A kind of low agglomeration aluminum
nitride powder preparation method, comprising the following steps: S1: 50-60 parts of
aluminum nitrate nine water, 60-80 parts of film-forming solution and 20-30 parts of
glucose monohydrate are mixed uniformly, after stirring 1-2h, it is poured into
polytetrafluoroethylene dish at
room temperature 25 ℃ and is stationary 4-6h, and crosslinked film is obtained;S2: the crosslinked film obtained in step S1 is burned at 300-400 ℃ for 30-40 min in
argon environment, calcined at 800-900 ℃ for 1-2h in
ammonia environment, then at 900-1000 ℃, heat preservation 1-2h, finally at 1200-1400 ℃, calcined 1-2h, and aluminum
nitride powder is obtained.The low agglomeration spherical aluminum
nitride powder machine preparation method of the application, the particle size of the prepared aluminum nitride powder is fine, the agglomeration rate is low, the conversion rate is high and the specific surface area is large.