size of the anode material prepared by the invention ranges from 80nm-180nm, the initial charging/discharging performance achieves 194.4-210.3mAh/g, and the electrochemical performance is excellent.
Owner:CENT SOUTH UNIV

Method for manufacturing nanometer tungsten/cobalt carbide composite powder

The invention discloses a method for manufacturing nanometer tungsten/cobalt carbide composite powder. The method is characterized by comprising technological steps of firstly, dissolving, by mass, 55-92% of water-soluble tungsten salt, 3-40% of water-soluble cobalt salt, 3-6% of water-soluble carburizing and nodulizing agents and 0.1-2% of water-soluble composite grain growth inhibitors into water with the mass 3-5 times that of a mixture of the water-soluble tungsten salt, the water-soluble cobalt salt, the water-soluble carburizing and nodulizing agents and the water-soluble composite grain growth inhibitors to prepare mixed aqueous solution; secondly, adding carbon nano-tubes (CNT) accounting for 1-10% of the total mass of the aqueous solution into the mixed aqueous solution obtained in the first step and enabling the carbon nano-tubes to be uniformly mixed in the mixed aqueous solution; thirdly, performing quick low-temperature spray drying for mixed aqueous solution obtained in the second step to obtain precursor powder of ultrafine tungsten and cobalt composite salt; and fourthly, performing reduction synthesis and carbon conditioning at the temperature ranging from 900 DEG C to 1000 DEG C for the precursor powder obtained in the third step to prepare tungsten/cobalt carbide composite powder materials with nanostructures.
Owner:ADVANCED FOR MATERIALS & EQUIP

Water eco-environment protection method based on water plant harvesting

A water eco-environment protection method based on water plant harvesting. The invention relates to a water eco-environment protection method, which is characterized in that water plants are cultivated in a water body or naturally recovered water plants are utilized; nitrogen and phosphorous nutrients are absorbed by water plant growth; the water plants are harvested in growth period by manual work or waterweed harvesting equipment so as to promote the regrowth of the water plants; harvesting is carried out for multiple times, ends in the growth period and is carried out for the last time after the water plants grow seeds or vegetative propagule so as to extract the nitrogen and phosphorus nutrients from water in the form of water plant residues. The invention aims to maximize the accumulated biomass of the water plants during the whole growth period or optimize the water quality purifying effect and simultaneously remove nutrients in the water body and deposits, alleviate the eutrophication process of the water body and prevent the water plants from decaying and polluting the water body once again. The method provided by the invention is suitable for daily ecological maintenance of shallow lakes, urban landscape water, slow flow rivers, small reservoirs, wetlands and ponds.
Owner:RES CENT FOR ECO ENVIRONMENTAL SCI THE CHINESE ACAD OF SCI +1

Capacitor carbon/lithium iron phosphate composite material, preparation method thereof and lithium-ion capacitor battery using same as cathode material

The invention discloses a capacitor carbon / lithium iron phosphate composite material, a preparation method thereof and a lithium-ion capacitor battery using the same as a cathode material and relates to a lithium iron phosphate material, a preparation method and a lithium-ion capacitor battery using the lithium iron phosphate material as a cathode material, solving the problems of higher preparation cost of the traditional lithium iron phosphate and poor high-magnification charge / discharge properties of the lithium-ion batteries prepared from the traditional lithium iron phosphate. The composite material is formed by loading the lithium iron phosphate on activated carbon. The preparation method comprises the following steps of: preparing a lithium iron phosphate precursor by using a trivalent ferric salt, a phosphorus compound, a lithium source compound and an organic micromolecule carbon source as raw materials; and then mixing the precursor with the activated carbon and sintering. In the invention, the cathode sizing agent of the lithium-ion capacitor battery comprises the capacitor carbon / lithium iron phosphate composite material, a conductive agent and a bonding agent; the particle size distribution of the composite material is uniform; the trivalent ferric salt is used as a raw material, and the cost on the preparation is low; and the capacitor battery has good charge / discharge cycle performances and the mass specific capacity larger than 60mA.h.g<-1> under 20C magnification.
Owner:HARBIN INST OF TECH

Method for preparing cathode material lithium vanadium phosphate of lithium ion battery by using fast sol-gel method

The invention discloses a method for preparing a cathode material lithium vanadium phosphate of a lithium ion battery by using a fast sol-gel method, which specifically comprises the following steps of: (1) adding vanadic oxide into the solution of a reducing acid, heating the mixed solution to 60 to 80 DEG C and stirring the mixed solution for 10 to 50 minutes at a constant temperature to obtain blue solution; (2) adding lithium salts into the blue solution, wherein a stoichiometric ratio of the lithium salts to the vanadic oxide is 3-3.2: 2.9-3.05: 0.95-1.05; (3) treating an obtained powder material in an inert atmosphere at 200 to 400 DEG C for 2 to 4 hours to obtain a precursor; and (4) mixing and grinding uniformly the obtained precursor and another carbon source and cooling the mixture to obtain the cathode material lithium vanadium phosphate of the lithium ion battery. The method has the advantages that: (1) a synthesis process is simplified, the cost is reduced and the method is applied to industrial production; (2) the baking time is greatly shortened, the granularity of the product is reduced and the synthesized material has a nano-size; and (3) the carbon source is mixed before baking, carbon granules also can prohibit the growth of material granules and the synthesized material granules are uniform and fine.
Owner:NANCHANG UNIV

Flue-cured tobacco cultivation method resisting spring drought

The invention relates to a flue-cured tobacco cultivation method resisting spring drought. The method comprises the steps that variety distribution is reasonably planned; ditching and ridging are carried out, and a two-row concave ridge which is 200-240cm in width and 20-25cm in height is implemented; for transplantation, seedlings are transplanted early in good time, transplantation is generally finished during the period from the end of March to the middle ten days of April, the method of a well cellar with the diameter of 8-9cm and the depth of 16-20cm is adopted, and a shovel is utilized for marking out a concave furrow which is 8-10cm in width and 2-3cm in depth on the ridge, so that the well cellar is dug easily, and water is prevented from being wasted; fertilizer is applied according to the equal nitrogen principle, and 30-50% of organic nitrogenous fertilizer is additionally applied to soil for the second time; film mulching is carried out, a film is uniformly compacted through soil in a line-shaped mode, and a gap between the surface of the soil and the film is 0.5-1cm. The method simple and easy to implement is adopted for carrying out flue-cured tobacco cultivation, harm to growth and development of flue-cured tobaccos due to the drought can be reduced, an effective yield increase way is provided for tobacco-growing areas suffering from the drought, the output value is increased, and the economic benefit is increased.
Owner:WEINING COUNTY BRANCH OF BIJIE CITY TOBACCO +1

Preparation method of dispersion fuel pellet with high uranium loading capacity

The invention discloses a preparation method of a dispersion fuel pellet with high uranium loading capacity, which comprises the steps of firstly adopting means such as pelleting, self-grinding balling and rolling coating to realize the balling of a uranium-based fuel and the coating with a reinforcing phase, then performing high temperature plasma sintering on a coated ball to obtain the uranium-based fuel pellet; forming a large amount of pores in a core pellet of the fuel by utilizing the volatilization of a pore-forming agent under high temperature, then promoting the low-temperature rapiddensification sintering of the reinforcing phase by combining the high temperature plasma sintering technology and a sintering aid, thus obtaining the dispersion fuel pellet with high uranium loadingcapacity, wherein the dispersion fuel pellet has a special core-shell structure in which the compact reinforcing phase coats the porous fuel core pellet, and the special core-shell structure is loosein the interior and compact in the exterior. The method has the advantages that the preparation is simple and the preparation cost is low, can be used for the scale production of the uranium-based fuel pellet; the uranium-based fuel pellet prepared by the method has the advantages of high thermal conductivity, high safety, high uranium loading capacity and high economy.
Owner:MATERIAL INST OF CHINA ACADEMY OF ENG PHYSICS

Multicomponent composite fertilizer special for peanuts

The invention discloses a multicomponent composite fertilizer special for peanuts, which belongs to a crop fertilizer. The multicomponent composite fertilizer special for peanuts comprises the following components: 35 percent of total nutrients including 16 percent of nitrogen, 10 percent of phosphorus and 9 percent potassium, more than or equal to 10 percent of medium and trace elements, 7-9 percent of organic matter and 2-5 percent of amino acid. The medium and trace elements comprise trace elements including molybdenum, zinc, manganese, boron and iron. The multicomponent composite fertilizer special for peanuts has the advantages of nutrient content assurance and reasonable proportioning balance. The multicomponent composite fertilizer special for peanuts can effectively improve the immunological competence of the peanuts, regulate endogenous hormone, inhibit the regeneration of insect eggs, activate the activity of root azotobacter, promote root development, quicken nutrient absorption, achieve the functions of strengthening seedlings, promoting growth and promoting flowering, prevent bacterial wilt, continuous cropping symptoms and leaf spots, also prevent excessive growth and take special effect on symptoms including mosaic disease, chlorotic disorder, flocculi, defoliation and the like. After applied, the multicomponent composite fertilizer special for peanuts can effectively improve the percentage of fertile fruits and the thousand grain weight, promote the mellow and full degrees of fruits and achieve remarkable effect of production increase.
Owner:江苏心实肥业集团有限公司
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